2-Boc-amino-4-formylpyridine

Product Name: 2-Boc-amino-4-formylpyridine
CAS No.: 304873-65-2
Chemical Name: 2-Boc-amino-4-formylpyridine
Synonyms: 2-Boc-amino-4-formylpyridin;2-Boc-amino-4-formylpyridine;2-(Boc-amino)pyridine-4-carboxaldehyde;tert-butyl 4-forMylpyridin-2-ylcarbaMate;tert-butyl N-(4-formyl-2-pyridyl)carbamate;(4-Formyl-pyridin-2-yl)-carbamic acid tert-butyl ester;N-(4-Formyl-2-pyridinyl)carbamic acid tert-butyl ester;2-[N,N-mono-(tert-butoxycarbonyl)amino]-pyridyl-4-aldehyde;Carbamic acid, N-(4-formyl-2-pyridinyl)-, 1,1-dimethylethyl ester
CBNumber: CB81501285
Molecular Formula: C11H14N2O3
Formula Weight: 222.24
MOL File: 304873-65-2.mol

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2-Boc-amino-4-formylpyridine Property

Melting point:: 125-126℃
Boiling point:: 308.8±27.0 °C(Predicted)
Density: 1.212
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 12.20±0.70(Predicted)
Appearance: White to off-white Solid

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Safety

HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: T206098
Product name: tert-Butyl(4-Formylpyridin-2-yl)carbamate
Packaging: 50mg
Price: $45
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0152248
Product name: TERT-BUTYL 4-FORMYLPYRIDIN-2-YLCARBAMATE
Purity: 95.00%
Packaging: 5G
Price: $1010.63
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H51-1-4B
Product name: tert-Butyl (4-formylpyridin-2-yl)carbamate
Packaging: 1g
Price: $1220
Updated: 2021/12/16

Matrix Scientific

Product number: 118102
Product name: tert-Butyl (4-formylpyridin-2-yl)carbamate
Packaging: 1g
Price: $1298
Updated: 2021/12/16

AK Scientific

Product number: 3201AB
Product name: tert-Butyl(4-formylpyridin-2-yl)carbamate
Packaging: 100mg
Price: $127
Updated: 2021/12/16

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2-Boc-amino-4-formylpyridine Chemical Properties,Usage,Production

Synthesis

304873-62-9

304873-65-2

General procedure for the synthesis of tert-butyl (4-formylpyridin-2-yl)carbamate from (4-(hydroxymethyl)pyridin-2-yl)carbamate: Synthesis of compound 2G: tert-butyl (4-formylpyridin-2-yl)carbamate Compound 2F ((tert-butyl (4-(hydroxymethyl)pyridin-2-yl)carbamate, 2.5 g, 11.15 mmol, 1.00 eq.) was dissolved in dichloroethane (DCE, 25 mL) followed by addition of manganese dioxide (MnO2, 19.4 g, 223.14 mmol, 20.02 eq.). The reaction mixture was stirred at 70 °C overnight. Upon completion of the reaction, the solid catalyst was removed by filtration. The filtrate was concentrated to dryness under reduced pressure to afford 1.4 g (57% yield) of the target product compound 2G as a white solid.

References

[1] Synthesis, 2007, # 16, p. 2529 - 2533
[2] Patent: WO2003/103669, 2003, A1. Location in patent: Page 21
[3] Patent: WO2008/108958, 2008, A2. Location in patent: Page/Page column 32
[4] Patent: WO2008/108957, 2008, A2. Location in patent: Page/Page column 30
[5] Patent: WO2018/209132, 2018, A1. Location in patent: Paragraph 0526

2-Boc-amino-4-formylpyridine Preparation Products And Raw materials

Raw materials

Preparation Products

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2-Boc-amino-4-formylpyridine Suppliers

China 61 India 1 Switzerland 1 United Kingdom 1 United States 5 Global 69

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304873-65-2, 2-Boc-amino-4-formylpyridineRelated Search:

tert-butyl 2-bromothiazol-4-ylcarbamate 2-Boc-amino-4-formylpyridine ETHYL 2-(TERT-BUTOXYCARBONYLAMINO)ISONICOTINATE 2-Boc-amino-4-pyridinecarboxylic acid (4-METHYL-PYRIDIN-2-YL)-CARBAMIC ACID TERT-BUTYL ESTER

2-Boc-amino-4-formylpyridine

N-(4-Formyl-2-pyridinyl)carbamic acid tert-butyl ester

tert-butyl 4-forMylpyridin-2-ylcarbaMate

2-Boc-amino-4-formylpyridin

(4-Formyl-pyridin-2-yl)-carbamic acid tert-butyl ester

Carbamic acid, N-(4-formyl-2-pyridinyl)-, 1,1-dimethylethyl ester

2-[N,N-mono-(tert-butoxycarbonyl)amino]-pyridyl-4-aldehyde

tert-butyl N-(4-formyl-2-pyridyl)carbamate

2-(Boc-amino)pyridine-4-carboxaldehyde

304873-65-2

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