ChemicalBook > CAS DataBase List > O-ALLYL-2,2,2-TRICHLOROACETIMIDATE

O-ALLYL-2,2,2-TRICHLOROACETIMIDATE

Product Name: O-ALLYL-2,2,2-TRICHLOROACETIMIDATE
CAS No.: 51479-73-3
Chemical Name: O-ALLYL-2,2,2-TRICHLOROACETIMIDATE
Synonyms: ALLYL 2,2,2-TRICHLOROACETIMIDATE;Allyl Trichloroacetimidate;O-ALLYL-2,2,2-TRICHLOROACETIMIDATE;2,2,2-trichloroacetamide allyl ester;Allyl 2,2,2-Trichloroacetimidate >O-Allyl 2,2,2-trichloroacetimidate 96%;2,2,2-TRICHLORACETIMIDIC ACID ALLYLESTER;O-Allyl 2,2,2-trichloroacetimidate;2,2,2-TRICHLOROACETIMIDIC ACID ALLYL ESTER;Ethanimidic acid, 2,2,2-trichloro-, 2-propen-1-yl ester
CBNumber: CB8100737
Molecular Formula: C5H6Cl3NO
Formula Weight: 202.47
MOL File: 51479-73-3.mol

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O-ALLYL-2,2,2-TRICHLOROACETIMIDATE Property

Boiling point:: 54-70 °C/7.5-11.25 mmHg
Density: 1.333 g/mL at 25 °C
refractive index: n20/D 1.489
Flash point:: 74 °C
storage temp.: 2-8°C
solubility: sol hexane, ether, dichloromethane.
pka: 2?+-.0.70(Predicted)
form: clear liquid
color: Colorless to Almost colorless
BRN: 1907084

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Safety

Hazard Codes: Xn
Risk Statements: 22-37/38-41
Safety Statements: 26-39
WGK Germany: 3
HS Code: 29252900

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H227Combustible liquid

H302Harmful if swallowed

H315Causes skin irritation

H318Causes serious eye damage

H335May cause respiratory irritation

Precautionary statements

P210Keep away from heat/sparks/open flames/hot surfaces. — No smoking.

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P403+P235Store in a well-ventilated place. Keep cool.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TCI Chemical

Product number: A2186
Product name: Allyl 2,2,2-Trichloroacetimidate
Purity: >98.0%(GC)
Packaging: 5g
Price: $167
Updated: 2025/07/31

TRC

Product number: T896098
Product name: 2,2,2-TrichloroacetimidicAcidAllylEster
Packaging: 50mg
Price: $45
Updated: 2021/12/16

AK Scientific

Product number: 5073AL
Product name: 2,2,2-Trichloroacetimidicacidallylester
Packaging: 25g
Price: $392
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0066568
Product name: O-ALLYL 2,2,2-TRICHLOROACETIMIDATE
Purity: 95.00%
Packaging: 5G
Price: $212.1
Updated: 2021/12/16

Crysdot

Product number: CD00003706
Product name: Allyl 2,2,2-Trichloroacetimidate
Purity: 97%
Packaging: 25g
Price: $252
Updated: 2021/12/16

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O-ALLYL-2,2,2-TRICHLOROACETIMIDATE Chemical Properties,Usage,Production

Uses

Reagent used for the protection of an alcohol as its allyl ether in the presence of base sensitive functionality.

Application

O-allyl-2,2,2-trichloroacetimidate can be used to release allyl groups under mild conditions; used to prepare nitrogen-containing intermediates.

Preparation

Sodium Hydride (0.5 g, 21 mmol) is slurried in anhydrous ether (20 mL) under a nitrogen blanket. Allyl alcohol (210 mmol) is introduced in ether (30 mL) dropwise with stirring to the slurry. After 20 min, the homogeneous solution is cooled to 0 °C and Trichloroacetonitrile (20 mL, 200 mmol) is added over 15 min. The mixture is allowed to warm to 20 °C over 60 min and then concentrated to a syrup. Pentane (20 mL) containing methanol (0.8 mL, 21 mmol) is added followed by vigorous shaking, filtration, and concentration of the filtrate and pentane washings (2 × 20 mL). The product imidate is obtained as a clear liquid (90-97%). No further purification is required. Alternatively, the imidate can be prepared by using sodium methoxide as a catalyst instead of sodium hydride. Other procedures for the preparation of allyl trichloroacetimidate have been reported.

O-ALLYL-2,2,2-TRICHLOROACETIMIDATE Preparation Products And Raw materials

Raw materials

Preparation Products

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O-ALLYL-2,2,2-TRICHLOROACETIMIDATE Suppliers

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View Lastest Price from O-ALLYL-2,2,2-TRICHLOROACETIMIDATE manufacturers

Career Henan Chemical Co

Product: O-ALLYL-2,2,2-TRICHLOROACETIMIDATE 51479-73-3
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 200kg
Release date: 2019-09-03

51479-73-3, O-ALLYL-2,2,2-TRICHLOROACETIMIDATERelated Search:

Di-tert-butyl dicarbonate ETHYL 2,2,2-TRICHLOROACETIMIDATE 3-(2-CHLORO-ETHOXY)-PROPENE METHYL 2,2,2-TRICHLOROACETIMIDATE O-ALLYL-2,2,2-TRICHLOROACETIMIDATE

2,2,2-TRICHLORACETIMIDIC ACID ALLYLESTER

2,2,2-TRICHLOROACETIMIDIC ACID ALLYL ESTER

O-Allyl 2,2,2-trichloroacetimidate 96%

Allyl Trichloroacetimidate

O-ALLYL-2,2,2-TRICHLOROACETIMIDATE

ALLYL 2,2,2-TRICHLOROACETIMIDATE

Allyl 2,2,2-Trichloroacetimidate &gt

Ethanimidic acid, 2,2,2-trichloro-, 2-propen-1-yl ester

<i>O-</i>Allyl 2,2,2-trichloroacetimidate

2,2,2-trichloroacetamide allyl ester

51479-73-3

C5H6Cl3NO

Organic Building Blocks

Nitrogen Compounds

Building Blocks

Amidates/Imidates