3-METHOXY-5-METHYL-BENZOIC ACID METHYL ESTER
- Product Name
- 3-METHOXY-5-METHYL-BENZOIC ACID METHYL ESTER
- CAS No.
- 108593-44-8
- Chemical Name
- 3-METHOXY-5-METHYL-BENZOIC ACID METHYL ESTER
- Synonyms
- Methyl 3-Methoxy-5-Methylbenzoate;Methyl 5-methoxy-3-methylbenzoate;Methyl 3-methyl-5-(methyloxy)benzoate;3-METHOXY-5-METHYL-BENZOIC ACID METHYL ESTER;Benzoic acid, 3-Methoxy-5-Methyl-, Methyl ester
- CBNumber
- CB81010387
- Molecular Formula
- C10H12O3
- Formula Weight
- 180.2
- MOL File
- 108593-44-8.mol
3-METHOXY-5-METHYL-BENZOIC ACID METHYL ESTER Property
- Boiling point:
- 270.8±20.0 °C(Predicted)
- Density
- 1.075±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- Appearance
- Colorless to light yellow Liquid
Safety
- HS Code
- 2918999090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- M354428
- Product name
- Methyl3-Methoxy-5-methylbenzoate
- Packaging
- 10mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- OR907669
- Product name
- Methyl 5-methoxy-3-methylbenzoate
- Packaging
- 250mg
- Price
- $203
- Updated
- 2021/12/16
- Product number
- X8886
- Product name
- Methyl3-methoxy-5-methylbenzoate
- Packaging
- 250mg
- Price
- $203
- Updated
- 2021/12/16
- Product number
- X8886
- Product name
- Methyl3-methoxy-5-methylbenzoate
- Packaging
- 1g
- Price
- $431
- Updated
- 2021/12/16
- Product number
- CHM0092411
- Product name
- 3-METHOXY-5-METHYL-BENZOIC ACID METHYL ESTER
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $495.88
- Updated
- 2021/12/16
3-METHOXY-5-METHYL-BENZOIC ACID METHYL ESTER Chemical Properties,Usage,Production
Synthesis
2615-71-6
74-88-4
108593-44-8
General procedure for the synthesis of methyl 3-methoxy-5-methylbenzoate from methyl 3-hydroxy-5-methylbenzoate and iodomethane: To a solution of methyl 3-hydroxy-5-methylbenzoate (20.0 g, 120 mmol) in N,N-dimethylformamide (120 mL) was added sequentially iodomethane (11.2 mL, 180 mmol), cesium carbonate (4.65 g, 180 mmol) and catalytic amount of 4-dimethylaminopyridine. 180 mmol) and a catalytic amount of 4-dimethylaminopyridine. The reaction mixture was stirred at room temperature overnight. Upon completion of the reaction, it was diluted with water (200 mL) and extracted with ethyl acetate (3 x 150 mL). The organic phases were combined, washed with saturated aqueous sodium chloride solution, dried over anhydrous magnesium sulfate, filtered and concentrated to afford the target product methyl 3-methoxy-5-methylbenzoate (19.9 g, 92% yield). The product was characterized by 1H NMR (400 MHz, CDCl3): δ 2.38 (s, 3H), 3.84 (s, 3H), 3.91 (s, 3H), 6.93 (s, 1H), 7.37 (s, 1H), 7.48 (s, 1H).
References
[1] Patent: WO2007/105058, 2007, A2. Location in patent: Page/Page column 49
[2] Patent: WO2009/32667, 2009, A1. Location in patent: Page/Page column 137
3-METHOXY-5-METHYL-BENZOIC ACID METHYL ESTER Preparation Products And Raw materials
Raw materials
Preparation Products
3-METHOXY-5-METHYL-BENZOIC ACID METHYL ESTER Suppliers
- Tel
- --
- Fax
- --
- sales@ajchem.in
- Country
- India
- ProdList
- 6100
- Advantage
- 58
View Lastest Price from 3-METHOXY-5-METHYL-BENZOIC ACID METHYL ESTER manufacturers
- Product
- 3-METHOXY-5-METHYL-BENZOIC ACID METHYL ESTER 108593-44-8
- Price
- US $1.00/g
- Min. Order
- 1g
- Purity
- 98%
- Supply Ability
- 100KG
- Release date
- 2020-01-12