3-(DIMETHYLAMINO)BENZALDEHYDE
- Product Name
- 3-(DIMETHYLAMINO)BENZALDEHYDE
- CAS No.
- 619-22-7
- Chemical Name
- 3-(DIMETHYLAMINO)BENZALDEHYDE
- Synonyms
- VinylBenzoate（Assumed）;3-N,N-DIMETHYLBENZALDEHYDE;3-(DIMETHYLAMINO)BENZALDEHYDE;Benzaldehyde, 3-(dimethylamino)-;Benzaldehyde, m-(dimethylamino)-;3-(N,N-Dimethylamino)benzaldehyde;3-(Dimethylamino)benzaldehyde 95%
- CBNumber
- CB7831522
- Molecular Formula
- C9H11NO
- Formula Weight
- 149.19
- MOL File
- 619-22-7.mol
3-(DIMETHYLAMINO)BENZALDEHYDE Property
- Boiling point:
- 137.5-138 °C
- Density
- 1.072±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- pka
- 3.67±0.10(Predicted)
- form
- liquid
- color
- Yellow
Safety
- HS Code
- 2922390090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
N-Bromosuccinimide Price
- Product number
- 8139
- Product name
- 3-N,N-Dimethylbenzaldehyde
- Purity
- 97%
- Packaging
- 1g
- Price
- $318
- Updated
- 2021/12/16
- Product number
- 087143
- Product name
- 3-N,N-Dimethylbenzaldehyde
- Purity
- 97%
- Packaging
- 1g
- Price
- $319
- Updated
- 2021/12/16
- Product number
- W7397
- Product name
- 3-N,N-Dimethylbenzaldehyde
- Packaging
- 1g
- Price
- $371
- Updated
- 2021/12/16
- Product number
- OR400567
- Product name
- 3-(Dimethylamino)benzaldehyde
- Purity
- 95%
- Packaging
- 1g
- Price
- $430
- Updated
- 2021/12/16
- Product number
- 4656-1-2P
- Product name
- 3-(Dimethylamino)benzaldehyde
- Purity
- 95%
- Packaging
- 1g
- Price
- $474
- Updated
- 2021/12/16
3-(DIMETHYLAMINO)BENZALDEHYDE Chemical Properties,Usage,Production
Uses
3-(Dimethylamino)benzaldehyde can be used as a staining agent for identifying non-specific esterase activity in cells. This application is crucial in medical and biological research, as it aids in the detection and analysis of cellular processes and functions.
Synthesis
23501-93-1
619-22-7
General procedure for the synthesis of m-dimethylaminobenzaldehyde from 3-(dimethylamino)benzyl alcohol: commercially available 3-(dimethylamino)benzyl alcohol (750 mg, 5 mmol) was dissolved in a solvent mixture of dichloromethane (DCM) and dimethyl sulfoxide (DMSO). To this solution, triethylamine (Et3N, 2.8 mL, 20 mmol) and sulfur trioxide-pyridine complex (SO3-Py, 1.59 g, 10 mmol) were added sequentially. The reaction mixture was stirred for 2 h at room temperature. After completion of the reaction, dichloromethane was removed by distillation under reduced pressure. Saturated aqueous ammonium chloride (NH4Cl) was added to the residue, which was then extracted with ethyl acetate (EtOAc). The organic phase was washed with water, dried over anhydrous magnesium sulfate (MgSO4) and concentrated under reduced pressure. The crude product was purified by column chromatography (eluent ratio: ethyl acetate/hexane = 1/2) to afford m-dimethylaminobenzaldehyde (670 mg, 90% yield). Mass spectrometry analysis showed [M+H]+ = 150.
References
[1] Journal of Medicinal Chemistry, 2018, vol. 61, # 17, p. 7640 - 7656
[2] Bulletin of the Korean Chemical Society, 2015, vol. 36, # 1, p. 413 - 416
[3] Patent: WO2009/38411, 2009, A2. Location in patent: Page/Page column 36-37
[4] Organic Letters, 2016, vol. 18, # 20, p. 5396 - 5399
[5] Tetrahedron, 2004, vol. 60, # 49, p. 11099 - 11107
3-(DIMETHYLAMINO)BENZALDEHYDE Preparation Products And Raw materials
Raw materials
Preparation Products
3-(DIMETHYLAMINO)BENZALDEHYDE Suppliers
- Tel
- --
- Fax
- --
- sales@ajchem.in
- Country
- India
- ProdList
- 6100
- Advantage
- 58
View Lastest Price from 3-(DIMETHYLAMINO)BENZALDEHYDE manufacturers
- Product
- 3-(DIMETHYLAMINO)BENZALDEHYDE 619-22-7
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 1000KG
- Release date
- 2019-12-18