ChemicalBook > CAS DataBase List > 1-(4-BROMOPHENYL)PYRROLIDINE

1-(4-BROMOPHENYL)PYRROLIDINE

Product Name
1-(4-BROMOPHENYL)PYRROLIDINE
CAS No.
22090-26-2
Chemical Name
1-(4-BROMOPHENYL)PYRROLIDINE
Synonyms
N-(4-BROMOPHENYL)PYRROLIDINE;1-(4-BROMOPHENYL)PYRROLIDINE;1-Bromo-4-pyrrolidinobenzene;Pyrrolidine, 1-(4-broMophenyl)-;1-(4-Bromophenyl)pyrrolidine >1-(4-Bromophenyl)pyrrolidine 97+%
CBNumber
CB8113953
Molecular Formula
C10H12BrN
Formula Weight
226.11
MOL File
22090-26-2.mol
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1-(4-BROMOPHENYL)PYRROLIDINE Property

Melting point:
105.0 to 109.0 °C
Boiling point:
306.1±25.0 °C(Predicted)
Density 
1.411±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
form 
powder to crystal
pka
4.81±0.40(Predicted)
color 
White to Almost white
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Safety

HS Code 
2933998090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TCI Chemical
Product number
B3900
Product name
1-(4-Bromophenyl)pyrrolidine
Purity
>98.0%(GC)(T)
Packaging
1g
Price
$38
Updated
2025/07/31
TCI Chemical
Product number
B3900
Product name
1-(4-Bromophenyl)pyrrolidine
Purity
>98.0%(GC)(T)
Packaging
5g
Price
$126
Updated
2025/07/31
TRC
Product number
B700898
Product name
1-(4-Bromophenyl)pyrrolidine
Packaging
100mg
Price
$75
Updated
2021/12/16
SynQuest Laboratories
Product number
3H32-9-BU
Product name
1-(4-Bromophenyl)pyrrolidine
Packaging
1g
Price
$37
Updated
2021/12/16
AK Scientific
Product number
N539
Product name
N-(4-Bromophenyl)pyrrolidine
Packaging
1g
Price
$85
Updated
2021/12/16
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1-(4-BROMOPHENYL)PYRROLIDINE Chemical Properties,Usage,Production

Synthesis

110-52-1

106-40-1

22090-26-2

Step 82a: Synthesis of 1-(4-bromophenyl)pyrrolidine (compound 0601-155) A mixture of 4-bromoaniline (1 g, 5.81 mmol), Cs2CO3 (5.68 g, 17.44 mmol), and 1,4-dibromobutane (1.88 g, 8.72 mmol) was dissolved in DMF (20 mL), and the reaction was stirred at 60 °C overnight. After completion of the reaction, the mixture was cooled to room temperature, diluted with water (200 mL) and extracted with ethyl acetate (2 x 100 mL). The organic layers were combined, washed sequentially with water (3 x 100 mL) and brine (100 mL) and dried over anhydrous Na2SO4. After concentration under reduced pressure, purified by silica gel column chromatography (eluent: petroleum ether), the target compound 0601-155 (720 mg, 46% yield) was obtained as a colorless oil.LCMS: 226 [M + 1]+.1H NMR (400MHz, DMSO-d6) δ1.94 (t, J=6.4Hz, 4H), 3.18 (t, J=6.4Hz, 4H), 6.18 (t, J=6.4Hz, 4H). Hz, 4H), 6.47 (d, J=9.2Hz, 2H), 7.27 (d, J=9.2Hz, 2H).

References

[1] Journal of the American Chemical Society, 2014, vol. 136, # 33, p. 11602 - 11605
[2] Journal of Organic Chemistry, 2006, vol. 71, # 1, p. 135 - 141
[3] Patent: WO2011/130628, 2011, A1. Location in patent: Page/Page column 221
[4] Patent: US2013/102595, 2013, A1. Location in patent: Paragraph 0550
[5] Patent: JP2015/187145, 2015, A. Location in patent: Paragraph 0468

1-(4-BROMOPHENYL)PYRROLIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

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1-(4-BROMOPHENYL)PYRROLIDINE Suppliers

Americas 1 Belgium 1 China 79 Europe 1 Germany 2 India 2 Japan 1 United Kingdom 2 United States 13 Global 102
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View Lastest Price from 1-(4-BROMOPHENYL)PYRROLIDINE manufacturers

Career Henan Chemical Co
Product
1-(4-BROMOPHENYL)PYRROLIDINE 22090-26-2
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
200kg
Release date
2019-12-30

22090-26-2, 1-(4-BROMOPHENYL)PYRROLIDINERelated Search:

1-(4-BROMOPHENYL)-2-PYRROLIDINONE (S)-2-(2-BROMOPHENYL)PYRROLIDINE (3S,4R)-4-(2-BROMOPHENYL)PYRROLIDINE-3-CARBOXYLIC ACID (S)-2-(4-BROMOPHENYL)PYRROLIDINE 2-(2-Bromophenyl)pyrrolidine (R)-2-(2-BROMOPHENYL)PYRROLIDINE (3S,4R)-4-(3-BROMOPHENYL)PYRROLIDINE-3-CARBOXYLIC ACID (R)-2-(3-BROMOPHENYL)PYRROLIDINE (3S,4R)-4-(4-BROMOPHENYL)PYRROLIDINE-3-CARBOXYLIC ACID (R)-2-(4-BROMOPHENYL)PYRROLIDINE N-(3-BROMOPHENYL)PYRROLIDINE,1-(3-Bromophenyl)pyrrolidine 97%,1-(3-BROMOPHENYL)PYRROLIDINE 1-(4-BROMOPHENYL)-5-OXOPYRROLIDINE-3-CARBOXYLIC ACID 1-(4-BROMOPHENYL)PYRROLIDINE-2,5-DIONE BOC-(+/-)-TRANS-4-(3-BROMOPHENYL)-PYRROLIDINE-3-CARBOXYLIC ACID (+/-)-TRANS-4-(3-BROMOPHENYL)PYRROLIDINE-3-CARBOXYLIC ACID HYDROCHLORIDE 3-(2-BROMOPHENYL)PYRROLIDINE BOC-(+/-)-TRANS-4-(2-BROMOPHENYL)-PYRROLIDINE-3-CARBOXYLIC ACID 3-(3-BROMOPHENYL)PYRROLIDINE

  • 1-(4-BROMOPHENYL)PYRROLIDINE
  • N-(4-BROMOPHENYL)PYRROLIDINE
  • Pyrrolidine, 1-(4-broMophenyl)-
  • 1-Bromo-4-pyrrolidinobenzene
  • 1-(4-Bromophenyl)pyrrolidine 97+%
  • 1-(4-Bromophenyl)pyrrolidine &gt
  • 22090-26-2
  • Miscellaneous