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N-METHYLPIPERIDINE-4-CARBOXAMIDE

Product Name
N-METHYLPIPERIDINE-4-CARBOXAMIDE
CAS No.
1903-69-1
Chemical Name
N-METHYLPIPERIDINE-4-CARBOXAMIDE
Synonyms
N-Methyl-piperidin-4-carboxamide;N-Methyl-4-piperidinecarboxaMide;4-Piperidinecarboxamide, N-methyl-;N-methylpiperidin-4-carboxylic acid amide
CBNumber
CB81491915
Molecular Formula
C7H14N2O
Formula Weight
142.2
MOL File
1903-69-1.mol
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N-METHYLPIPERIDINE-4-CARBOXAMIDE Property

Melting point:
123～125℃
Boiling point:
318.5±31.0 °C(Predicted)
Density 
0.997±0.06 g/cm3(Predicted)
pka
16.06±0.20(Predicted)
form 
powder
color 
Yellow
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Safety

HazardClass 
IRRITANT
HS Code 
2933399990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

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N-Bromosuccinimide Price

TRC
Product number
M104460
Product name
N-methylpiperidine-4-carboxamide
Packaging
100mg
Price
$45
Updated
2021/12/16
Apolloscientific
Product number
OR949865
Product name
N-Methylpiperidine-4-carboxamide
Purity
95%
Packaging
250mg
Price
$35
Updated
2021/12/16
Apolloscientific
Product number
OR949865
Product name
N-Methylpiperidine-4-carboxamide
Purity
95%
Packaging
1g
Price
$60
Updated
2021/12/16
AK Scientific
Product number
6412AD
Product name
N-Methylpiperidine-4-carboxamide
Packaging
250mg
Price
$83
Updated
2021/12/16
Matrix Scientific
Product number
016440
Product name
N-Methylpiperidine-4-carboxamide
Packaging
500mg
Price
$184
Updated
2021/12/16
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N-METHYLPIPERIDINE-4-CARBOXAMIDE Chemical Properties,Usage,Production

Synthesis

544696-01-7

1903-69-1

GENERAL STEPS: 1-Boc-4-piperidinyl-N-methylamide (68 mg, 0.28 mmol) was dissolved in methanol (2 mL) and cooled to 0°C. A 1,4-dioxane solution (2 mL) of 4 M hydrogen chloride was slowly added. The reaction mixture was stirred at 0°C for 15 minutes and then gradually warmed to room temperature and continued stirring for 3 hours. After completion of the reaction, the solvent was removed by distillation under reduced pressure. The crude product was purified by SCX-2 column chromatography, eluting first with methanol and then with 0.5 M ammonia in methanol solution to afford N-methylpiperidine-4-carboxamide as a colorless oil (41 mg, 99% yield). The product was detected by infrared spectroscopy (CHCl3) with characteristic absorption peaks of 1308, 2948, 1663, 1525, 1227, 1119 cm-1; mass spectrometry (ESI) analysis showed that the theoretical value of the [M+H]+ ion peak of C7H15N2O was 143.1179 and the measured value was 143.1178.

References

[1] Patent: WO2010/41054, 2010, A1. Location in patent: Page/Page column 32

N-METHYLPIPERIDINE-4-CARBOXAMIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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N-METHYLPIPERIDINE-4-CARBOXAMIDE Suppliers

China 29 Ukraine 1 United States 5 Global 35
Enamine
Tel
--
Fax
--
Email
enamine@enamine.net
Country
Ukraine
ProdList
6216
Advantage
67
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View Lastest Price from N-METHYLPIPERIDINE-4-CARBOXAMIDE manufacturers

Career Henan Chemical Co
Product
N-METHYLPIPERIDINE-4-CARBOXAMIDE 1903-69-1
Price
US $1.00/KG
Min. Order
1KG
Purity
99.0%
Supply Ability
100kg
Release date
2020-01-14

1903-69-1, N-METHYLPIPERIDINE-4-CARBOXAMIDERelated Search:

SPIPERONE FLUSPIRILENE 1-PHENYL-1,3,8-TRIAZASPIRO[4.5]DECAN-4-ONE SPIROXATRINE 1-[3-CHLORO-5-(TRIFLUOROMETHYL)-2-PYRIDINYL]-N-(2-HYDROXYETHYL)-N-METHYL-4-PIPERIDINECARBOXAMIDE 8-[4-(4-FLUOROPHENYL)-4-OXOBUTYL]-1-PHENYL-1,3,8-TRIAZASPIRO[4,5]DECAN-4-ONE HYDROCHLORIDE 1-[3-CHLORO-5-(TRIFLUOROMETHYL)-2-PYRIDINYL]-N-(2-HYDROXYETHYL)-4-PIPERIDINECARBOXAMIDE 7 7 9 9-TETRAMETHYL-1 3 8-TRIAZASPIRO- 8-acetyl-3-dodecyl-7,7,9,9-tetramethyl-1,3,8-triazaspiro[4.5]decane-2,4-dione N-(([(2,6-DICHLOROBENZYL)OXY]IMINO)METHYL)-1-(2-PYRIMIDINYL)-4-PIPERIDINECARBOXAMIDE (1-[3-CHLORO-5-(TRIFLUOROMETHYL)-2-PYRIDINYL]-4-PIPERIDINYL)[4-(4-METHOXYPHENYL)PIPERAZINO]METHANONE N-(P-ISOTHIOCYANATOPHENETHYL)SPIPERONE HYDROCHLORIDE (1-[3-CHLORO-5-(TRIFLUOROMETHYL)-2-PYRIDINYL]-4-PIPERIDINYL)(PIPERIDINO)METHANONE (1-[3-CHLORO-5-(TRIFLUOROMETHYL)-2-PYRIDINYL]-4-PIPERIDINYL)(MORPHOLINO)METHANONE N-(([(4-CHLOROBENZYL)OXY]IMINO)METHYL)-1-(2-PYRIMIDINYL)-4-PIPERIDINECARBOXAMIDE N-METHYL-8-[4-(4-FLUOROPHENYL)-4-OXOBUTYL]-1-PHENYL-1,3,8-TRIAZASPIRO-[4.5]DECAN-4-ONE HYDROCHLORIDE N-(([(3,4-DICHLOROBENZYL)OXY]IMINO)METHYL)-1-(2-PYRIMIDINYL)-4-PIPERIDINECARBOXAMIDE (1-[3-CHLORO-5-(TRIFLUOROMETHYL)-2-PYRIDINYL]-4-PIPERIDINYL)(4-METHYLPIPERAZINO)METHANONE

  • N-Methyl-4-piperidinecarboxaMide
  • 4-Piperidinecarboxamide, N-methyl-
  • N-methylpiperidin-4-carboxylic acid amide
  • N-Methyl-piperidin-4-carboxamide
  • 1903-69-1