ChemicalBook > CAS DataBase List > 3-(DIMETHYLAMINO)BENZALDEHYDE

3-(DIMETHYLAMINO)BENZALDEHYDE

Product Name
3-(DIMETHYLAMINO)BENZALDEHYDE
CAS No.
619-22-7
Chemical Name
3-(DIMETHYLAMINO)BENZALDEHYDE
Synonyms
VinylBenzoate（Assumed）;3-N,N-DIMETHYLBENZALDEHYDE;3-(DIMETHYLAMINO)BENZALDEHYDE;Benzaldehyde, 3-(dimethylamino)-;Benzaldehyde, m-(dimethylamino)-;3-(N,N-Dimethylamino)benzaldehyde;3-(Dimethylamino)benzaldehyde 95%
CBNumber
CB7831522
Molecular Formula
C9H11NO
Formula Weight
149.19
MOL File
619-22-7.mol
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3-(DIMETHYLAMINO)BENZALDEHYDE Property

Boiling point:
137.5-138 °C
Density 
1.072±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
pka
3.67±0.10(Predicted)
form 
liquid
color 
Yellow
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Safety

HS Code 
2922390090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

Rieke Metals
Product number
8139
Product name
3-N,N-Dimethylbenzaldehyde
Purity
97%
Packaging
1g
Price
$318
Updated
2021/12/16
Matrix Scientific
Product number
087143
Product name
3-N,N-Dimethylbenzaldehyde
Purity
97%
Packaging
1g
Price
$319
Updated
2021/12/16
AK Scientific
Product number
W7397
Product name
3-N,N-Dimethylbenzaldehyde
Packaging
1g
Price
$371
Updated
2021/12/16
Apolloscientific
Product number
OR400567
Product name
3-(Dimethylamino)benzaldehyde
Purity
95%
Packaging
1g
Price
$430
Updated
2021/12/16
SynQuest Laboratories
Product number
4656-1-2P
Product name
3-(Dimethylamino)benzaldehyde
Purity
95%
Packaging
1g
Price
$474
Updated
2021/12/16
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3-(DIMETHYLAMINO)BENZALDEHYDE Chemical Properties,Usage,Production

Uses

3-(Dimethylamino)benzaldehyde can be used as a staining agent for identifying non-specific esterase activity in cells. This application is crucial in medical and biological research, as it aids in the detection and analysis of cellular processes and functions.

Synthesis

23501-93-1

619-22-7

General procedure for the synthesis of m-dimethylaminobenzaldehyde from 3-(dimethylamino)benzyl alcohol: commercially available 3-(dimethylamino)benzyl alcohol (750 mg, 5 mmol) was dissolved in a solvent mixture of dichloromethane (DCM) and dimethyl sulfoxide (DMSO). To this solution, triethylamine (Et3N, 2.8 mL, 20 mmol) and sulfur trioxide-pyridine complex (SO3-Py, 1.59 g, 10 mmol) were added sequentially. The reaction mixture was stirred for 2 h at room temperature. After completion of the reaction, dichloromethane was removed by distillation under reduced pressure. Saturated aqueous ammonium chloride (NH4Cl) was added to the residue, which was then extracted with ethyl acetate (EtOAc). The organic phase was washed with water, dried over anhydrous magnesium sulfate (MgSO4) and concentrated under reduced pressure. The crude product was purified by column chromatography (eluent ratio: ethyl acetate/hexane = 1/2) to afford m-dimethylaminobenzaldehyde (670 mg, 90% yield). Mass spectrometry analysis showed [M+H]+ = 150.

References

[1] Journal of Medicinal Chemistry, 2018, vol. 61, # 17, p. 7640 - 7656
[2] Bulletin of the Korean Chemical Society, 2015, vol. 36, # 1, p. 413 - 416
[3] Patent: WO2009/38411, 2009, A2. Location in patent: Page/Page column 36-37
[4] Organic Letters, 2016, vol. 18, # 20, p. 5396 - 5399
[5] Tetrahedron, 2004, vol. 60, # 49, p. 11099 - 11107

3-(DIMETHYLAMINO)BENZALDEHYDE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3-(DIMETHYLAMINO)BENZALDEHYDE manufacturers

Career Henan Chemical Co
Product
3-(DIMETHYLAMINO)BENZALDEHYDE 619-22-7
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
1000KG
Release date
2019-12-18

619-22-7, 3-(DIMETHYLAMINO)BENZALDEHYDERelated Search:

3-(Dimethylamino)benzoic acid 3-(2,5-DIOXO-2,5-DIHYDRO-PYRROL-1-YL)-BENZOIC ACID ACEPROMAZINE MALEATE PIPERACETAZINE (250 MG) (6-[N-(6-AMINOHEXYL)-N-ETHYL]AMINO-2,3-DIHYDRO-1,4-PHTHALAZINE-1,4-DIONE Iohexol ALIZARIN RUBINOL R Metrizamide 3'-DIMETHYLAMINOACETOPHENONE 6-bromo-3-methyl-3H-dibenz[f,ij]isoquinoline-2,7-dione 3-Maleimidobenzoic acid N-hydroxysuccinimide ester sodium metrizoate N-(4-Aminobutyl)-N-ethylisoluminol FLUORESCEIN-5-MALEIMIDE Minocycline Crystal violet lactone M-MALEIMIDOBENZOYL-N-HYDROXYSULFOSUCCINIMIDE ESTER 2-DIMETHYLAMINO-9-FLUORENONE

  • 3-N,N-DIMETHYLBENZALDEHYDE
  • 3-(DIMETHYLAMINO)BENZALDEHYDE
  • Benzaldehyde, m-(dimethylamino)-
  • 3-(Dimethylamino)benzaldehyde 95%
  • Benzaldehyde, 3-(dimethylamino)-
  • 3-(N,N-Dimethylamino)benzaldehyde
  • VinylBenzoate（Assumed）
  • 619-22-7