ChemicalBook > CAS DataBase List > 3-(Boc-aMino)-3-Methylpyrrolidine

3-(Boc-aMino)-3-Methylpyrrolidine

Product Name: 3-(Boc-aMino)-3-Methylpyrrolidine
CAS No.: 147459-52-7
Chemical Name: 3-(Boc-aMino)-3-Methylpyrrolidine
Synonyms: 3-(Boc-aMino)-3-Methylpyr...;3-(Boc-aMino)-3-Methylpyrrolidine;tert-Butyl (3-Methylpyrrolidin-3-yl)carbaMate;tert-butyl N-(3-methylpyrrolidin-3-yl)carbamate;(3-Methyl-pyrrolidin-3-yl)-carbamic acid tert-butyl ester;Carbamic acid, (3-methyl-3-pyrrolidinyl)-, 1,1-dimethylethyl ester;Carbamic acid, N-(3-methyl-3-pyrrolidinyl)-, 1,1-dimethylethyl ester
CBNumber: CB82615189
Molecular Formula: C10H20N2O2
Formula Weight: 200.28
MOL File: 147459-52-7.mol

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3-(Boc-aMino)-3-Methylpyrrolidine Property

Boiling point:: 289.8±29.0 °C(Predicted)
Density: 1.02±0.1 g/cm3(Predicted)
storage temp.: 2-8°C(protect from light)
pka: 12.58±0.20(Predicted)
Appearance: White to off-white Solid
InChI: InChI=1S/C10H20N2O2/c1-9(2,3)14-8(13)12-10(4)5-6-11-7-10/h11H,5-7H2,1-4H3,(H,12,13)
InChIKey: DIQWSFWWYVRXRO-UHFFFAOYSA-N
SMILES: C(OC(C)(C)C)(=O)NC1(C)CCNC1

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

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N-Bromosuccinimide Price

American Custom Chemicals Corporation

Product number: CHM0382147
Product name: 3-(BOC-AMINO)-3-METHYLPYRROLIDINE
Purity: 95.00%
Packaging: 5MG
Price: $501.72
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H56-1-166
Product name: 3-(Boc-amino)-3-methylpyrrolidine
Packaging: 1g
Price: $925
Updated: 2021/12/16

Matrix Scientific

Product number: 112346
Product name: 3-(Boc-amino)-3-methylpyrrolidine
Packaging: 1g
Price: $1683
Updated: 2021/12/16

J&W Pharmlab

Product number: 75R0509
Product name: (3-Methyl-pyrrolidin-3-yl)-carbamicacidtert-butylester
Purity: 97%
Packaging: 50mg
Price: $117
Updated: 2021/12/16

J&W Pharmlab

Product number: 75R0509
Product name: (3-Methyl-pyrrolidin-3-yl)-carbamicacidtert-butylester
Purity: 97%
Packaging: 100mg
Price: $137
Updated: 2021/12/16

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3-(Boc-aMino)-3-Methylpyrrolidine Chemical Properties,Usage,Production

Synthesis

927389-50-2

147459-52-7

Step E: A solution of benzyl 3-(tert-butoxycarbonylamino)-3-methylpyrrolidine-1-carboxylate (2.00 g, 5.98 mmol) and 10% Pd/C (0.32 g, 0.30 mmol) in methanol (20 mL) was reacted under stirring conditions for 1 hour in a hydrogen atmosphere. Upon completion of the reaction, the catalyst was removed by filtration and washed with methanol. The filtrate was concentrated to afford tert-butyl (3-methylpyrrolidin-3-yl)carbamate (1.15 g, 96% yield) in solid form.

References

[1] Patent: WO2009/140320, 2009, A1. Location in patent: Page/Page column 74-75

3-(Boc-aMino)-3-Methylpyrrolidine Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3-(Boc-aMino)-3-Methylpyrrolidine manufacturers

Career Henan Chemical Co

Product: 3-(Boc-aMino)-3-Methylpyrrolidine 147459-52-7
Price: US $6.60/KG
Min. Order: 1KG
Purity: 97%-99%
Supply Ability: 1kg-1000kg
Release date: 2019-12-26

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147459-52-7