ChemicalBook > CAS DataBase List > 2-PHENYL-CYCLOPROPANECARBOXYLIC ACID

2-PHENYL-CYCLOPROPANECARBOXYLIC ACID

Product Name
2-PHENYL-CYCLOPROPANECARBOXYLIC ACID
CAS No.
5685-38-1
Chemical Name
2-PHENYL-CYCLOPROPANECARBOXYLIC ACID
Synonyms
Nsc245855;AKOS B022610;AKOS MSC-0115;TIMTEC-BB SBB003944;1-Carboxy-2-phenylcyclopropane;2-PHENYL-CYCLOPROPANECARBOXYLIC ACID;Cyclopropanecarboxylic acid, 2-phenyl-;2-Phenyl-1-cyclopropanecarboxylic acid;2-Phenylcyclopropane-1-carboxylic acid 95+%;1-Carboxy-2-phenylcyclopropane, (2-Carboxycycloprop-1-yl)benzene
CBNumber
CB8174039
Molecular Formula
C10H10O2
Formula Weight
162.19
MOL File
5685-38-1.mol
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2-PHENYL-CYCLOPROPANECARBOXYLIC ACID Property

Melting point:
89-90 °C(Solv: water (7732-18-5))
Boiling point:
317.1±31.0 °C(Predicted)
Density 
1.250±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
form 
solid
pka
4.57±0.10(Predicted)
color 
White
InChI
InChI=1S/C10H10O2/c11-10(12)9-6-8(9)7-4-2-1-3-5-7/h1-5,8-9H,6H2,(H,11,12)
InChIKey
AHDDRJBFJBDEPW-UHFFFAOYSA-N
SMILES
C1(C(O)=O)CC1C1=CC=CC=C1
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Safety

Hazard Codes 
Xi
Hazard Note 
Irritant
HS Code 
2916399090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

TRC
Product number
P400185
Product name
2-PhenylcyclopropanecarboxylicAcid
Packaging
10mg
Price
$45
Updated
2021/12/16
ChemScene
Product number
CS-W021743
Product name
2-Phenylcyclopropanecarboxylicacid
Purity
97.94%
Packaging
250mg
Price
$50
Updated
2021/12/16
AK Scientific
Product number
8324AB
Product name
2-Phenylcyclopropanecarboxylicacid
Packaging
100mg
Price
$104
Updated
2021/12/16
ChemScene
Product number
CS-W021743
Product name
2-Phenylcyclopropanecarboxylicacid
Purity
97.94%
Packaging
1g
Price
$114
Updated
2021/12/16
SynQuest Laboratories
Product number
2621-1-X5
Product name
2-Phenylcyclopropane-1-carboxylic acid
Packaging
1g
Price
$225
Updated
2021/12/16
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2-PHENYL-CYCLOPROPANECARBOXYLIC ACID Chemical Properties,Usage,Production

Synthesis

946-38-3

5685-38-1

In a 3000 mL round bottom flask, a methanol (600 mL) solution of ethyl cis-2-phenylcyclopropane-1-carboxylate (120 g, 0.63 mol, 1.00 eq.) was added, followed by a slow addition of a methanol (600 mL) solution of potassium hydroxide (177 g, 3.16 mol, 5.00 eq.). The reaction mixture was stirred at room temperature for 5 hours. Upon completion of the reaction, the reaction solution was concentrated in vacuum by rotary evaporator. The concentrated residue was diluted with 1000 mL of deionized water and the pH was adjusted to 2 with 2 M hydrochloric acid solution. the aqueous phase was extracted with dichloromethane (3 x 1000 mL), the organic layers were combined and washed with brine (1 x 1500 mL). Finally, the organic layer was concentrated in vacuum to give 2-phenylcyclopropanecarboxylic acid (100 g, 98% yield) as a white solid.

References

[1] Patent: WO2014/164867, 2014, A1. Location in patent: Paragraph 0254
[2] Helvetica Chimica Acta, 1986, vol. 69, p. 1655 - 1665

2-PHENYL-CYCLOPROPANECARBOXYLIC ACID Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-PHENYL-CYCLOPROPANECARBOXYLIC ACID manufacturers

Career Henan Chemical Co
Product
2-PHENYL-CYCLOPROPANECARBOXYLIC ACID 5685-38-1
Price
US $9.80/KG
Min. Order
1g
Purity
≥99%
Supply Ability
100kg
Release date
2020-01-14

5685-38-1, 2-PHENYL-CYCLOPROPANECARBOXYLIC ACIDRelated Search:

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  • Nsc245855
  • 1-Carboxy-2-phenylcyclopropane, (2-Carboxycycloprop-1-yl)benzene
  • AKOS B022610
  • AKOS MSC-0115
  • 2-PHENYL-CYCLOPROPANECARBOXYLIC ACID
  • TIMTEC-BB SBB003944
  • 1-Carboxy-2-phenylcyclopropane
  • 2-Phenylcyclopropane-1-carboxylic acid 95+%
  • 2-Phenyl-1-cyclopropanecarboxylic acid
  • Cyclopropanecarboxylic acid, 2-phenyl-
  • 5685-38-1
  • 939-36-2