2-ACETAMIDO-6-CHLOROPURINE
- Product Name
- 2-ACETAMIDO-6-CHLOROPURINE
- CAS No.
- 7602-01-9
- Chemical Name
- 2-ACETAMIDO-6-CHLOROPURINE
- Synonyms
- 2-ACETAMIDO-6-CHLOROPURINE;2-(Acetylamino)-6-chloropurine;N-(6-Chloro-7H-purin-2-yl)acetamide;N-(6-Chloro-9H-purin-2-yl)acetamide;N-(6-chloro-5H-purin-2-yl)acetamide;Acetamide, N-(6-chloro-9H-purin-2-yl)-
- CBNumber
- CB7843640
- Molecular Formula
- C7H6ClN5O
- Formula Weight
- 211.61
- MOL File
- 7602-01-9.mol
2-ACETAMIDO-6-CHLOROPURINE Property
- Melting point:
- >300 °C
- Density
- 1.80
- pka
- 9.22±0.40(Predicted)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- FA06027
- Product name
- 2-Acetamido-6-chloropurine
- Packaging
- 2g
- Price
- $50
- Updated
- 2021/12/16
- Product number
- FA06027
- Product name
- 2-Acetamido-6-chloropurine
- Packaging
- 5G
- Price
- $100
- Updated
- 2021/12/16
- Product number
- 097089
- Product name
- N-(6-Chloro-7H-purin-2-yl)acetamide
- Purity
- 95+%
- Packaging
- 1g
- Price
- $114
- Updated
- 2021/12/16
- Product number
- FA06027
- Product name
- 2-Acetamido-6-chloropurine
- Packaging
- 10g
- Price
- $150
- Updated
- 2021/12/16
- Product number
- 1823AC
- Product name
- N-(6-Chloro-7H-purin-2-yl)acetamide
- Packaging
- 5g
- Price
- $185
- Updated
- 2021/12/16
2-ACETAMIDO-6-CHLOROPURINE Chemical Properties,Usage,Production
Synthesis
108-24-7
10310-21-1
7602-01-9
Step 1: 2-Amino-6-chloropurine (2 g) was added to acetic anhydride (25 mL) preheated to 180 °C and the reaction was heated to reflux overnight. Upon completion of the reaction, the mixture was cooled to room temperature. The precipitate was precipitated by the addition of ether and the solid product was collected by filtration and dried. The crude product was purified by reversed-phase fast column chromatography (elution gradient: 0-60% aqueous methanol) to afford N-(6-chloro-9H-purin-2-yl)acetamide (450 mg, 17% yield) as a white solid. m/z 212 ([M+H]+) was obtained by LC-MS analysis.
References
[1] Tetrahedron Letters, 1997, vol. 38, # 8, p. 1451 - 1454
[2] Tetrahedron, 1997, vol. 53, # 34, p. 11595 - 11626
[3] Patent: WO2015/123365, 2015, A1. Location in patent: Page/Page column 140
[4] Tetrahedron, 1992, vol. 48, # 21, p. 4259 - 4270
2-ACETAMIDO-6-CHLOROPURINE Preparation Products And Raw materials
Raw materials
Preparation Products
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