Ethanone,1-(2-amino-3-methoxyphenyl)-

Product Name: Ethanone,1-(2-amino-3-methoxyphenyl)-
CAS No.: 42465-54-3
Chemical Name: Ethanone,1-(2-amino-3-methoxyphenyl)-
Synonyms: 1-(2-Amino-3-methoxyphenyl);2’-Amino-3’-methoxyacetophenone;1-(2-Amino-3-methoxy-phenyl)-ethanone;Ethanone,1-(2-amino-3-methoxyphenyl)-
CBNumber: CB82077374
Molecular Formula: C9H11NO2
Formula Weight: 165.19
MOL File: 42465-54-3.mol

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Ethanone,1-(2-amino-3-methoxyphenyl)- Property

storage temp.: Keep in dark place,Inert atmosphere,Room temperature
Appearance: White to light yellow Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H313May be harmful in contact with skin

H317May cause an allergic skin reaction

H373May cause damage to organs through prolonged or repeated exposure

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P270Do not eat, drink or smoke when using this product.

P272Contaminated work clothing should not be allowed out of the workplace.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P314Get medical advice/attention if you feel unwell.

P330Rinse mouth.

P333+P313IF SKIN irritation or rash occurs: Get medical advice/attention.

P363Wash contaminated clothing before reuse.

P403Store in a well-ventilated place.

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N-Bromosuccinimide Price

AK Scientific

Product number: 5856AB
Product name: 1-(2-Amino-3-methoxyphenyl)ethanone
Packaging: 100mg
Price: $108
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FA11527
Product name: 1-(2-Amino-3-methoxyphenyl)ethanone
Packaging: 50mg
Price: $160
Updated: 2021/12/16

AK Scientific

Product number: 5856AB
Product name: 1-(2-Amino-3-methoxyphenyl)ethanone
Packaging: 1g
Price: $308
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0386658
Product name: 1-(2-AMINO-3-METHOXYPHENYL)ETHANONE
Purity: 95.00%
Packaging: 5MG
Price: $504.65
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FA11527
Product name: 1-(2-Amino-3-methoxyphenyl)ethanone
Packaging: 500mg
Price: $600
Updated: 2021/12/16

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Ethanone,1-(2-amino-3-methoxyphenyl)- Chemical Properties,Usage,Production

Synthesis

33852-43-6

42465-54-3

The general steps for the synthesis of 1-(2-amino-3-methoxy-phenyl)-acetophenone from 3'-methoxy-2'-nitroacetophenone are as follows: Step 1. Preparation of 3-methoxy-2-amino benzaldehyde A 1:1 mixture of ethanol and acetic acid was used as reaction solvent and 3-methoxy-2-nitrobenzaldehyde (1 eq.) and iron powder (3 eq.) were added in batches. The reaction was completed within 3 hours. Upon completion of the reaction, the reaction mixture was filtered and subsequently concentrated. The concentrate was partitioned between ethyl acetate and water. The organic layer was washed with saturated sodium bicarbonate solution, dried and concentrated to give 2-amino-3-methoxybenzaldehyde in 85% yield.ES/MS m/z 151 (MH+).

References

[1] Patent: WO2007/117607, 2007, A2. Location in patent: Page/Page column 348
[2] Journal of Organic Chemistry, 2007, vol. 72, # 18, p. 6873 - 6877
[3] Patent: US4620000, 1986, A
[4] Patent: US4666499, 1987, A
[5] Patent: US2011/144115, 2011, A1. Location in patent: Page/Page column 7

Ethanone,1-(2-amino-3-methoxyphenyl)- Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from Ethanone,1-(2-amino-3-methoxyphenyl)- manufacturers

Shaanxi Dideu New Materials Co. Ltd

Product: Ethanone,1-(2-amino-3-methoxyphenyl)- 42465-54-3
Price: US $0.00/kg
Min. Order: 1kg
Purity: 98%
Supply Ability: 1000kg
Release date: 2025-06-11

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Ethanone,1-(2-amino-3-methoxyphenyl)-

1-(2-Amino-3-methoxy-phenyl)-ethanone

1-(2-Amino-3-methoxyphenyl)

2’-Amino-3’-methoxyacetophenone

42465-54-3