ChemicalBook > CAS DataBase List > 2-(Hydroxymethyl)isonicotinic acid

2-(Hydroxymethyl)isonicotinic acid

Product Name
2-(Hydroxymethyl)isonicotinic acid
CAS No.
915140-06-6
Chemical Name
2-(Hydroxymethyl)isonicotinic acid
Synonyms
2-Hydroxymethylisonicotinic acid;2-(hydroxymethyl)-4-pyridinecarboxylic acid;4-PYRIDINECARBOXYLIC ACID, 2-(HYDROXYMETHYL)-
CBNumber
CB82468677
Molecular Formula
C7H7NO3
Formula Weight
153.14
MOL File
915140-06-6.mol
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2-(Hydroxymethyl)isonicotinic acid Property

Boiling point:
478.4±35.0 °C(Predicted)
Density 
1.404
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
pka
1.95±0.10(Predicted)
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

American Custom Chemicals Corporation
Product number
CHM0388281
Product name
2-(HYDROXYMETHYL)ISONICOTINIC ACID
Purity
95.00%
Packaging
5MG
Price
$497.45
Updated
2021/12/16
Medical Isotopes, Inc.
Product number
35932
Product name
2-(Hydroxymethyl)isonicotinicacid
Purity
95+%
Packaging
1g
Price
$880
Updated
2021/12/16
Chemenu
Product number
CM178301
Product name
2-(Hydroxymethyl)isonicotinicacid
Purity
95%
Packaging
5g
Price
$1122
Updated
2021/12/16
Chemenu
Product number
CM178301
Product name
2-(Hydroxymethyl)isonicotinicacid
Purity
95%
Packaging
10g
Price
$1683
Updated
2021/12/16
Chemenu
Product number
CM178301
Product name
2-(Hydroxymethyl)isonicotinicacid
Purity
95%
Packaging
25g
Price
$2992
Updated
2021/12/16
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2-(Hydroxymethyl)isonicotinic acid Chemical Properties,Usage,Production

Synthesis

Ethyl 2-(hydroxymethyl)isonicotinate (iso-EhmnH) (4.84 g, 26.7 mmol) was dissolved in THF/H2O (40 mL, v:v = 1:1). KOH (4.58 g, 81.6 mmol, 3 eq.) was added as solid and the mixture stirred at 100 °C for 20 h and then cooled to r.t. The mixture was further cooled in ice-water and then HNO3 added to adjust the pH to 4–5. The solvent was removed under vacuum. The organic part in the solid mixture was then extracted twice with 400 mL of ethanol and the solvent removed. The powder contains inorganic material was added in hot isopropanol and then filtered, evaporation of iso-propanol yielded iso-hmnH2 as white powder. Yield 2.93 g, 72%[1].

References

[1] Armaghan M, et al. Isolation of first row transition metal–carboxylate zwitterions. RSC Advances, 2015; 5: 42978-42989.

2-(Hydroxymethyl)isonicotinic acid Preparation Products And Raw materials

Raw materials

Preparation Products

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2-(Hydroxymethyl)isonicotinic acid Suppliers

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915140-06-6, 2-(Hydroxymethyl)isonicotinic acidRelated Search:


  • 4-PYRIDINECARBOXYLIC ACID, 2-(HYDROXYMETHYL)-
  • 2-Hydroxymethylisonicotinic acid
  • 2-(hydroxymethyl)-4-pyridinecarboxylic acid
  • 915140-06-6