ChemicalBook > CAS DataBase List > 3,5-dibromosulfanilamide

3,5-dibromosulfanilamide

Product Name
3,5-dibromosulfanilamide
CAS No.
39150-45-3
Chemical Name
3,5-dibromosulfanilamide
Synonyms
dibromosulfanilamide;2,6-dibromosulfanilamide;3,5-DIBROMOSULFANILAMIDE;3,5-DIBROMOSULPHANILAMIDE;3,5-Dibromosulfanilamide >3,5-DIBROMOSULFANILAMIDE 97+%;3,5-DIBROMOSULPHANILAMIDE 80%;3,5-DIBROMOSULFANILAMIDE: TECH., 80%;3,5-Dibromo-4-aminobenzenesulfonamide;4-Amino-3,5-dibromobenzenesulfonamide
CBNumber
CB8318794
Molecular Formula
C6H6Br2N2O2S
Formula Weight
330
MOL File
39150-45-3.mol
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3,5-dibromosulfanilamide Property

Melting point:
235-237°C
Boiling point:
458.2±55.0 °C(Predicted)
Density 
2.156±0.06 g/cm3(Predicted)
storage temp. 
Keep in dark place,Inert atmosphere,Room temperature
form 
powder to crystal
pka
9.57±0.60(Predicted)
color 
White to Light yellow to Light orange
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Safety

Risk Statements 
36/37/38
Safety Statements 
26-36
HS Code 
2935.90.9500
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P405Store locked up.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
S659525
Product name
3,5-DIBROMOSULFANILAMIDE
Purity
Aldrich
Packaging
250mg
Price
$29.8
Updated
2024/03/01
TCI Chemical
Product number
D0212
Product name
3,5-Dibromosulfanilamide
Purity
>97.0%(T)
Packaging
25g
Price
$280
Updated
2024/03/01
TRC
Product number
A576783
Product name
4-Amino-3,5-dibromobenzenesulfonamide
Packaging
2.5g
Price
$130
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD11829
Product name
3,5-Dibromosulphanilamide
Packaging
500mg
Price
$75
Updated
2021/12/16
Biosynth Carbosynth
Product number
FD11829
Product name
3,5-Dibromosulphanilamide
Packaging
1g
Price
$128
Updated
2021/12/16
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3,5-dibromosulfanilamide Chemical Properties,Usage,Production

Synthesis

Fifty grams (0.29 mole) of sulfanilamide is dissolved in a mixture of 850 ml. of water and 100 ml. (0.68 mole) of 40% hydrobromic acid. The solution is heated as above but to 70–75° and 65 g. (59 ml., 0.58 mole) of 30% hydrogen peroxide is added. A precipitate settles in 2–3 minutes, and the solution becomes yellow. The heat of the reaction causes the internal temperature to rise without further application of heat to a maximum of 85–90℃ after 10 minutes; by the end of the reaction time, the temperature will have fallen to about 70℃. After a total reaction time of 30 minutes, when the mixture has become almost solid and is very difficult to stir, the material is filtered hot. The yield of 3,5-dibromosulfanilamide is 85–90 g (90–94%), and the crude tan product melts over a range of 1–2° in the region 230–237℃.

3,5-dibromosulfanilamide Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3,5-dibromosulfanilamide manufacturers

Career Henan Chemical Co
Product
4-Amino-3,5-dibromobenzenesulfonamide 39150-45-3
Price
US $1.00/g
Min. Order
1g
Purity
99%
Supply Ability
1ton
Release date
2020-01-10

39150-45-3, 3,5-dibromosulfanilamideRelated Search:


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