ChemicalBook > CAS DataBase List > 5-BROMO-2,4-DIMETHYLPYRIDINE

5-BROMO-2,4-DIMETHYLPYRIDINE

Product Name
5-BROMO-2,4-DIMETHYLPYRIDINE
CAS No.
27063-92-9
Chemical Name
5-BROMO-2,4-DIMETHYLPYRIDINE
Synonyms
5-BROMO-2,4-DIMETHYLPYRIDINE;3-Bromo-4,6-dimethylpyridine;PYRIDINE, 5-BROMO-2,4-DIMETHYL-;5-BROMO-2,4-DIMETHYLPYRIDINE ISO 9001：2015 REACH
CBNumber
CB82451680
Molecular Formula
C7H8BrN
Formula Weight
186.05
MOL File
27063-92-9.mol
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5-BROMO-2,4-DIMETHYLPYRIDINE Property

Boiling point:
205-210 °C
Density 
1.415±0.06 g/cm3(Predicted)
storage temp. 
Inert atmosphere,Room Temperature
pka
4.25±0.18(Predicted)
Appearance
Light yellow to gray Liquid
InChI
InChI=1S/C7H8BrN/c1-5-3-6(2)9-4-7(5)8/h3-4H,1-2H3
InChIKey
SLMUXUHXAIPROA-UHFFFAOYSA-N
SMILES
C1(C)=NC=C(Br)C(C)=C1
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Safety

HS Code 
2933399990
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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC
Product number
B623685
Product name
5-Bromo-2,4-dimethylpyridine
Packaging
50mg
Price
$90
Updated
2021/12/16
TRC
Product number
B623685
Product name
5-Bromo-2,4-dimethylpyridine
Packaging
100mg
Price
$130
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB55723
Product name
5-Bromo-2,4-dimethylpyridine
Packaging
50mg
Price
$65
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB55723
Product name
5-Bromo-2,4-dimethylpyridine
Packaging
100mg
Price
$100
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB55723
Product name
5-Bromo-2,4-dimethylpyridine
Packaging
250mg
Price
$175
Updated
2021/12/16
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5-BROMO-2,4-DIMETHYLPYRIDINE Chemical Properties,Usage,Production

Synthesis

3430-26-0

75-16-1

27063-92-9

A solution of 2,5-dibromo-4-methylpyridine (2.51 g, 10.0 mmol) in anhydrous THF (50 mL) was added to a three-necked flask, followed by tetrakis(triphenylphosphine)palladium (1.15 g, 1.0 mmol). The reaction mixture was cooled to 0 °C under nitrogen protection and stirred. A THF solution of methylmagnesium bromide (15 mL, 15.0 mmol, 1 mol/L) was added slowly and dropwise. After the dropwise addition, the reaction mixture was heated to reflux for 3 hours. After completion of the reaction, it was cooled to room temperature, the reaction was quenched with 1N hydrochloric acid and extracted with ethyl acetate (100 mL x 3). The organic layers were combined, washed sequentially with water (50 mL x 2) and saturated saline (50 mL) and dried over anhydrous sodium sulfate. After concentration under reduced pressure, the crude product was purified by Biotage fast chromatography (petroleum ether/ethyl acetate = 5%-10%) to afford 2,4-dimethyl-5-bromopyridine (301 mg, 16.2%) as a colorless oil.1H NMR (400 MHz, CDCl3) δppm: 2.35 (d, 3H), 2.47 (s, 3H), 7.04 ( s, 1H), 8.50 (s, 1H).

References

[1] Patent: WO2017/221092, 2017, A1. Location in patent: Paragraph 00190

5-BROMO-2,4-DIMETHYLPYRIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

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5-BROMO-2,4-DIMETHYLPYRIDINE Suppliers

China 68 Germany 1 India 1 United Kingdom 1 United States 5 Global 76
Aikon International Limited
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View Lastest Price from 5-BROMO-2,4-DIMETHYLPYRIDINE manufacturers

Dideu Industries Group Limited
Product
5-BROMO-2,4-DIMETHYLPYRIDINE 27063-92-9
Price
US $1.10/g
Min. Order
1g
Purity
99.00%
Supply Ability
100 Tons min
Release date
2021-08-24
Shaanxi Dideu Medichem Co. Ltd
Product
5-Bromo-2,4-Dimethylpyridine 27063-92-9
Price
US $0.00-0.00/Kg
Min. Order
1KG
Purity
99.0%
Supply Ability
500 MT
Release date
2020-05-12
Career Henan Chemical Co
Product
5-BROMO-2,4-DIMETHYLPYRIDINE 27063-92-9
Price
US $1.00/KG
Min. Order
1KG
Purity
97%-99.9%
Supply Ability
100kg
Release date
2019-12-20

27063-92-9, 5-BROMO-2,4-DIMETHYLPYRIDINERelated Search:

BIS(2,4,6-TRIMETHYLPYRIDINE)BROMONIUM HEXAFLUOROPHOSPHATE 5-BROMO-4-METHYL-PYRIDINE-2-CARBOXYLIC ACID 3,5-DIBROMO-2,4,6-TRIMETHYLPYRIDINE 3-Bromo-2,4,6-trimethylpyridine 3-Amino-4-methylpyridine 5-Bromo-2,4-bis(trifluoromethyl)pyridine 5-BROMO-2-(TRIFLUOROMETHYL)PYRIDINE-4-CARBOXYLIC ACID (5-BROMO-4-METHYL-PYRIDIN-2-YL)-ACETONITRILE 5-BROMO-4-METHYL-PYRIDINE-2-CARBOXYLIC ACID METHYL ESTER 5-BROMO-4-METHYL-PYRIDINE-2-CARBONITRILE 5-BROMO-2,4-DIMETHYLPYRIDINE 2-Amino-3,5-dibromo-4,6-dimethylpyridine (5-BROMO-4-METHYL-PYRIDIN-2-YL)-ACETIC ACID METHYL ESTER AKOS 90390 5-BROMO-4-METHYL-PYRIDINE-2-CARBALDEHYDE (5-BROMO-4-METHYL-PYRIDIN-2-YL)-ACETIC ACID 2-(5-BROMO-4-METHYL-PYRIDIN-2-YL)-ETHYLAMINE C-(5-BROMO-4-METHYL-PYRIDIN-2-YL)-METHYLAMINE

  • 5-BROMO-2,4-DIMETHYLPYRIDINE
  • PYRIDINE, 5-BROMO-2,4-DIMETHYL-
  • 3-Bromo-4,6-dimethylpyridine
  • 5-BROMO-2,4-DIMETHYLPYRIDINE ISO 9001：2015 REACH
  • 27063-92-9
  • Heterocycle-Pyridine series