3-Hydroxy-2-naphthalenecarboxylic acid ethyl ester
- Product Name
- 3-Hydroxy-2-naphthalenecarboxylic acid ethyl ester
- CAS No.
- 7163-25-9
- Chemical Name
- 3-Hydroxy-2-naphthalenecarboxylic acid ethyl ester
- Synonyms
- 3-Hydroxy-2-naphthoic acid ethyl ester;Ethyl 3-hydroxynaphthalene-2-carboxylate;3-Hydroxy-2-naphthalenecarboxylic acid ethyl ester;3-Hydroxy-naphthalene-2-carboxylic acid ethyl ester;2-Naphthalenecarboxylic acid, 3-hydroxy-, ethyl ester
- CBNumber
- CB82263942
- Molecular Formula
- C13H12O3
- Formula Weight
- 216.23
- MOL File
- 7163-25-9.mol
3-Hydroxy-2-naphthalenecarboxylic acid ethyl ester Property
- Melting point:
- 79.0 to 83.0 °C
- Boiling point:
- 291°C(lit.)
- Density
- 1.1652 (rough estimate)
- refractive index
- 1.5090 (estimate)
- solubility
- soluble in Toluene
- form
- powder to crystal
- pka
- 9.53±0.40(Predicted)
- color
- White to Orange to Green
Safety
- HS Code
- 2918290090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
N-Bromosuccinimide Price
- Product number
- E1249
- Product name
- Ethyl 3-Hydroxy-2-naphthoate
- Purity
- >98.0%(GC)
- Packaging
- 1g
- Price
- $57
- Updated
- 2024/03/01
- Product number
- E1249
- Product name
- Ethyl 3-Hydroxy-2-naphthoate
- Purity
- >98.0%(GC)
- Packaging
- 5g
- Price
- $284
- Updated
- 2024/03/01
- Product number
- E940608
- Product name
- Ethyl 3-Hydroxy-2-naphthoate
- Packaging
- 50mg
- Price
- $155
- Updated
- 2021/12/16
- Product number
- OR27972
- Product name
- Ethyl 3-Hydroxy-2-naphthoate
- Packaging
- 1g
- Price
- $206
- Updated
- 2021/12/16
- Product number
- 2629-1-Z9
- Product name
- Ethyl 3-hydroxy-2-naphthoate
- Packaging
- 1g
- Price
- $228
- Updated
- 2021/12/16
3-Hydroxy-2-naphthalenecarboxylic acid ethyl ester Chemical Properties,Usage,Production
Uses
3-Hydroxy-2-naphthalenecarboxylic acid ethyl ester can be used as organic synthesis intermediate and pharmaceutical intermediate, mainly used in laboratory research and development process and chemical production process.
Synthesis
To a round bottom flask were added 5 g 3-hydroxy-2-naphthalic acidand 16 mL ethanol. The reaction mixture was refluxed for 6 h. After thecompletion of the reaction, the reaction mixture was cooled down to room temperature and washed with distilled water. The organic layerwas recovered and washed with saturated sodium bicarbonate followedby drying with anhydrous MgSO4. The MgSO4 was removed by filtrationand the filtrate was dried under reduced pressure. The resulted solid waspurified by silica chromatography with petroleum ether and ethyl acetate(10:1, v/v) as eluent to give the compound ethyl 3-hydroxy-2-naphthoate(4.1229 g, yield 70.60%).
3-Hydroxy-2-naphthalenecarboxylic acid ethyl ester Preparation Products And Raw materials
Raw materials
Preparation Products
3-Hydroxy-2-naphthalenecarboxylic acid ethyl ester Suppliers
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