ChemicalBook > CAS DataBase List > 5-BroMo-6-hydroxypicolinic acid
5-BroMo-6-hydroxypicolinic acid
- Product Name
- 5-BroMo-6-hydroxypicolinic acid
- CAS No.
- 1214385-51-9
- Chemical Name
- 5-BroMo-6-hydroxypicolinic acid
- Synonyms
- 5-BroMo-6-hydroxypicolinic acid;5-bromo-6-hydroxypyridine-2-carboxylic acid;5-bromo-6-oxo-1H-pyridine-2-carboxylic acid;5-bromo-6-oxo-1,6-dihydropyridine-2-carboxylic acid;2-Pyridinecarboxylic acid, 5-bromo-1,6-dihydro-6-oxo-
- CBNumber
- CB82619950
- Molecular Formula
- C6H4BrNO3
- Formula Weight
- 218
- MOL File
- 1214385-51-9.mol
More
Less
5-BroMo-6-hydroxypicolinic acid Property
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- Appearance
- White to off-white Solid
More
Less
N-Bromosuccinimide Price
TRC
- Product number
- B997868
- Product name
- 5-Bromo-6-hydroxypicolinicAcid
- Packaging
- 100mg
- Price
- $65
- Updated
- 2021/12/16
Matrix Scientific
- Product number
- 119772
- Product name
- 5-Bromo-6-hydroxypicolinic acid
- Purity
- 95+%
- Packaging
- 1g
- Price
- $810
- Updated
- 2021/12/16
Matrix Scientific
- Product number
- 119772
- Product name
- 5-Bromo-6-hydroxypicolinic acid
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $324
- Updated
- 2021/12/16
American Custom Chemicals Corporation
- Product number
- HCH0367047
- Product name
- 5-BROMO-6-HYDROXYPICOLINIC ACID
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $502.17
- Updated
- 2021/12/16
AK Scientific
- Product number
- X9492
- Product name
- 5-Bromo-6-hydroxypicolinicacid
- Packaging
- 10g
- Price
- $1399
- Updated
- 2021/12/16
More
Less
5-BroMo-6-hydroxypicolinic acid Chemical Properties,Usage,Production
Synthesis
19621-92-2
1214385-51-9
General procedure for the synthesis of 5-bromo-6-hydroxypyridinecarboxylic acid from 6-hydroxypyridine-2-carboxylic acid: bromine (115 g, 720 mmol) was added dropwise to a suspension of 6-oxo-1,6-dihydropyridine-2-carboxylic acid (25 g, 180 mmol) in acetic acid (400 mL). The reaction mixture was heated to 80 °C and kept for 16 hours. Upon completion of the reaction, the mixture was concentrated to dryness under reduced pressure. The residue was ground with tert-butyl methyl ether (200 mL) and subsequently filtered. The filter cake was washed with tert-butyl methyl ether (3 x 100 mL) to give a gray solid product. Yield: 39.0 g, 179 mmol, 99% yield. The product was characterized by 1H NMR (400 MHz, DMSO-d6): δ 8.03 (d, J = 7.3 Hz, 1H), 6.83 (d, J = 7.3 Hz, 1H).
References
[1] Patent: US2016/222007, 2016, A1. Location in patent: Paragraph 0354; 0355
5-BroMo-6-hydroxypicolinic acid Preparation Products And Raw materials
Raw materials
Preparation Products
More
Less
5-BroMo-6-hydroxypicolinic acid Suppliers
- Tel
- 025-86918202 4000255188
- Fax
- 86-025-86918232
- sales@pharmablock.com
- Country
- China
- ProdList
- 5000
- Advantage
- 55
- Tel
- 400-6009262 16621234537
- Fax
- 021-64823266
- chenyj@titansci.com
- Country
- China
- ProdList
- 14101
- Advantage
- 59
- Tel
- 4009903999 13355009207
- Fax
- 0539-6365991
- 3007715519@qq.com
- Country
- China
- ProdList
- 18729
- Advantage
- 57
- Tel
- 13761627472
- Fax
- 86-21-64965863
- 183009664@qq.com
- Country
- China
- ProdList
- 649
- Advantage
- 62
- Tel
- 400-164-7117 13681763483
- Fax
- +86-21-61629029
- product02@bidepharm.com
- Country
- China
- ProdList
- 39966
- Advantage
- 60
- Tel
- 微信 17321281695 18019252918
- Fax
- 17321281695
- sale@amkchem.com
- Country
- China
- ProdList
- 15136
- Advantage
- 55
- Tel
- 02161555100
- Fax
- -
- Country
- China
- ProdList
- 820
- Advantage
- 58
- Tel
- 021-34979681; 17701870669
- Fax
- 021-34979681
- 41513101@qq.com
- Country
- China
- ProdList
- 1785
- Advantage
- 55
- Tel
- 13162380607
- Fax
- QQ:1696175688
- 1696175688@qq.com
- Country
- China
- ProdList
- 817
- Advantage
- 55
- Tel
- 0573-11111111-1111 18969316891
- Fax
- -
- richmol@163.com
- Country
- China
- ProdList
- 449
- Advantage
- 50
More
Less
View Lastest Price from 5-BroMo-6-hydroxypicolinic acid manufacturers
Hong Kong Tiansheng New Material Trading Co., Ltd
- Product
- 5-Bromo-6-hydroxypicolinic acid 1214385-51-9
- Price
- US $100.00/Kg/Bag
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 10kg
- Release date
- 2021-09-14
Hong Kong Tiansheng New Material Trading Co., Ltd
- Product
- 5-Bromo-6-hydroxypicolinic acid 1214385-51-9
- Price
- US $100.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 100KG
- Release date
- 2021-09-15
Hong Kong Tiansheng New Material Trading Co., Ltd
- Product
- 5-Bromo-6-hydroxypicolinic acid 1214385-51-9
- Price
- US $100.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 10KG
- Release date
- 2021-09-17