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dibenzyl phosphate, silver salt

Product Name: dibenzyl phosphate, silver salt
CAS No.: 50651-75-7
Chemical Name: dibenzyl phosphate, silver salt
Synonyms: Silver(I) dibenzyl phosphate;dibenzylphosphate,sliversalt;dibenzyl phosphate, silver salt;Phosphoric acid silver(I)dibenzyl ester salt
CBNumber: CB82078977
Formula Weight: 0
MOL File: 50651-75-7.mol

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dibenzyl phosphate, silver salt Property

Melting point:: 215 °C
storage temp.: Keep in dark place,Inert atmosphere,Room temperature
solubility: DMSO (Slightly), Methanol (Slightly, Heated)
form: Solid
color: Pale Beige to Light Brown

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: P359405
Product name: PhosphoricAcidDibenzylEsterSilverSalt
Packaging: 2.5g
Price: $1390
Updated: 2021/12/16

AK Scientific

Product number: X3715
Product name: Silverdibenzylphosphatesalt
Packaging: 5g
Price: $662
Updated: 2021/12/16

Ark Pharm

Product number: AK554457
Product name: Silver(I)dibenzylphosphate
Purity: 97%
Packaging: 250mg
Price: $34
Updated: 2021/12/16

AK Scientific

Product number: X3715
Product name: Silverdibenzylphosphatesalt
Packaging: 100mg
Price: $192
Updated: 2021/12/16

AK Scientific

Product number: X3715
Product name: Silverdibenzylphosphatesalt
Packaging: 250mg
Price: $232
Updated: 2021/12/16

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dibenzyl phosphate, silver salt Chemical Properties,Usage,Production

Uses

Phosphoric Acid Dibenzyl Ester Silver Salt is a reactant of cortisone 21-phosphate.

Synthesis

1623-08-1

50651-75-7

Dibenzyl phosphate (2.78 g, 10 mmol) was dissolved in water (40 mL) and cooled in an ice bath. Under stirring conditions, a 1 N NaOH solution was added slowly and dropwise until the pH of the reaction mixture was about 7, at which point the solid was almost completely dissolved. Subsequently, a solution of silver nitrate (1.89 g, 11 mmol) in water (20 mL) was slowly added. After addition, the resulting white solid was collected by filtration and washed with deionized water. Finally, the resulting solid was placed on phosphorus pentoxide and vacuum dried to give silver dibenzyl phosphate (3.18 g, 82.5% yield) as a white solid.

References

[1] Patent: WO2013/16668, 2013, A2. Location in patent: Paragraph 00249; 00250

dibenzyl phosphate, silver salt Preparation Products And Raw materials

Raw materials

Preparation Products

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50651-75-7, dibenzyl phosphate, silver saltRelated Search:

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50651-75-7