ChemicalBook > CAS DataBase List > 5-BROMO-2-PHENOXYPYRIMIDINE

5-BROMO-2-PHENOXYPYRIMIDINE

Product Name: 5-BROMO-2-PHENOXYPYRIMIDINE
CAS No.: 257280-25-4
Chemical Name: 5-BROMO-2-PHENOXYPYRIMIDINE
Synonyms: 5-BROMO-2-PHENOXYPYRIMIDINE;Pyrimidine, 5-bromo-2-phenoxy-;5-BROMO-2-PHENOXYPYRIMIDINE ISO 9001：2015 REACH
CBNumber: CB8203520
Molecular Formula: C10H7BrN2O
Formula Weight: 251.08
MOL File: 257280-25-4.mol

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5-BROMO-2-PHENOXYPYRIMIDINE Property

storage temp.: Sealed in dry,Room Temperature

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Safety

Risk Statements: 43
Safety Statements: 36/37

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B687403
Product name: 5-Bromo-2-phenoxypyrimidine
Packaging: 250mg
Price: $55
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB140721
Product name: 5-Bromo-2-phenoxypyrimidine
Packaging: 2g
Price: $55
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB140721
Product name: 5-Bromo-2-phenoxypyrimidine
Packaging: 5G
Price: $110
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: COR0003308
Product name: 5-BROMO-2-PHENOXYPYRIMIDINE
Purity: 95.00%
Packaging: 1G
Price: $135.45
Updated: 2021/12/16

Matrix Scientific

Product number: 072020
Product name: 5-Bromo-2-phenoxypyrimidine
Purity: 95+%
Packaging: 1g
Price: $185
Updated: 2021/12/16

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5-BROMO-2-PHENOXYPYRIMIDINE Chemical Properties,Usage,Production

Synthesis

183438-24-6

108-95-2

257280-25-4

Step A: Synthesis of 5-bromo-2-phenoxypyrimidine 5-Bromo-2-iodopyrimidine (Bridge Organics, 1.01 g, 3.57 mmol), phenol (Aldrich, 3.35 g, 35.7 mmol) and potassium carbonate (Aldrich, 4.93 g, 35.7 mmol) were mixed under nitrogen protection and the reaction was stirred for 4 hr at 165°C. Upon completion of the reaction, the mixture was cooled to room temperature, followed by liquid-liquid partition extraction with ethyl acetate (250 mL) and 1N hydrochloric acid (4 × 200 mL). The organic phase was washed with 1N hydrochloric acid until the aqueous phase was colorless. The organic phase was separated and washed sequentially with water (100 mL) and saturated saline (100 mL). The organic layer was dried over anhydrous magnesium sulfate and concentrated under reduced pressure to give an orange oily crude product (1.1 g). The crude product was purified by fast silica gel column chromatography using an 80 g Silicycle silica gel column with 10% ethyl acetate in hexane solution as eluent to afford the target compound 5-bromo-2-phenoxypyrimidine as a white solid (0.82 g, 92% yield). Thin layer chromatography (TLC) analysis showed an Rf value of 0.51 (unfolding agent: hexane-ethyl acetate, 8:2 v/v). Product characterization data: 1H-NMR (400 MHz, CDCl3) δ 8.56 (s, 2H), 7.46-7.41 (m, 2H), 7.30-7.24 (m, 1H), 7.20-7.16 (m, 2H); Mass spectrum (APCI+) m/z 252.9 (M + 1).

References

[1] Patent: US2010/75990, 2010, A1. Location in patent: Page/Page column 40
[2] Patent: CN108069974, 2018, A. Location in patent: Paragraph 0194-0196

5-BROMO-2-PHENOXYPYRIMIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 5-BROMO-2-PHENOXYPYRIMIDINE manufacturers

Dideu Industries Group Limited

Product: 5-BROMO-2-PHENOXYPYRIMIDINE 257280-25-4
Price: US $1.10/g
Min. Order: 1g
Purity: 99.00%
Supply Ability: 100 Tons Min
Release date: 2021-12-01

Zhuozhou Wenxi import and Export Co., Ltd

Product: 5-BROMO-2-PHENOXYPYRIMIDINE 257280-25-4
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-07-10

Zhuozhou Wenxi import and Export Co., Ltd

Product: 5-BROMO-2-PHENOXYPYRIMIDINE 257280-25-4
Price: US $15.00-10.00/KG
Min. Order: 1KG
Purity: 99%+ HPLC
Supply Ability: Monthly supply of 1 ton
Release date: 2021-07-09

257280-25-4, 5-BROMO-2-PHENOXYPYRIMIDINERelated Search:

5-BROMO-2-PHENOXYPYRIMIDINE 5-BROMO-2-(4-CHLOROPHENOXY)PYRIMIDINE 5-BROMO-2-(P-TOLYLOXY)PYRIMIDINE N-(4-(5-bromo-2-pyrimidinyloxy)-3-chlorophenyl)-N'-(2-nitrobenzoyl)urea 5-BROMO-2-(4-METHOXYPHENOXY)PYRIMIDINE 4-[(5-BROMOPYRIMIDIN-2-YL)OXY]BENZONITRILE 5-BROMO-2-(4-FLUOROPHENOXY)PYRIMIDINE 2-(4-[(5-BROMOPYRIMIDIN-2-YL)OXY]PHENYL)ACETAMIDE N-(4-[(5-BROMOPYRIMIDIN-2-YL)OXY]PHENYL)ACETAMIDE 8-[(5-BROMOPYRIMIDIN-2-YL)OXY]-2-METHYLQUINOLINE 5-BROMO-2-(4-PHENOXYPHENOXY)PYRIMIDINE 5-BROMO-2-[4-(TRIFLUOROMETHYL)PHENOXY]PYRIMIDINE 5-BROMO-2-[4-(METHYLSULFONYL)PHENOXY]PYRIMIDINE N-(3-[(5-BROMOPYRIMIDIN-2-YL)OXY]PHENYL)ACETAMIDE 5-BROMO-2-(4-TERT-BUTYLPHENOXY)PYRIMIDINE 8-[(5-BROMOPYRIMIDIN-2-YL)OXY]QUINOLINE 2-((4-[(5-BROMOPYRIMIDIN-2-YL)OXY]PHENYL)THIO)-4,6-DIMETHYLPYRIMIDINE N-(((4-((5-Bromo-2-pyrimidinyl)oxy)-3-nitrophenyl)amino)carbonyl)-2-ni trobenzamide

5-BROMO-2-PHENOXYPYRIMIDINE

Pyrimidine, 5-bromo-2-phenoxy-

5-BROMO-2-PHENOXYPYRIMIDINE ISO 9001：2015 REACH

257280-25-4

Heterocycle-Pyrimidine series