ChemicalBook > CAS DataBase List > 4-BROMO-2,6-DIMETHOXY-PYRIMIDINE

4-BROMO-2,6-DIMETHOXY-PYRIMIDINE

Product Name
4-BROMO-2,6-DIMETHOXY-PYRIMIDINE
CAS No.
60186-89-2
Chemical Name
4-BROMO-2,6-DIMETHOXY-PYRIMIDINE
Synonyms
6-Bromo-2,4-dimethoxypyrimidine;4-BROMO-2,6-DIMETHOXY-PYRIMIDINE;Pyrimidine, 4-bromo-2,6-dimethoxy-;4-BROMO-2,6-DIMETHOXY-PYRIMIDINE ISO 9001：2015 REACH
CBNumber
CB7845376
Molecular Formula
C6H7BrN2O2
Formula Weight
219.04
MOL File
60186-89-2.mol
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4-BROMO-2,6-DIMETHOXY-PYRIMIDINE Property

Boiling point:
294.7±43.0 °C(Predicted)
Density 
1.563±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
pka
-1.75±0.30(Predicted)
Appearance
White to light yellow Solid
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Biosynth Carbosynth
Product number
FB72020
Product name
4-Bromo-2,6-dimethoxypyrimidine
Packaging
100mg
Price
$150
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB72020
Product name
4-Bromo-2,6-dimethoxypyrimidine
Packaging
250mg
Price
$275
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB72020
Product name
4-Bromo-2,6-dimethoxypyrimidine
Packaging
500mg
Price
$340
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB72020
Product name
4-Bromo-2,6-dimethoxypyrimidine
Packaging
1g
Price
$450
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB72020
Product name
4-Bromo-2,6-dimethoxypyrimidine
Packaging
2g
Price
$620
Updated
2021/12/16
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4-BROMO-2,6-DIMETHOXY-PYRIMIDINE Chemical Properties,Usage,Production

Synthesis

67-56-1

36847-11-7

60186-89-2

To a 2L three-necked round-bottomed flask was added 2,4,6-tribromopyrimidine (54 g, 170.47 mmol, 1 eq.), methanol (500 mL), ethyl ether (500 mL), and a methanolic solution of sodium methanolate (30%, 76.7 g, 2.50 eq.), dropwise. The reaction mixture was stirred at room temperature for 2 hours. After completion of the reaction, the mixture was concentrated in vacuum. The concentrate was diluted with 1 L of ethyl acetate and the organic layer was subsequently washed with 3 x 500 mL of saturated sodium chloride solution. The organic layer was again concentrated in vacuum. The residue was purified by silica gel column chromatography with ethyl acetate/petroleum ether (1:100 to 1:10) as eluent. The fractions containing the target product were combined and concentrated in vacuo to afford 23 g (62% yield) of 4-bromo-2,6-dimethoxypyrimidine as a white solid. The product was confirmed by LC-MS analysis: (ES, m/z): RT = 1.287 min, LCMS 28: m/z = 219 [M + 1].

References

[1] Patent: WO2017/181177, 2017, A1. Location in patent: Paragraph 01122; 01125-01127

4-BROMO-2,6-DIMETHOXY-PYRIMIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 4-BROMO-2,6-DIMETHOXY-PYRIMIDINE manufacturers

Dideu Industries Group Limited
Product
4-BROMO-2,6-DIMETHOXY-PYRIMIDINE 60186-89-2
Price
US $1.10/g
Min. Order
1g
Purity
99.00%
Supply Ability
100 Tons Min
Release date
2021-12-01
Career Henan Chemical Co
Product
4-BROMO-2,6-DIMETHOXY-PYRIMIDINE 60186-89-2
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
Customized
Release date
2020-03-05

60186-89-2, 4-BROMO-2,6-DIMETHOXY-PYRIMIDINERelated Search:

5-Bromo-4,6-dichloropyrimidine 5-Bromo-2,4-dichloropyrimidine Pyrimidine, 4-bromo- (8CI,9CI) 4-BROMO-2-HYDROXYPYRIMIDINE 4-BROMO-2,6-DIMETHOXY-PYRIMIDINE

  • 4-BROMO-2,6-DIMETHOXY-PYRIMIDINE
  • 6-Bromo-2,4-dimethoxypyrimidine
  • Pyrimidine, 4-bromo-2,6-dimethoxy-
  • 4-BROMO-2,6-DIMETHOXY-PYRIMIDINE ISO 9001：2015 REACH
  • 60186-89-2