(4-Chloro-pyriMidin-2-yl)-diMethyl-aMine

Product Name: (4-Chloro-pyriMidin-2-yl)-diMethyl-aMine
CAS No.: 23631-02-9
Chemical Name: (4-Chloro-pyriMidin-2-yl)-diMethyl-aMine
Synonyms: 4-Chloro-2-(dimethylamino)pyrimidine;4-Chloro-N,N-diMethylpyriMidin-2-aMine;2-Pyrimidinamine, 4-chloro-N,N-dimethyl-;(4-Chloro-pyriMidin-2-yl)-diMethyl-aMine
CBNumber: CB82575254
Molecular Formula: C6H8ClN3
Formula Weight: 157.6
MOL File: 23631-02-9.mol

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(4-Chloro-pyriMidin-2-yl)-diMethyl-aMine Property

Boiling point:: 248.9±32.0 °C(Predicted)
Density: 1.252±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 3.83±0.10(Predicted)

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P310Immediately call a POISON CENTER or doctor/physician.

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N-Bromosuccinimide Price

TRC

Product number: C368955
Product name: 4-Chloro-N,N-dimethylpyrimidin-2-amine
Packaging: 10mg
Price: $45
Updated: 2021/12/16

AK Scientific

Product number: J96447
Product name: (4-Chloro-pyrimidin-2-yl)-dimethyl-amine
Packaging: 100mg
Price: $80
Updated: 2021/12/16

Medical Isotopes, Inc.

Product number: 34197
Product name: 4-chloro-N,N-dimethylpyrimidin-2-amine
Purity: 97%
Packaging: 1g
Price: $850
Updated: 2021/12/16

Ambeed

Product number: A273539
Product name: 4-Chloro-N,N-dimethylpyrimidin-2-amine
Purity: 97%
Packaging: 1g
Price: $292
Updated: 2021/12/16

Crysdot

Product number: CD11161139
Product name: 4-Chloro-N,N-dimethylpyrimidin-2-amine
Purity: 97%
Packaging: 1g
Price: $392
Updated: 2021/12/16

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(4-Chloro-pyriMidin-2-yl)-diMethyl-aMine Chemical Properties,Usage,Production

Synthesis

3934-20-1

74-89-5

31058-81-8

23631-02-9

Step B: Synthesis of 2-chloro-N,N-dimethylpyrimidin-4-amine. To a solution of 2,4-dichloropyrimidine (15.0 g, 10.15 mmol) in tetrahydrofuran (THF, 150 mL) was slowly added 50% aqueous methylamine (MeNH2) (22.7 g, 25.2 mmol). The reaction mixture was stirred at room temperature for 2 hours. After completion of the reaction, the reaction solution was poured into saturated aqueous sodium bicarbonate (NaHCO3) solution and the aqueous phase was extracted three times with chloroform (CHCl3). The organic layers were combined, dried with anhydrous magnesium sulfate (MgSO4), filtered and concentrated. The crude product was purified by fast chromatography (amino silica gel column, 20% ethyl acetate/hexane as eluent) to afford 2-chloro-N,N-dimethylpyrimidin-4-amine (8.66 g, 55% yield) and 4-chloro-N,N-dimethylpyrimidin-2-amine (0.87 g, 6% yield), both as white solids.

References

[1] Patent: EP1464335, 2004, A2. Location in patent: Page/Page column 172

(4-Chloro-pyriMidin-2-yl)-diMethyl-aMine Preparation Products And Raw materials

Raw materials

Preparation Products

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(4-Chloro-pyriMidin-2-yl)-diMethyl-aMine Suppliers

China 29 India 1 United States 3 Global 33

Shanghai Sunway Pharmaceutical Technology Co., Ltd

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SHANGHAI FDC-CHEMICAL CO.,LTD

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View Lastest Price from (4-Chloro-pyriMidin-2-yl)-diMethyl-aMine manufacturers

Nanjing jinheyou Trading Co., Ltd.

Product: (4-Chloro-pyriMidin-2-yl)-diMethyl-aMine 23631-02-9
Price: US $0.00/g
Min. Order: 1g
Purity: 95%min
Supply Ability: 20kg/month
Release date: 2019-12-19

23631-02-9, (4-Chloro-pyriMidin-2-yl)-diMethyl-aMineRelated Search:

(4-Chloro-pyriMidin-2-yl)-diMethyl-aMine

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2-Pyrimidinamine, 4-chloro-N,N-dimethyl-

4-Chloro-2-(dimethylamino)pyrimidine

23631-02-9