ChemicalBook > CAS DataBase List > 2-Boc-amino-4-formylpyridine

2-Boc-amino-4-formylpyridine

Product Name
2-Boc-amino-4-formylpyridine
CAS No.
304873-65-2
Chemical Name
2-Boc-amino-4-formylpyridine
Synonyms
2-Boc-amino-4-formylpyridin;2-Boc-amino-4-formylpyridine;2-(Boc-amino)pyridine-4-carboxaldehyde;tert-butyl 4-forMylpyridin-2-ylcarbaMate;tert-butyl N-(4-formyl-2-pyridyl)carbamate;(4-Formyl-pyridin-2-yl)-carbamic acid tert-butyl ester;N-(4-Formyl-2-pyridinyl)carbamic acid tert-butyl ester;2-[N,N-mono-(tert-butoxycarbonyl)amino]-pyridyl-4-aldehyde;Carbamic acid, N-(4-formyl-2-pyridinyl)-, 1,1-dimethylethyl ester
CBNumber
CB81501285
Molecular Formula
C11H14N2O3
Formula Weight
222.24
MOL File
304873-65-2.mol
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2-Boc-amino-4-formylpyridine Property

Melting point:
125-126℃
Boiling point:
308.8±27.0 °C(Predicted)
Density 
1.212
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
pka
12.20±0.70(Predicted)
Appearance
White to off-white Solid
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Safety

HS Code 
2933399990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
T206098
Product name
tert-Butyl(4-Formylpyridin-2-yl)carbamate
Packaging
50mg
Price
$45
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
CHM0152248
Product name
TERT-BUTYL 4-FORMYLPYRIDIN-2-YLCARBAMATE
Purity
95.00%
Packaging
5G
Price
$1010.63
Updated
2021/12/16
SynQuest Laboratories
Product number
4H51-1-4B
Product name
tert-Butyl (4-formylpyridin-2-yl)carbamate
Packaging
1g
Price
$1220
Updated
2021/12/16
Matrix Scientific
Product number
118102
Product name
tert-Butyl (4-formylpyridin-2-yl)carbamate
Packaging
1g
Price
$1298
Updated
2021/12/16
AK Scientific
Product number
3201AB
Product name
tert-Butyl(4-formylpyridin-2-yl)carbamate
Packaging
100mg
Price
$127
Updated
2021/12/16
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2-Boc-amino-4-formylpyridine Chemical Properties,Usage,Production

Synthesis

304873-62-9

304873-65-2

General procedure for the synthesis of tert-butyl (4-formylpyridin-2-yl)carbamate from (4-(hydroxymethyl)pyridin-2-yl)carbamate: Synthesis of compound 2G: tert-butyl (4-formylpyridin-2-yl)carbamate Compound 2F ((tert-butyl (4-(hydroxymethyl)pyridin-2-yl)carbamate, 2.5 g, 11.15 mmol, 1.00 eq.) was dissolved in dichloroethane (DCE, 25 mL) followed by addition of manganese dioxide (MnO2, 19.4 g, 223.14 mmol, 20.02 eq.). The reaction mixture was stirred at 70 °C overnight. Upon completion of the reaction, the solid catalyst was removed by filtration. The filtrate was concentrated to dryness under reduced pressure to afford 1.4 g (57% yield) of the target product compound 2G as a white solid.

References

[1] Synthesis, 2007, # 16, p. 2529 - 2533
[2] Patent: WO2003/103669, 2003, A1. Location in patent: Page 21
[3] Patent: WO2008/108958, 2008, A2. Location in patent: Page/Page column 32
[4] Patent: WO2008/108957, 2008, A2. Location in patent: Page/Page column 30
[5] Patent: WO2018/209132, 2018, A1. Location in patent: Paragraph 0526

2-Boc-amino-4-formylpyridine Preparation Products And Raw materials

Raw materials

Preparation Products

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2-Boc-amino-4-formylpyridine Suppliers

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304873-65-2, 2-Boc-amino-4-formylpyridineRelated Search:

tert-butyl 2-bromothiazol-4-ylcarbamate 2-Boc-amino-4-formylpyridine ETHYL 2-(TERT-BUTOXYCARBONYLAMINO)ISONICOTINATE 2-Boc-amino-4-pyridinecarboxylic acid (4-METHYL-PYRIDIN-2-YL)-CARBAMIC ACID TERT-BUTYL ESTER

  • 2-Boc-amino-4-formylpyridine
  • N-(4-Formyl-2-pyridinyl)carbamic acid tert-butyl ester
  • tert-butyl 4-forMylpyridin-2-ylcarbaMate
  • 2-Boc-amino-4-formylpyridin
  • (4-Formyl-pyridin-2-yl)-carbamic acid tert-butyl ester
  • Carbamic acid, N-(4-formyl-2-pyridinyl)-, 1,1-dimethylethyl ester
  • 2-[N,N-mono-(tert-butoxycarbonyl)amino]-pyridyl-4-aldehyde
  • tert-butyl N-(4-formyl-2-pyridyl)carbamate
  • 2-(Boc-amino)pyridine-4-carboxaldehyde
  • 304873-65-2
  • pharmacetical