Serine, N-[(1,1-dimethylethoxy)carbonyl]- (9CI)

Product Name: Serine, N-[(1,1-dimethylethoxy)carbonyl]- (9CI)
CAS No.: 3850-40-6
Chemical Name: Serine, N-[(1,1-dimethylethoxy)carbonyl]- (9CI)
Synonyms: N-BOC-Serine;Boc-DL-serine;(tert-Butoxycarbonyl)serine;(Tert-Butoxy)Carbonyl DL-Ser-OH;N-[(1,1-Dimethylethoxy)carbonyl]serine;Serine,N-[(1,1-diMethylethoxy)carbonyl]-;Serine, N-[(1,1-dimethylethoxy)carbonyl]- (9CI);3-hydroxy-2-[(2-methylpropan-2-yl)oxycarbonylamino]propanoic acid
CBNumber: CB81072758
Molecular Formula: C8H15NO5
Formula Weight: 205.21
MOL File: 3850-40-6.mol

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Serine, N-[(1,1-dimethylethoxy)carbonyl]- (9CI) Property

Boiling point:: 385.1±37.0 °C(Predicted)
Density: 1.240±0.06 g/cm3(Predicted)
storage temp.: 2-8°C
pka: 3.62±0.10(Predicted)
Appearance: White to off-white Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

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N-Bromosuccinimide Price

TRC

Product number: B810043
Product name: 2-((tert-Butoxycarbonyl)amino)-3-hydroxypropanoicAcid
Packaging: 2.5g
Price: $75
Updated: 2021/12/16

Activate Scientific

Product number: AS47679
Product name: Boc-DL-serine
Purity: 95+%
Packaging: 1g
Price: $40
Updated: 2021/12/16

Activate Scientific

Product number: AS47679
Product name: Boc-DL-serine
Purity: 95+%
Packaging: 5G
Price: $132
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0092775
Product name: 2-TERT-BUTOXYCARBONYLAMINO-3-HYDROXY-PROPIONIC ACID
Purity: 95.00%
Packaging: 10MG
Price: $618.5
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0092775
Product name: 2-TERT-BUTOXYCARBONYLAMINO-3-HYDROXY-PROPIONIC ACID
Purity: 95.00%
Packaging: 5MG
Price: $623.82
Updated: 2021/12/16

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Serine, N-[(1,1-dimethylethoxy)carbonyl]- (9CI) Chemical Properties,Usage,Production

Synthesis

312-84-5

24424-99-5

3262-72-4

Sodium hydroxide (8.4 g, 0.110 mol) was dissolved in water (53 mL) and stirred at room temperature until completely dissolved, followed by cooling to 5-10 °C. D-serine (10.5 g, 0.100 mol) and di-tert-butyl dicarbonate (26.2 g, 0.120 mol) were slowly added while the temperature was maintained at ≤10 °C. The reaction mixture was gradually heated to 30-35 °C and the reaction was stirred at this temperature for 20 hours. Upon completion of the reaction, an aqueous solution of BOC-L-serine was obtained (yield based on 100%, HPLC purity 99.1%, chiral purity 99.4%). This aqueous solution can be used directly in the subsequent synthesis steps without further purification.

References

[1] Journal of the American Chemical Society, 1994, vol. 116, # 18, p. 8402 - 8403
[2] Journal of the American Chemical Society, 2008, vol. 130, # 7, p. 2351 - 2364
[3] Advanced Synthesis and Catalysis, 2016, vol. 358, # 1, p. 34 - 40
[4] Patent: CN104030943, 2016, B. Location in patent: Paragraph 0095; 0096
[5] Beilstein Journal of Organic Chemistry, 2014, vol. 10, p. 1114 - 1120

Serine, N-[(1,1-dimethylethoxy)carbonyl]- (9CI) Preparation Products And Raw materials

Raw materials

Preparation Products

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Serine, N-[(1,1-dimethylethoxy)carbonyl]- (9CI) Suppliers

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View Lastest Price from Serine, N-[(1,1-dimethylethoxy)carbonyl]- (9CI) manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: Serine, N-[(1,1-dimethylethoxy)carbonyl]- (9CI) 3850-40-6
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 20T
Release date: 2024-08-13

3850-40-6, Serine, N-[(1,1-dimethylethoxy)carbonyl]- (9CI)Related Search:

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