(R)-3-Benzyloxy-Pyrrolidine Hydrochloride
- Product Name
- (R)-3-Benzyloxy-Pyrrolidine Hydrochloride
- CAS No.
- 927819-90-7
- Chemical Name
- (R)-3-Benzyloxy-Pyrrolidine Hydrochloride
- Synonyms
- (3R)-3-benzyloxypyrrolidine;(R)-3-Benzyloxy Pyrrolidine Hcl;3-phenylmethoxypyrrolidine hydrochloride;(R)-3-BENZYLOXY-PYRROLIDINE HYDROCHLORIDE;(3R)-3-(benzyloxy)pyrrolidine hydrochloride
- CBNumber
- CB81118928
- Molecular Formula
- C11H16ClNO
- Formula Weight
- 213.71
- MOL File
- 927819-90-7.mol
(R)-3-Benzyloxy-Pyrrolidine Hydrochloride Property
- storage temp.
- Sealed in dry,Room Temperature
Safety
- HS Code
- 2933998090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B130245
- Product name
- (R)-3-BENZYLOXY-PYRROLIDINEHYDROCHLORIDE
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- AS35806
- Product name
- (R)-3-Benzyloxypyrrolidine hydrochloride
- Purity
- 95+% ee
- Packaging
- 5G
- Price
- $655
- Updated
- 2021/12/16
- Product number
- W9561
- Product name
- (R)-3-Benzyloxypyrrolidinehydrochloride
- Packaging
- 5g
- Price
- $728
- Updated
- 2021/12/16
- Product number
- AS35806
- Product name
- (R)-3-Benzyloxypyrrolidine hydrochloride
- Purity
- 95+% ee
- Packaging
- 1g
- Price
- $229
- Updated
- 2021/12/16
- Product number
- CCH0004337
- Product name
- (R)-3-BENZYLOXY-PYRROLIDINE HYDROCHLORIDE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $263.55
- Updated
- 2021/12/16
(R)-3-Benzyloxy-Pyrrolidine Hydrochloride Chemical Properties,Usage,Production
Uses
(R)-3-Benzyloxy-Pyrrolidine Hydrochloride is an important organic reagent that can be used as a building block for the synthesis of many organic compounds, such as (R)-ethyl 4-(3-(benzyloxy)pyrrolidin-1-yl)butanoate.
Synthesis
After N-tert-butoxycarbonyl-(R)-3-benzyloxypyrrolidine separately obtained was dissolved in isopropanol and heated to 40 °C, isopropanol solution of hydrogen chloride was dropped for 6 hours. After the reaction finished, the mixture was cooled to 23 °C and was concentrated to distil the solvent away. Further, ethyl acetate was added and the mixture was concentrated, thereby obtaining a concentrate in an amount of about. Then, the concentrate was heated to 40 °C, and isopropanol was added until (R)-3-benzyloxypyrrolidine hydrochloride which had been separated as an oily substance became completely dissolved. After (R) -3-benzyloxypyrrolidine hydrochloride was crystallized by gradually cooling the solution and suitably adding a seed crystal, hexane was further added. At the time, crystallization solvent was in a following proportion: isopropanol/ethyl acetate/hexane = 1/71.5/71.5. A deposited crystal was subjected to filtration under reduced pressure, and the resultant wet crystal was washed with ethyl acetate, and then a wet crystal was dried under reduced pressure, thereby obtaining dry crystal of (R)-3-benzyloxypyrrolidine hydrochloride (yield of 82 %, purity of 99.8 %).
(R)-3-Benzyloxy-Pyrrolidine Hydrochloride Preparation Products And Raw materials
Raw materials
Preparation Products
(R)-3-Benzyloxy-Pyrrolidine Hydrochloride Suppliers
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