1H-Indole, 6-broMo-2-Methyl-

Product Name: 1H-Indole, 6-broMo-2-Methyl-
CAS No.: 6127-19-1
Chemical Name: 1H-Indole, 6-broMo-2-Methyl-
Synonyms: NSC 115145;6-BroMo-2-Methylindole;1H-Indole, 6-broMo-2-Methyl-
CBNumber: CB82638883
Molecular Formula: C9H8BrN
Formula Weight: 210.07
MOL File: 6127-19-1.mol

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1H-Indole, 6-broMo-2-Methyl- Property

Melting point:: 134.5-135.5℃
Boiling point:: 325.1±22.0 °C(Predicted)
Density: 1.563±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 16?+-.0.30(Predicted)
Appearance: White to off-white Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B405243
Product name: 6-Bromo-2-methyl-1H-indole
Packaging: 50mg
Price: $45
Updated: 2021/12/16

Matrix Scientific

Product number: 119526
Product name: 6-Bromo-2-methyl-1H-indole
Purity: 95+%
Packaging: 1g
Price: $335
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0352522
Product name: 6-BROMO-2-METHYL-1H-INDOLE
Purity: 95.00%
Packaging: 5MG
Price: $504.94
Updated: 2021/12/16

Medical Isotopes, Inc.

Product number: 35259
Product name: 6-Bromo-2-methyl-1H-indole
Purity: 95+%
Packaging: 1000mg
Price: $620
Updated: 2021/12/16

AK Scientific

Product number: Z4943
Product name: 6-Bromo-2-methylindole
Packaging: 10g
Price: $942
Updated: 2021/12/16

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1H-Indole, 6-broMo-2-Methyl- Chemical Properties,Usage,Production

Synthesis

67-64-1

591-19-5

6127-19-1

General procedure for the synthesis of 6-bromo-2-methyl-1H-indole (CXXXIII): 3-bromoaniline (4 g, 0.041 mmol), copper(II) acetate monohydrate (14.0 g, 0.129 mmol), palladium(II) acetate (0.1 g, 0.000801 mmol), and acetone (100 mL) were combined in a dimethyl sulfoxide (50 mL) The solution was heated at 90 °C for 24 hours. After completion of the reaction, the reaction mixture was poured into cold water and extracted with ethyl acetate (2 x 250 mL). The organic layers were combined, washed sequentially with water and brine, and then dried over anhydrous sodium sulfate. The organic layer was concentrated under reduced pressure to give the crude product. The crude product was purified by silica gel column chromatography (100-200 mesh) to afford the target compound CXXXIII (1.3 mg, 27% yield) using hexane solution of 5% ethyl acetate as eluent. The product characterization data were as follows: 1H NMR (400 MHz, CDCl3): δ 7.83 (brs, 1H), 7.40 (s, 1H), 7.34 (d, J=8.3 Hz, 1H), 7.14 (dd, J=8.5,1.7 Hz, 1H), 6.17 (s, 1H), 2.41 (s, 3H); MS (ESI, positive mode) m/z 208/210 (MH+, 79/81Br).

References

[1] Patent: WO2015/73528, 2015, A1. Location in patent: Page/Page column 197

1H-Indole, 6-broMo-2-Methyl- Preparation Products And Raw materials

Raw materials

Preparation Products

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1H-Indole, 6-broMo-2-Methyl- Suppliers

China 83 India 1 United Kingdom 1 United States 5 Global 90

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View Lastest Price from 1H-Indole, 6-broMo-2-Methyl- manufacturers

Career Henan Chemical Co

Product: 6-Bromo-2-methyl-1H-indole 6127-19-1
Price: US $1.00/g
Min. Order: 1g
Purity: 99%
Supply Ability: 1ton
Release date: 2020-01-10

Career Henan Chemical Co

Product: 6-Bromo-2-methyl-1H-indole 6127-19-1
Price: US $1.00/g
Min. Order: 1g
Purity: 95-99%
Supply Ability: 1ton
Release date: 2020-01-09

6127-19-1, 1H-Indole, 6-broMo-2-Methyl-Related Search:

6-Bromo-3-methoxy-2-nitro-pyridine Dibenzofuran, 6-bromo-2-chloro- ethyl 6-bromo-2-methylpyridine-3-carboxylate

1H-Indole, 6-broMo-2-Methyl-

6-BroMo-2-Methylindole

NSC 115145

6127-19-1