(R)-1-(3-Bromophenyl)ethylamine
- Product Name
- (R)-1-(3-Bromophenyl)ethylamine
- CAS No.
- 176707-77-0
- Chemical Name
- (R)-1-(3-Bromophenyl)ethylamine
- Synonyms
- (R)-1-(3-BROMOPHENYL)ETHANAMINE;(R)-1-(3-bromophenyl)ethan-1-amine;Albb-005066;?-1-(3-Bromophenyl)ethanamine;(R)-3-Bromo-α-methylbenzylamine;(R)-1-(3-BROMOPHENYL)ETHYLAMINE;[(1R)-1-(3-Bromophenyl)ethyl]amine;(R)-(+)-3-BROMO A-METHYLBENZYLAMINE;(R)-3-BROMO-ALPHA-METHYLBENZYLAMINE;(1R)-1-(3-bromophenyl)ethan-1-amine
- CBNumber
- CB8302375
- Molecular Formula
- C8H10BrN
- Formula Weight
- 200.08
- MOL File
- 176707-77-0.mol
(R)-1-(3-Bromophenyl)ethylamine Property
- Boiling point:
- 96°C/4mm
- Density
- 1.33
- Flash point:
- 96°C/4mm
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- pka
- 8.73±0.10(Predicted)
- Appearance
- Colorless to light yellow Liquid
- optical activity
- Consistent with structure
- Sensitive
- Air Sensitive
Safety
- Hazard Codes
- C,N
- Risk Statements
- 34-51/53-43-22
- Safety Statements
- 26-36/37/39-61-45
- RIDADR
- 2735
- HazardClass
- 8
- PackingGroup
- III
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H302Harmful if swallowed
H314Causes severe skin burns and eye damage
H317May cause an allergic skin reaction
H318Causes serious eye damage
H411Toxic to aquatic life with long lasting effects
- Precautionary statements
-
P273Avoid release to the environment.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P310Immediately call a POISON CENTER or doctor/physician.
N-Bromosuccinimide Price
- Product number
- FB116420
- Product name
- 1-(3-Bromophenyl)ethanamine
- Packaging
- 2g
- Price
- $434
- Updated
- 2021/12/16
- Product number
- 167633
- Product name
- (R)-1-(3-Bromophenyl)ethanamine
- Packaging
- 5g
- Price
- $497
- Updated
- 2021/12/16
- Product number
- 167633
- Product name
- (R)-1-(3-Bromophenyl)ethanamine
- Packaging
- 10g
- Price
- $809
- Updated
- 2021/12/16
- Product number
- FB116420
- Product name
- 1-(3-Bromophenyl)ethanamine
- Packaging
- 5G
- Price
- $868
- Updated
- 2021/12/16
- Product number
- HCH0029337
- Product name
- BENZENEMETHANAMINE, 3-BROMO-.ALPHA.-METHYL-, (.ALPHA.R)-
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $983.52
- Updated
- 2021/12/16
(R)-1-(3-Bromophenyl)ethylamine Chemical Properties,Usage,Production
Synthesis
24280-05-5
176707-77-0
The general procedure for the synthesis of (R)-1-(3-bromophenyl)ethylamine from 1-(3-bromophenyl)ethanone oxime is as follows: 1 equiv. of N-[1-(3-bromophenyl)ethylidene]hydroxylamine, 5 mol% of RuCl(Cymene)(S-tol-Binap)Cl catalyst, 5 equiv. of additives, and 70 vol. of methanol (relative to the amount of the oxime) are added to a glass vial. The glass vials were placed in a parallel autoclave, which was pressurized to 30 bar with hydrogen, then heated to 90 °C and kept for 24 hours. After completion of the reaction, the system was cooled to 20 °C. The reaction mixture was diluted with isopropyl alcohol. The reaction mixture was diluted with isopropanol and analyzed by chiral HPLC.
References
[1] Patent: WO2015/178847, 2015, A1. Location in patent: Page/Page column 7-8
(R)-1-(3-Bromophenyl)ethylamine Preparation Products And Raw materials
Raw materials
Preparation Products
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