6-broMo-1,2,4-triazin-3-aMine
- Product Name
- 6-broMo-1,2,4-triazin-3-aMine
- CAS No.
- 69249-22-5
- Chemical Name
- 6-broMo-1,2,4-triazin-3-aMine
- Synonyms
- 3-AMino-6-broMo-1,2,4-triazine;INC280-3;3-Amino-6-bromo-1;Amino-6-bromo-1,2,4-triazine;broMo-1,2,4-triazin-3-a Mine;3-amine-6-bromo-1,2,4-triazin;6-broMo-1,2,4-triazin-3-aMine;3-Amine-6-bromo-1,2,4-triazine;6-BroMo-1,2,4-triazine-3-aMine;1,2,4-Triazin-3-amine, 6-bromo-
- CBNumber
- CB82599324
- Molecular Formula
- C3H3BrN4
- Formula Weight
- 174.99
- MOL File
- 69249-22-5.mol
6-broMo-1,2,4-triazin-3-aMine Property
- Boiling point:
- 373.6±34.0 °C(Predicted)
- Density
- 1.998±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- pka
- 2.02±0.63(Predicted)
- Appearance
- Light yellow to brown Solid
- InChI
- InChI=1S/C3H3BrN4/c4-2-1-6-3(5)8-7-2/h1H,(H2,5,6,8)
- InChIKey
- WIBIPFPOGMLYJQ-UHFFFAOYSA-N
- SMILES
- N1C(Br)=CN=C(N)N=1
Safety
- HS Code
- 2933698090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- OR930027
- Product name
- 6-Bromo-1,2,4-triazin-3-amine
- Purity
- 95%
- Packaging
- 1g
- Price
- $30
- Updated
- 2021/12/16
- Product number
- OR930027
- Product name
- 6-Bromo-1,2,4-triazin-3-amine
- Purity
- 95%
- Packaging
- 5g
- Price
- $89
- Updated
- 2021/12/16
- Product number
- 6428AJ
- Product name
- 6-Bromo-1,2,4-triazin-3-amine
- Packaging
- 1g
- Price
- $105
- Updated
- 2021/12/16
- Product number
- 3H30-9-0N
- Product name
- 6-Bromo-1,2,4-triazin-3-amine
- Purity
- 97%
- Packaging
- 1g
- Price
- $125
- Updated
- 2021/12/16
- Product number
- 3H30-9-0N
- Product name
- 6-Bromo-1,2,4-triazin-3-amine
- Purity
- 97%
- Packaging
- 5G
- Price
- $272
- Updated
- 2021/12/16
6-broMo-1,2,4-triazin-3-aMine Chemical Properties,Usage,Production
Flammability and Explosibility
Flammable
Synthesis
1120-99-6
69249-22-5
General procedure for the synthesis of 3-amino-6-bromo-1,2,4-triazine from 1,2,4-triazin-3-amine: 3-amino-1,2,4-triazine (I) (0.96 g, 10 mmol) was dissolved in 100 mL of N,N-dimethylformamide (DMF) with thorough stirring. A 100 mL DMF solution of N-bromosuccinimide (NBS) (17.8 g, 100 mmol) was added slowly and dropwise under the cooling of an ice bath. The reaction temperature was maintained between 0-30 °C with continuous stirring for 12 hours. After completion of the reaction, sodium hydroxide (12 g, 300 mmol) was added to the reaction mixture for neutralization. The precipitate was collected by filtration and dried to afford the target product 3-amino-6-bromo-1,2,4-triazine (1.43 g, 81.7% yield).
References
[1] Patent: CN108129409, 2018, A. Location in patent: Paragraph 0043; 0044; 0045
[2] Journal of the American Chemical Society, 2015, vol. 137, # 26, p. 8388 - 8391
[3] Patent: US2016/251361, 2016, A1. Location in patent: Paragraph 1004-1006
[4] Russian Chemical Bulletin, 2014, vol. 63, # 6, p. 1359 - 1363
[5] Izv. Akad. Nauk, Ser. Khim., 2014, # 6, p. 1359 - 1363,5
6-broMo-1,2,4-triazin-3-aMine Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 6-broMo-1,2,4-triazin-3-aMine manufacturers
- Product
- 6-broMo-1,2,4-triazin-3-aMine 69249-22-5
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 1Ton
- Release date
- 2022-10-08
- Product
- 6-Bromo-1,2,4-triazin-3-amine 69249-22-5
- Price
- US $0.00-0.00/kg
- Min. Order
- 1kg
- Purity
- 98%
- Supply Ability
- 1 ton
- Release date
- 2023-12-21
- Product
- 6-broMo-1,2,4-triazin-3-aMine 69249-22-5
- Price
- US $5.00-0.10/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2024-04-09