(5-iodo-2-Methylphenyl)Methanol
- Product Name
- (5-iodo-2-Methylphenyl)Methanol
- CAS No.
- 1260242-01-0
- Chemical Name
- (5-iodo-2-Methylphenyl)Methanol
- Synonyms
- 5-Iodo-2-methylbenzyl Alcohol;5-Iodo-2-methylbenzenemethanol;(5-iodo-2-Methylphenyl)Methanol;Benzenemethanol, 5-iodo-2-methyl-
- CBNumber
- CB82574257
- Molecular Formula
- C8H9IO
- Formula Weight
- 248.06
- MOL File
- 1260242-01-0.mol
(5-iodo-2-Methylphenyl)Methanol Property
- storage temp.
- 2-8°C(protect from light)
- Appearance
- Brown to reddish brown Solid
- InChI
- InChI=1S/C8H9IO/c1-6-2-3-8(9)4-7(6)5-10/h2-4,10H,5H2,1H3
- InChIKey
- CIEQOCDUTRABFK-UHFFFAOYSA-N
- SMILES
- C1(CO)=CC(I)=CC=C1C
Safety
- HS Code
- 2906290090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B449575
- Product name
- (5-iodo-2-methylphenyl)methanol
- Packaging
- 10mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- 1761DP
- Product name
- (5-Iodo-2-methylphenyl)methanol
- Packaging
- 5g
- Price
- $451
- Updated
- 2021/12/16
- Product number
- CM248556
- Product name
- (5-Iodo-2-methylphenyl)methanol
- Purity
- 95+%
- Packaging
- 10g
- Price
- $468
- Updated
- 2021/12/16
- Product number
- 1260242010
- Product name
- 5-Iodo-2-methylbenzylalcohol
- Packaging
- 250mg
- Price
- $489.6
- Updated
- 2021/12/16
- Product number
- CD12168059
- Product name
- (5-Iodo-2-methylphenyl)methanol
- Purity
- 97%
- Packaging
- 10g
- Price
- $495
- Updated
- 2021/12/16
(5-iodo-2-Methylphenyl)Methanol Chemical Properties,Usage,Production
Synthesis
612833-45-1
1260242-01-0
Step 3: Synthesis of (5-iodo-2-methylphenyl)methanol To a solution of THF (300 mL) containing ester 4 (41.0 g, 141 mmol) was slowly added lithium borohydride (2.0 M solution of THF, 212 mL). The reaction mixture was heated to reflux and stirred overnight. Upon completion of the reaction, the mixture was cooled to 0 °C and water was carefully added to quench the reaction, followed by the addition of saturated NH4Cl solution. The reaction mixture was diluted with water and extracted with EtOAc. The organic layers were combined, washed with brine, dried over anhydrous MgSO4, filtered and concentrated under reduced pressure to afford the title compound (5-iodo-2-methylphenyl)methanol (34.0 g, 97% yield) as a white solid, which could be used in the next reaction without further purification. [M-OH]+ m/z: 231.
References
[1] Patent: WO2011/159067, 2011, A2. Location in patent: Page/Page column 51
(5-iodo-2-Methylphenyl)Methanol Preparation Products And Raw materials
Raw materials
Preparation Products
(5-iodo-2-Methylphenyl)Methanol Suppliers
- Tel
- --
- Fax
- --
- info@synthonix.com
- Country
- United States
- ProdList
- 6872
- Advantage
- 58
- Tel
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- Fax
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- enquiries@acints.com
- Country
- United States
- ProdList
- 4893
- Advantage
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View Lastest Price from (5-iodo-2-Methylphenyl)Methanol manufacturers
- Product
- (5-iodo-2-Methylphenyl)Methanol 1260242-01-0
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-06-27