ChemicalBook > CAS DataBase List > 3-FLUORO-5-NITROBENZONITRILE

3-FLUORO-5-NITROBENZONITRILE

Product Name
3-FLUORO-5-NITROBENZONITRILE
CAS No.
110882-60-5
Chemical Name
3-FLUORO-5-NITROBENZONITRILE
Synonyms
3-FLUORO-5-NITROBENZONITRILE;3-Cyano-5-fluoronitrobenzene;3-fluoro-5-nitrobenzenitrile;Benzonitrile,3-fluoro-5-nitro-;3-FLUORO-5-NITROBENZONITRILE, 97% MIN.
CBNumber
CB8175935
Molecular Formula
C7H3FN2O2
Formula Weight
166.11
MOL File
110882-60-5.mol
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3-FLUORO-5-NITROBENZONITRILE Property

Melting point:
50°C
Boiling point:
255.3±25.0 °C(Predicted)
Density 
1.41±0.1 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
form 
solid
color 
off-white to yellow
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Safety

HS Code 
2926907090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
F594918
Product name
3-Fluoro-5-nitrobenzonitrile
Packaging
100mg
Price
$45
Updated
2021/12/16
Oakwood
Product number
022023
Product name
3-Fluoro-5-nitrobenzonitrile
Packaging
100mg
Price
$30
Updated
2021/12/16
AK Scientific
Product number
X8963
Product name
3-Fluoro-5-nitrobenzonitrile
Packaging
250mg
Price
$89
Updated
2021/12/16
SynQuest Laboratories
Product number
4655-3-53
Product name
3-Fluoro-5-nitrobenzonitrile
Purity
97%
Packaging
1g
Price
$185
Updated
2021/12/16
Matrix Scientific
Product number
114183
Product name
3-Fluoro-5-nitrobenzonitrile
Purity
97%
Packaging
1g
Price
$480
Updated
2021/12/16
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3-FLUORO-5-NITROBENZONITRILE Chemical Properties,Usage,Production

Synthesis

3819-88-3

557-21-1

110882-60-5

Step 1: Zinc cyanide (0.92 eq.) and tetrakis(triphenylphosphine)palladium (0.058 eq.) were sequentially added to a 1.0 eq. solution of 1-fluoro-3-iodo-5-nitrobenzene in anhydrous DMF (0.37 M) under nitrogen protection. The reaction mixture was heated to 80 °C and the reaction was stirred overnight. Subsequently, 0.023 equivalents of tetrakis(triphenylphosphine)palladium was added and the reaction continued to be stirred at 80°C for 6 hours. Upon completion of the reaction, the mixture was cooled to room temperature and diluted with 15 volumes of ethyl acetate (based on the amount of 1-fluoro-3-iodo-5-nitrobenzene). The organic phase was sequentially washed three times with water and once with saturated saline. The organic layer was dried over anhydrous sodium sulfate, filtered and concentrated under reduced pressure. The crude product was purified by silica gel column chromatography with 10% ether/hexane as eluent to give 3-fluoro-5-nitrobenzonitrile as a solid in 90% yield.

References

[1] Patent: US2006/14761, 2006, A1. Location in patent: Page/Page column 29
[2] Patent: WO2007/75377, 2007, A2. Location in patent: Page/Page column 52-53
[3] Patent: WO2007/70626, 2007, A2. Location in patent: Page/Page column 40
[4] Patent: WO2007/70683, 2007, A2. Location in patent: Page/Page column 83
[5] Patent: WO2007/78839, 2007, A2. Location in patent: Page/Page column 40-41

3-FLUORO-5-NITROBENZONITRILE Preparation Products And Raw materials

Raw materials

Preparation Products

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3-FLUORO-5-NITROBENZONITRILE Suppliers

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View Lastest Price from 3-FLUORO-5-NITROBENZONITRILE manufacturers

Career Henan Chemical Co
Product
3-FLUORO-5-NITROBENZONITRILE 110882-60-5
Price
US $6.60/KG
Min. Order
1KG
Purity
97%-99%
Supply Ability
1kg-1000kg
Release date
2019-12-26

110882-60-5, 3-FLUORO-5-NITROBENZONITRILERelated Search:

2-bromo-4-fluoro-5-nitrobenzonitrile 4-amino-2-fluoro-5-nitrobenzonitrile 5-Fluoro-2-nitrobenzonitrile98%,5-FLUORO-2-NITROBENZONITRILE,5-Fluoro-2-nitrobenzonitrile 98% 2-CHLORO-6-FLUORO-3-NITROBENZONITRILE 3-FLUORO-4-NITROBENZONITRILE 4-FLUORO-2-NITROBENZONITRILE 4-FLUORO-3-NITROBENZONITRILE 3-Fluoro-2-nitrobenzonitrile 2-Fluoro-5-nitrobenzonitrile 97%,2-Fluoro-5-nitrobenzonitrile, 98+%,2-Fluoro-5-nitrobenzonitrile97%,2-FLUORO-5-NITROBENZONITRILE 2-FLUORO-6-NITROBENZONITRILE 2-AMINO-5-FLUORO-4-NITROBENZONITRILE 2-FLUORO-4-NITROBENZONITRILE,2-Fluoro-4-nitrobenzonitrile ,98% 3,4-Difluoro-5-Nitrobenzonitrile 3-FLUORO-5-NITROBENZONITRILE 5-Amino-3-fluorobenzonitrile 3-Fluoro-5-nitrotoluene

  • 3-FLUORO-5-NITROBENZONITRILE
  • 3-FLUORO-5-NITROBENZONITRILE, 97% MIN.
  • 3-Cyano-5-fluoronitrobenzene
  • Benzonitrile,3-fluoro-5-nitro-
  • 3-fluoro-5-nitrobenzenitrile
  • 110882-60-5
  • 11082-60-5