2-PHENYL-CYCLOPROPANECARBOXYLIC ACID

Product Name: 2-PHENYL-CYCLOPROPANECARBOXYLIC ACID
CAS No.: 5685-38-1
Chemical Name: 2-PHENYL-CYCLOPROPANECARBOXYLIC ACID
Synonyms: Nsc245855;AKOS B022610;AKOS MSC-0115;TIMTEC-BB SBB003944;1-Carboxy-2-phenylcyclopropane;2-PHENYL-CYCLOPROPANECARBOXYLIC ACID;Cyclopropanecarboxylic acid, 2-phenyl-;2-Phenyl-1-cyclopropanecarboxylic acid;2-Phenylcyclopropane-1-carboxylic acid 95+%;1-Carboxy-2-phenylcyclopropane, (2-Carboxycycloprop-1-yl)benzene
CBNumber: CB8174039
Molecular Formula: C10H10O2
Formula Weight: 162.19
MOL File: 5685-38-1.mol

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2-PHENYL-CYCLOPROPANECARBOXYLIC ACID Property

Melting point:: 89-90 °C(Solv: water (7732-18-5))
Boiling point:: 317.1±31.0 °C(Predicted)
Density: 1.250±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
form: solid
pka: 4.57±0.10(Predicted)
color: White
InChI: InChI=1S/C10H10O2/c11-10(12)9-6-8(9)7-4-2-1-3-5-7/h1-5,8-9H,6H2,(H,11,12)
InChIKey: AHDDRJBFJBDEPW-UHFFFAOYSA-N
SMILES: C1(C(O)=O)CC1C1=CC=CC=C1

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Safety

Hazard Codes: Xi
Hazard Note: Irritant
HS Code: 2916399090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

TRC

Product number: P400185
Product name: 2-PhenylcyclopropanecarboxylicAcid
Packaging: 10mg
Price: $45
Updated: 2021/12/16

ChemScene

Product number: CS-W021743
Product name: 2-Phenylcyclopropanecarboxylicacid
Purity: 97.94%
Packaging: 250mg
Price: $50
Updated: 2021/12/16

AK Scientific

Product number: 8324AB
Product name: 2-Phenylcyclopropanecarboxylicacid
Packaging: 100mg
Price: $104
Updated: 2021/12/16

ChemScene

Product number: CS-W021743
Product name: 2-Phenylcyclopropanecarboxylicacid
Purity: 97.94%
Packaging: 1g
Price: $114
Updated: 2021/12/16

SynQuest Laboratories

Product number: 2621-1-X5
Product name: 2-Phenylcyclopropane-1-carboxylic acid
Packaging: 1g
Price: $225
Updated: 2021/12/16

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2-PHENYL-CYCLOPROPANECARBOXYLIC ACID Chemical Properties,Usage,Production

Synthesis

946-38-3

5685-38-1

In a 3000 mL round bottom flask, a methanol (600 mL) solution of ethyl cis-2-phenylcyclopropane-1-carboxylate (120 g, 0.63 mol, 1.00 eq.) was added, followed by a slow addition of a methanol (600 mL) solution of potassium hydroxide (177 g, 3.16 mol, 5.00 eq.). The reaction mixture was stirred at room temperature for 5 hours. Upon completion of the reaction, the reaction solution was concentrated in vacuum by rotary evaporator. The concentrated residue was diluted with 1000 mL of deionized water and the pH was adjusted to 2 with 2 M hydrochloric acid solution. the aqueous phase was extracted with dichloromethane (3 x 1000 mL), the organic layers were combined and washed with brine (1 x 1500 mL). Finally, the organic layer was concentrated in vacuum to give 2-phenylcyclopropanecarboxylic acid (100 g, 98% yield) as a white solid.

References

[1] Patent: WO2014/164867, 2014, A1. Location in patent: Paragraph 0254
[2] Helvetica Chimica Acta, 1986, vol. 69, p. 1655 - 1665

2-PHENYL-CYCLOPROPANECARBOXYLIC ACID Preparation Products And Raw materials

Raw materials

Preparation Products

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2-PHENYL-CYCLOPROPANECARBOXYLIC ACID Suppliers

China 42 Germany 2 India 1 Russia 1 The Netherlands 1 United Kingdom 4 United States 8 Global 59

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View Lastest Price from 2-PHENYL-CYCLOPROPANECARBOXYLIC ACID manufacturers

Career Henan Chemical Co

Product: 2-PHENYL-CYCLOPROPANECARBOXYLIC ACID 5685-38-1
Price: US $9.80/KG
Min. Order: 1g
Purity: ≥99%
Supply Ability: 100kg
Release date: 2020-01-14

5685-38-1, 2-PHENYL-CYCLOPROPANECARBOXYLIC ACIDRelated Search:

Nsc245855

1-Carboxy-2-phenylcyclopropane, (2-Carboxycycloprop-1-yl)benzene

AKOS B022610

AKOS MSC-0115

2-PHENYL-CYCLOPROPANECARBOXYLIC ACID

TIMTEC-BB SBB003944

1-Carboxy-2-phenylcyclopropane

2-Phenylcyclopropane-1-carboxylic acid 95+%

2-Phenyl-1-cyclopropanecarboxylic acid

Cyclopropanecarboxylic acid, 2-phenyl-

5685-38-1

939-36-2