ChemicalBook > CAS DataBase List > 7-broMoquinolin-5-ol
7-broMoquinolin-5-ol
- Product Name
- 7-broMoquinolin-5-ol
- CAS No.
- 1261677-80-8
- Chemical Name
- 7-broMoquinolin-5-ol
- Synonyms
- 7-broMoquinolin-5-ol;5-Quinolinol, 7-bromo-;7-Bromo-5-hydroxyquinoline
- CBNumber
- CB82553496
- Molecular Formula
- C9H6BrNO
- Formula Weight
- 224.05
- MOL File
- 1261677-80-8.mol
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7-broMoquinolin-5-ol Property
- storage temp.
- Sealed in dry,Store in freezer, under -20°C
- Appearance
- Light brown to brown Solid
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N-Bromosuccinimide Price
American Custom Chemicals Corporation
- Product number
- HCH0368283
- Product name
- 7-BROMOQUINOLIN-5-OL
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $903
- Updated
- 2021/12/16
Medical Isotopes, Inc.
- Product number
- 35902
- Product name
- 7-Bromoquinolin-5-ol
- Purity
- 95+%
- Packaging
- 1g
- Price
- $985
- Updated
- 2021/12/16
American Custom Chemicals Corporation
- Product number
- HCH0368283
- Product name
- 7-BROMOQUINOLIN-5-OL
- Purity
- 95.00%
- Packaging
- 2.5G
- Price
- $1275
- Updated
- 2021/12/16
AK Scientific
- Product number
- Z4051
- Product name
- 7-Bromoquinolin-5-ol
- Packaging
- 100mg
- Price
- $410
- Updated
- 2021/12/16
Crysdot
- Product number
- CD11309459
- Product name
- 7-Bromoquinolin-5-ol
- Purity
- 95+%
- Packaging
- 1g
- Price
- $460
- Updated
- 2021/12/16
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7-broMoquinolin-5-ol Chemical Properties,Usage,Production
Synthesis
1378860-76-4
1261677-80-8
Step 2: 1.5 g (0.0064 mol) of 7-bromo-5-methoxyquinoline was mixed with 48% hydrobromic acid (30 mL) and reacted at reflux for 20 hours. After completion of the reaction, it was cooled to room temperature and the reaction mixture was poured into 100 mL of water and the pH was adjusted to alkaline with saturated ammonia solution. The solid product was collected by filtration, washed with water and dried under vacuum at 50 °C to give 600 mg of 7-bromoquinolin-5-ol in 41% yield.1H-NMR (400 MHz, d6-DMSO): δ 7.48 (1H, m), 7.18 (1H, s) ppm.
References
[1] Patent: WO2013/14060, 2013, A1. Location in patent: Page/Page column 49
[2] Patent: US2013/29949, 2013, A1. Location in patent: Paragraph 0122; 0123
7-broMoquinolin-5-ol Preparation Products And Raw materials
Raw materials
Preparation Products
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