3-METHOXY-4-NITROBENZALDEHYDE
- Product Name
- 3-METHOXY-4-NITROBENZALDEHYDE
- CAS No.
- 80410-57-7
- Chemical Name
- 3-METHOXY-4-NITROBENZALDEHYDE
- Synonyms
- 3-METHOXY-4-NITROBENZALDEHYDE;Benzaldehyde, 3-Methoxy-4-nitro-;3-Methoxy-4-nitrobenzaldehyde 97%
- CBNumber
- CB7829893
- Molecular Formula
- C8H7NO4
- Formula Weight
- 181.15
- MOL File
- 80410-57-7.mol
3-METHOXY-4-NITROBENZALDEHYDE Property
- Melting point:
- 104 °C
- Boiling point:
- 354.7±27.0 °C(Predicted)
- Density
- 1.322±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- form
- crystalline powder
- color
- Cream/gold/faint tan
Safety
- HS Code
- 2912290090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- M266588
- Product name
- 3-methoxy-4-nitrobenzaldehyde
- Packaging
- 50mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- OR400210
- Product name
- 3-Methoxy-4-nitrobenzaldehyde
- Purity
- 97%
- Packaging
- 1g
- Price
- $127
- Updated
- 2021/12/16
- Product number
- 4654-1-4M
- Product name
- 3-Methoxy-4-nitrobenzaldehyde
- Purity
- 97%
- Packaging
- 1g
- Price
- $140
- Updated
- 2021/12/16
- Product number
- 2531AC
- Product name
- 3-Methoxy-4-nitrobenzaldehyde
- Packaging
- 5g
- Price
- $577
- Updated
- 2021/12/16
- Product number
- OR400210
- Product name
- 3-Methoxy-4-nitrobenzaldehyde
- Purity
- 97%
- Packaging
- 5g
- Price
- $414
- Updated
- 2021/12/16
3-METHOXY-4-NITROBENZALDEHYDE Chemical Properties,Usage,Production
Synthesis
704-13-2
74-88-4
80410-57-7
(1) Synthesis of 3-methoxy-4-nitrobenzaldehyde: 3-hydroxy-4-nitrobenzaldehyde (500 mg, 2.99 mmol) and potassium carbonate (0.42 g, 3.0 mmol) were dissolved in 6.0 mL of N,N-dimethylformamide. Iodomethane (0.38 mL, 6.0 mmol) was slowly added to the reaction system at room temperature, followed by continuous stirring at the same temperature for 5 hours. After completion of the reaction, the reaction mixture was diluted with ethyl acetate and water and separated. The organic layer was washed twice with saturated brine and subsequently dried with anhydrous magnesium sulfate. After filtration, the filtrate was concentrated under reduced pressure and the residue was purified by silica gel column chromatography (eluent: hexane/ethyl acetate = 4/1 to 1/1) to afford the target compound, 3-methoxy-4-nitrobenzaldehyde, as a light yellow powder (518 mg, 96% yield).
References
[1] ACS Medicinal Chemistry Letters, 2017, vol. 8, # 10, p. 1002 - 1006
[2] Patent: WO2016/124747, 2016, A1. Location in patent: Page/Page column 62; 63
[3] Patent: US2018/202388, 2018, A1
[4] Patent: EP2123637, 2009, A1. Location in patent: Page/Page column 19
[5] Organic and Biomolecular Chemistry, 2014, vol. 12, # 30, p. 5629 - 5633
3-METHOXY-4-NITROBENZALDEHYDE Preparation Products And Raw materials
Raw materials
Preparation Products
3-METHOXY-4-NITROBENZALDEHYDE Suppliers
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