4-(6-Acryloyloxyhexyloxy)-benzoesure (4-cyanophenylester)
- Product Name
- 4-(6-Acryloyloxyhexyloxy)-benzoesure (4-cyanophenylester)
- CAS No.
- 83847-14-7
- Chemical Name
- 4-(6-Acryloyloxyhexyloxy)-benzoesure (4-cyanophenylester)
- Synonyms
- RM23;VE6OPEPN;4-Cyanophenol 4-(6-acryloyloxyhexyloxy)benzoate;4-Cyanophenyl 4'-(6-acryloyloxyhexyloxy)benzoate;6-[4-(4-Cyanophenoxycarbonyl)phenoxy]hexyl acrylate;(4-cyanophenyl) 4-(6-prop-2-enoyloxyhexoxy)benzoate;4[4[6-Acryloxyhex-1-yl)oxyphenyl]carboxy-benzonitrile;4-(6-Acryloyloxyhexyloxy)-benzoesure (4-cyanophenylester);4-Cyanophenyl 4-[[6-[(1-oxo-2-propen-1-yl)oxy]hexyl]oxy]benzoate;Benzoic acid, 4-[[6-[(1-oxo-2-propenyl)oxy]hexyl]oxy]-, 4-cyanophenylester
- CBNumber
- CB81448429
- Molecular Formula
- C23H23NO5
- Formula Weight
- 393.43
- MOL File
- 83847-14-7.mol
4-(6-Acryloyloxyhexyloxy)-benzoesure (4-cyanophenylester) Property
- Boiling point:
- 563.1±45.0 °C(Predicted)
- Density
- 1.19
- vapor pressure
- 0-0Pa at 25-50℃
- form
- Solid:crystalline
- LogP
- 4.5 at 40℃ and pH7
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- A1442086
- Product name
- 4-Cyanophenyl4-((6-(acryloyloxy)hexyl)oxy)benzoate
- Purity
- 97%
- Packaging
- 5g
- Price
- $41
- Updated
- 2021/12/16
- Product number
- AA00G3VU
- Product name
- 4''-((6-(Acryloyloxy)hexyl)oxy)-4-cyano-[1,1''-biphenyl]-3-carboxylicacid
- Purity
- 97%
- Packaging
- 5g
- Price
- $86
- Updated
- 2021/12/16
- Product number
- A1442086
- Product name
- 4-Cyanophenyl4-((6-(acryloyloxy)hexyl)oxy)benzoate
- Purity
- 97%
- Packaging
- 25g
- Price
- $137
- Updated
- 2021/12/16
- Product number
- AA00G3VU
- Product name
- 4''-((6-(Acryloyloxy)hexyl)oxy)-4-cyano-[1,1''-biphenyl]-3-carboxylicacid
- Purity
- 97%
- Packaging
- 25g
- Price
- $194
- Updated
- 2021/12/16
4-(6-Acryloyloxyhexyloxy)-benzoesure (4-cyanophenylester) Chemical Properties,Usage,Production
Uses
4-(6-Acryloyloxyhexyloxy)-benzoesure (4-cyanophenylester) can be used as an intermediate in organic synthesis, mainly used in laboratory research and development and in the process of chemical and pharmaceutical synthesis.
Synthesis
The target monomer was prepared by firstly converting the
acid into the corresponding acid chloride, then condensing this
withp-cyanophenol. The acid (17.32 g, 0.059 mol) was stirred with thionyl chloride (35.7 g, 0.3 mol) in the presence of DMF
(2 drops) and 2,6-di-tert-butyl-4-methyl phenol (4.4 g, 0.02
mol). After ca. 25 min, by which time solution was achieved,
the excess thionyl chloride was removed by rotary evaporation
and high vacuum (1-2 h). The acid chloride residue was dis-
solved in anhydrous chloroform (30 mL), then added slowly
dropwise into a stirred solution of p-cyanophenol (7.03 g,
0.059 mol) and triethylamine (6.07 g, 0.06 mol) in chloroform
(20 mL) at 0??C. After the addition the mixture was stirred at
room temperature for 24 h and then chloroform (200 mL)
added. This solution was washed with water (50 mL) followed
by 2 N sodium hydroxide solution (3 x 50 mL) and water (2 x
50 mL). The organic layer was dried (MgSO,), evaporated,
then subjected to flash chromatography, using dichloro-
methane as both the solvent and the eluant. The monomer was
finally recrystallized from isopropanol and shown to be pure
by tlc. Yield: 16 g, 69%.
4-(6-Acryloyloxyhexyloxy)-benzoesure (4-cyanophenylester) Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 4-(6-Acryloyloxyhexyloxy)-benzoesure (4-cyanophenylester) manufacturers
- Product
- 4-cyanophenyl 4-((6-(acryloyloxy)hexyl)oxy)benzoate 83847-14-7
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 98.00%
- Supply Ability
- 1000KG/month
- Release date
- 2021-11-02
- Product
- 4-(6-Acryloyloxyhexyloxy)-benzoesure (4-cyanophenylester) 83847-14-7
- Price
- US $0.00-0.00/g
- Min. Order
- 10g
- Purity
- 0.95
- Supply Ability
- 50kg
- Release date
- 2023-08-02