ChemicalBook > CAS DataBase List > 1-chloro-3-methyl-5-nitro-benzene

1-chloro-3-methyl-5-nitro-benzene

Product Name: 1-chloro-3-methyl-5-nitro-benzene
CAS No.: 16582-38-0
Chemical Name: 1-chloro-3-methyl-5-nitro-benzene
Synonyms: NSC 169207;3-Chlor-5-nitrotoluene;5-Chloro-3-nitrotoluene;3-CHLORO-5-NITROTOLUENE;1-chloro-3-methyl-5-nitro-benzene;Benzene, 1-chloro-3-methyl-5-nitro-;1-chloro-3-methyl-5-nitro-benzene ISO 9001：2015 REACH
CBNumber: CB81454181
Molecular Formula: C7H6ClNO2
Formula Weight: 171.58
MOL File: 16582-38-0.mol

Less

1-chloro-3-methyl-5-nitro-benzene Property

Melting point:: 54-55℃
Boiling point:: 253℃
Density: 1.324
refractive index: 1.
Flash point:: 107℃
storage temp.: Sealed in dry,Room Temperature
form: solid
color: Brown

Less

Safety

HS Code: 2904990090

Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

Less

N-Bromosuccinimide Price

TRC

Product number: C596843
Product name: 3-Chloro-5-nitrotoluene
Packaging: 50mg
Price: $45
Updated: 2021/12/16

TRC

Product number: C596843
Product name: 3-Chloro-5-nitrotoluene
Packaging: 100mg
Price: $60
Updated: 2021/12/16

TRC

Product number: C596843
Product name: 3-Chloro-5-nitrotoluene
Packaging: 500mg
Price: $75
Updated: 2021/12/16

AK Scientific

Product number: 8420AA
Product name: 1-Chloro-3-methyl-5-nitrobenzene
Packaging: 5g
Price: $39
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0049385
Product name: 3-CHLORO-5-NITROTOLUENE
Purity: 95.00%
Packaging: 5G
Price: $909.56
Updated: 2021/12/16

Less

1-chloro-3-methyl-5-nitro-benzene Chemical Properties,Usage,Production

Synthesis

69951-02-6

16582-38-0

The general procedure for the synthesis of 3-chloro-5-nitrotoluene from 2-chloro-6-methyl-4-nitroaniline was as follows: 2-chloro-4-nitro-6-methylaniline (55.0 g, 0.295 mol) was mixed with ethanol (500 mL) in a 2 L four-neck flask. Sulfuric acid (120 mL) was added slowly and dropwise to the reaction mixture at below room temperature. The temperature of the reaction mixture was maintained at 5 to 10 °C and an aqueous sodium nitrite solution (26.44 g, 0.381 mol dissolved in 40 mL of water) was added dropwise over 40 min. Subsequently, the reaction mixture was stirred at room temperature. After the reaction was observed to be exothermic raising the temperature to 45 °C, it was cooled naturally to below 40 °C and stirring was continued at 40 to 45 °C until no bubbles were produced. After cooling the reaction mixture to room temperature, it was poured into 2500 mL of ice water and precipitated. The precipitate was collected by filtration and dried under reduced pressure to give 45.95 g of yellow solid product in 90% yield. The product was characterized by 1H-NMR (500 MHz, CDCl3): δ 8.03 (broad peak, 1H), 7.94 (broad peak, 1H), 7.50 (broad peak, 1H), 2.46 (single peak, 3H).

References

[1] Patent: US2004/147776, 2004, A1. Location in patent: Page 2
[2] Chem. News J. Ind. Sci., 1895, vol. 72, p. 58
[3] Chem. Zentralbl., 1895, vol. 66, # II, p. 530
[4] P. Ch. S., # 154,

1-chloro-3-methyl-5-nitro-benzene Preparation Products And Raw materials

Raw materials

Preparation Products

Less

1-chloro-3-methyl-5-nitro-benzene Suppliers

China 74 India 3 United States 6 Global 83

Meryer (Shanghai) Chemical Technology Co., Ltd.

Tel: 4006356688 18621169109
Fax: 86-21-61259102
Email: market03@meryer.com
Country: China
ProdList: 40228
Advantage: 62

Jia Xing Isenchem Co.,Ltd

Tel: 0573-85285100 18627885956
Fax: 0573-85285100
Email: isenchem@163.com
Country: China
ProdList: 9310
Advantage: 66

Adamas Reagent, Ltd.

Tel: 400-6009262 16621234537
Fax: 021-64823266
Email: chenyj@titansci.com
Country: China
ProdList: 14101
Advantage: 59

Shanghai Longsheng chemical Co.,Ltd.

Tel: 021-58099652-8005 13585536065
Fax: 021-58099609
Email: bin.wu@shlschem.com
Country: China
ProdList: 9883
Advantage: 59

Shanghai Hanhong Scientific Co.,Ltd.

Tel: 021-54306202 13764082696
Email: info@hanhongsci.com
Country: China
ProdList: 42934
Advantage: 64

Tianjin heowns Biochemical Technology Co., Ltd.

Tel: 400 638 7771
Email: sales@heowns.com
Country: China
ProdList: 14435
Advantage: 57

Hangzhou Yuhao Chemical Technology Co., Ltd

Tel: 0571-82693216
Fax: +86-571-82880190
Email: info@yuhaochemical.com
Country: China
ProdList: 6387
Advantage: 52

Hangzhou Sage Chemical Co., Ltd.

Tel: +86057186818502 13588463833
Fax: Pls mail us for more information!
Email: info@sagechem.com
Country: China
ProdList: 10266
Advantage: 58

Candia Thamtech Company Limited

Tel: 0371-86615086 18203638366 0371-86159066 13526786601
Fax: 0371-86159066
Country: China
ProdList: 2015
Advantage: 60

SynAsst Chemical.

Tel: 021-60343070
Fax: 021-35122006
Country: China
ProdList: 12740
Advantage: 55

Shanghai Raise Chemical Technology Co.,Ltd

Tel: +86-021-50935922
Fax: +86-021-33847795
Country: China
ProdList: 7865
Advantage: 55

Shanghai Hong-chuang Pharma Tech Co., Ltd.

Tel: 18151128828
Fax: -
Email: hc-sales@foxmail.com
Country: China
ProdList: 2647
Advantage: 55

Bide Pharmatech Ltd.

Tel: 400-164-7117 13681763483
Fax: +86-21-61629029
Email: product02@bidepharm.com
Country: China
ProdList: 39966
Advantage: 60

Quzhou synpartner PharmaTech co.,ltd

Tel: 0570-3856196 13615701454
Fax: 0570-3856347
Email: Bella@synpartner.com
Country: China
ProdList: 67
Advantage: 65

Shanghai Worldyang Chemical Co.,Ltd.

Tel: 021-021-56795766
Fax: +86-21-56795266
Email: sales@worldyachem.com
Country: China
ProdList: 9476
Advantage: 58

Shanghai ACT chemical Limited

Tel: 021-59904146 18001826933
Fax: +86-21-59904146
Email: sales@actchemical.com
Country: China
ProdList: 476
Advantage: 56

Tianjin Anhao Biological Technology Co., Ltd.

Tel
Email: sales@ahpharmatech.com
Country: China
ProdList: 5734
Advantage: 55

Shanghai HuanChuan Industry Co.,Ltd.

Tel: 021-61478794
Fax: 021-61478794
Email: sales@hcshhai.com
Country: China
ProdList: 9793
Advantage: 50

Nanjing Duolong Bio-tech Co.,Ltd.

Tel: 18905173768
Fax: 025-83263139
Email: 52513593@qq.com
Country: China
ProdList: 2331
Advantage: 50

Jiangsu Aikon Biopharmaceutical R&D co.,Ltd.

Tel: 025-66028182 18626450290
Email: yftan@aikonchem.com
Country: China
ProdList: 16679
Advantage: 50

Changzhou Anxuan Chemical, Co., Ltd.

Tel: 13912302692 13912302692;
Fax: 0519-88064678
Email: sales@anxuanchem.com
Country: China
ProdList: 4828
Advantage: 58

Zhengzhou Alfachem Co.,Ltd.

Tel: 0371-53778726 18003825608
Fax: QQ：2885354392
Email: liuxiaoyan@alfachem.cn
Country: China
ProdList: 1986
Advantage: 58

Shanghai YuanYe Biotechnology Co., Ltd.

Tel: 021-61312847; 18021002903
Fax: QQ:3008007432
Email: 3008007409@qq.com
Country: China
ProdList: 71826
Advantage: 60

Chengdu Xiaojia Technology Co., Ltd.

Tel: 15902830537
Email: zhanghao@happysyn.com
Country: China
ProdList: 3180
Advantage: 55

Shanghai SuperLan Chemcial Technique Centre

Tel: 0-2022843681 15618226720
Fax: +86-21-51601218
Email: chaolaichem@foxmail.com
Country: China
ProdList: 12475
Advantage: 58

Amadis Chemical Company Limited

Tel: 571-89925085
Fax: 0086-571-89925065
Email: sales@amadischem.com
Country: China
ProdList: 131957
Advantage: 58

Henan Anky Chemical Technology Co., Ltd.

Tel: 17836913271
Fax: 0374-8348899
Email: 3224305243@qq.com
Country: China
ProdList: 2944
Advantage: 58

Capot Chemical Co.,Ltd.

Tel: +86-（0）57185586718; +8613336195806
Fax: +86-571-85864795
Email: sales@capot.com
Country: China
ProdList: 29735
Advantage: 60

Tianjin heowns Biochemical Technology Co., Ltd.

Tel: 400-6387771-6039 18920764717
Email: sales@heowns.com
Country: China
ProdList: 23771
Advantage: 60

Nanjing crow LuNing pharmaceutical technology co., LTD

Tel: 13382066392
Country: CHINA
ProdList: 4877
Advantage: 58

Xinyi Kaiwu Chemical Technology Co., Ltd.

Tel: 0516-0516-88997009 18651776937
Email: 4164357@qq.com
Country: China
ProdList: 3204
Advantage: 58

Hefei TNJ Chemical Industry Co.,Ltd.

Tel: +86-0551-65418671 +8618949823763
Fax: 0551-65418697
Email: sales@tnjchem.com
Country: China
ProdList: 34563
Advantage: 58

CD Chemical Group Limited

Tel: +8615986615575
Fax: 0086-13651442114
Email: info@codchem.com
Country: China
ProdList: 20342
Advantage: 58

Dayang Chem (Hangzhou) Co.,Ltd.

Tel: +86-0571-88938639 +8617705817739
Fax: +86-571-88938652，+86-571- 88492614
Email: info@dycnchem.com
Country: China
ProdList: 52846
Advantage: 58

Shaanxi Dideu Medichem Co. Ltd

Tel: +86-029-89586680 +86-18192503167
Fax: +86-29-88380327
Email: 1026@dideu.com
Country: China
ProdList: 8025
Advantage: 58

Win-Win chemical CO., Limited

Tel: +86-0086-577-64498589 +86-15355981851
Fax: 0086-577-56994596
Email: sales@win-winchemical.com
Country: China
ProdList: 14359
Advantage: 58

Hubei xin bonus chemical co. LTD

Tel: 86-13657291602
Fax: 027-59338440
Email: linda@hubeijusheng.com
Country: CHINA
ProdList: 22963
Advantage: 58

Qi Qi hang Biotechnology Co., Ltd.

Tel: 18151111370
Email: 1046215251@qq.com
Country: China
ProdList: 5999
Advantage: 58

CONIER CHEM AND PHARMA LIMITED

Tel: +8618523575427
Email: sales@conier.com
Country: China
ProdList: 49975
Advantage: 58

Fuxin Pharmaceutical

Tel: +86-021-021-50872116 +8613122107989
Email: contact@fuxinpharm.com
Country: China
ProdList: 10000
Advantage: 58

Energy Chemical

Tel: 021-58432009 400-005-6266
Fax: 021-58436166
Email: marketing1@energy-chemical.com
Country: China
ProdList: 44894
Advantage: 58

Nanjing Shizhou Biology Technology Co.,Ltd

Tel: 13675144456
Fax: 025-85563444
Email: sean.lv@synzest.com
Country: China
ProdList: 10784
Advantage: 58

Shanghai Sunway Pharmaceutical Technology Co.,Ltd.

Tel: 021-51816796-820 13611835272
Fax: 021-5161 3951
Email: sales2@sunwaypharm.com
Country: China
ProdList: 44119
Advantage: 58

Zhengzhou Akem Chemical Co., Ltd

Tel: 13303867194
Email: 3001317055@qq.com
Country: China
ProdList: 9681
Advantage: 58

Hubei Co-prosperity Medicine Technonlogy Co., Ltd

Tel: 2383948258 19172820304
Email: 2383948258@qq.com
Country: China
ProdList: 12987
Advantage: 58

Hebei Zhentian Food Additives Co., Ltd.

Tel: 0551-77777777-5 13333333333
Fax: 0319 5925599
Country: China
ProdList: 9998
Advantage: 58

Shanghai Haohong Pharmaceutical Co., Ltd.

Tel: 400-8210725 4008210725
Email: malulu@leyan.com
Country: China
ProdList: 40000
Advantage: 58

Bide Pharmatech Ltd.

Tel: 400-6005915
Email: sales@picasso-e.com
Country: China
ProdList: 39653
Advantage: 58

AAB-PHARMA LIMITED

Tel: 02566880956
Email: 3325708371@qq.com
Country: China
ProdList: 7869
Advantage: 58

Shanghai Lingfu Pharmaceutical Research Co. LTD

Tel: +86(21)5895 0110 19945755304
Email: sales@chemany.com
Country: China
ProdList: 9984
Advantage: 58

16582-38-0, 1-chloro-3-methyl-5-nitro-benzeneRelated Search:

2-Amino-3-chloro-5-nitrobenzonitrile 4-AMINO-3-CHLORO-5-NITROBENZOTRIFLUORIDE 3-CHLORO-5-NITROBENZONITRILE Benzoic acid,5-chloro-2-hydroxy-3-nitro- 2-CHLORO-6-METHYL-4-NITROANILINE 2,5-Dichloro-3-nitrobenzoic acid Methyl 3-chloro-5-nitrobenzoate 3-CHLORO-4-FLUORO-5-NITROBENZOTRIFLUORIDE NICLOFOLAN 3-CHLORO-2,6-DIMETHOXY-5-NITROBENZOIC ACID 4-CHLORO-2-METHYL-6-NITROANILINE 6-CHLORO-3,4-DIMETHYL-2-NITROPHENOL 6-chloro-4-nitro-o-cresol 5-CHLORO-2-HYDROXY-3-NITRO-BENZALDEHYDE Nitroclofene 1,2-DICHLORO-3-NITRONAPHTHALENE-BIS(HEXA -CHLOROCYCLOPENTADIENE) ADDUCT, TECH 3-CHLORO-2-IODO-5-NITROTOLUENE 3-CHLORO-2,6-DIMETHOXY-5-NITROBENZAMIDE

1-chloro-3-methyl-5-nitro-benzene

3-CHLORO-5-NITROTOLUENE

3-Chlor-5-nitrotoluene

5-Chloro-3-nitrotoluene

NSC 169207

Benzene, 1-chloro-3-methyl-5-nitro-

1-chloro-3-methyl-5-nitro-benzene ISO 9001：2015 REACH

16582-38-0