TETRABROMO-THIENO[3,2-B]THIOPHENE
- Product Name
- TETRABROMO-THIENO[3,2-B]THIOPHENE
- CAS No.
- 124638-53-5
- Chemical Name
- TETRABROMO-THIENO[3,2-B]THIOPHENE
- Synonyms
- perbromothieno[3,2-b]thiophen;Perbromothieno[3,2-b]thiophene;TETRABROMO-THIENO[3,2-B]THIOPHENE;Tetrabromothiopheno [3,2-B] thiophene;2,3,5,6-TetrabroMothieno[3,2-b]thiophene;Thieno[3,2-b]thiophene,2,3,5,6-tetrabromo-.;TIANFU CHEM-- TETRABROMO-THIENO[3,2-B]THIOPHENE;2,3,5,6-Tetrabromothieno[3,2-b]thiophene
- CBNumber
- CB8166722
- Molecular Formula
- C6Br4S2
- Formula Weight
- 455.81
- MOL File
- 124638-53-5.mol
TETRABROMO-THIENO[3,2-B]THIOPHENE Property
- Melting point:
- 232.0 to 236.0 °C
- Boiling point:
- 443.2±40.0 °C(Predicted)
- Density
- 2.725±0.06 g/cm3(Predicted)
- storage temp.
- Storage temp. 2-8°C
- form
- powder to crystal
- color
- White to Light yellow
Safety
- HS Code
- 2934.99.4400
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- T2772
- Product name
- 2,3,5,6-Tetrabromothieno[3,2-b]thiophene
- Purity
- >98.0%(GC)
- Packaging
- 1g
- Price
- $254
- Updated
- 2025/07/31
- Product number
- P288403
- Product name
- Perbromothieno[3,2-b]thiophene
- Packaging
- 50mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- 099390
- Product name
- Perbromothieno[3,2-b]thiophene
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $265
- Updated
- 2021/12/16
- Product number
- 4683AA
- Product name
- Perbromothieno[3,2-b]thiophene
- Packaging
- 1g
- Price
- $550
- Updated
- 2021/12/16
- Product number
- 099390
- Product name
- Perbromothieno[3,2-b]thiophene
- Purity
- 95+%
- Packaging
- 1g
- Price
- $588
- Updated
- 2021/12/16
TETRABROMO-THIENO[3,2-B]THIOPHENE Chemical Properties,Usage,Production
Synthesis
251-41-2
124638-53-5
S1. Thieno[3,2-b]thiophene (5 g, 35.7 mmol) was dissolved in a solvent mixture of glacial acetic acid (36 ml) and chloroform (10 ml). Bromine (28.5 g, 180.56 mmol) was added slowly dropwise at room temperature and stirring was continued for 30 min after completion of the dropwise addition. The reaction mixture was then heated to 78°C refluxing overnight. After completion of the reaction, it was cooled to room temperature and the reaction mixture was washed with water to precipitate a white solid product. The product was washed sequentially three times each with water and methanol and finally dried under vacuum at room temperature to afford tetrabromothieno[3,2-b]thiophene (Compound 1) as a white solid with mass spectrometry detection [M+] = 455.0 in 95% yield.
References
[1] Patent: CN106188090, 2016, A. Location in patent: Paragraph 0086
[2] Patent: CN107056798, 2017, A. Location in patent: Paragraph 0055; 0056; 0057
[3] Patent: WO2016/92065, 2016, A1. Location in patent: Page/Page column 21
[4] Journal of Materials Chemistry C, 2018, vol. 6, # 16, p. 4471 - 4478
[5] Bulletin of the Chemical Society of Japan, 1989, vol. 62, # 5, p. 1547 - 1555
TETRABROMO-THIENO[3,2-B]THIOPHENE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from TETRABROMO-THIENO[3,2-B]THIOPHENE manufacturers
- Product
- TETRABROMO-THIENO[3,2-B]THIOPHENE 124638-53-5
- Price
- US $0.01/KG
- Min. Order
- 1KG
- Purity
- 98%; 99%
- Supply Ability
- 500g; 1kg; 25kg
- Release date
- 2020-01-10