ChemicalBook > CAS DataBase List > 2-BROMO-5-NITROETHOXYBENZENE

2-BROMO-5-NITROETHOXYBENZENE

Product Name: 2-BROMO-5-NITROETHOXYBENZENE
CAS No.: 423165-33-7
Chemical Name: 2-BROMO-5-NITROETHOXYBENZENE
Synonyms: 2-BROMO-5-NITROPHENETOLE;2-BROMO-5-NITROETHOXYBENZENE;2-Bromo-4-nitrophenetole, 99%;1-BROMO-2-ETHOXY-4-NITROBENZENE;2-Bromo-5-nitrophenylethylether;1-broMo-4-(2-nitroethoxy)benzene;Benzene, 1-bromo-2-ethoxy-4-nitro-
CBNumber: CB8370408
Molecular Formula: C8H8BrNO3
Formula Weight: 246.06
MOL File: 423165-33-7.mol

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2-BROMO-5-NITROETHOXYBENZENE Property

Melting point:: 54-56°C
Boiling point:: 315℃
Density: 1.557
Flash point:: 144℃
storage temp.: 2-8°C
Appearance: Brown to khaki Solid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H301Toxic if swalloed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

TRC

Product number: B699778
Product name: 1-Bromo-2-ethoxy-4-nitrobenzene
Packaging: 500mg
Price: $75
Updated: 2021/12/16

Matrix Scientific

Product number: 071925
Product name: 2-Bromo-5-nitroethoxybenzene
Purity: 95+%
Packaging: 1g
Price: $116
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB64628
Product name: 2-Bromo-5-nitrophenetole
Packaging: 100g
Price: $160
Updated: 2021/12/16

Matrix Scientific

Product number: 071925
Product name: 2-Bromo-5-nitroethoxybenzene
Purity: 95+%
Packaging: 5g
Price: $301
Updated: 2021/12/16

AK Scientific

Product number: W6217
Product name: 2-Bromo-5-nitroethoxybenzene
Packaging: 100g
Price: $266
Updated: 2021/12/16

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2-BROMO-5-NITROETHOXYBENZENE Chemical Properties,Usage,Production

Synthesis

52427-05-1

75-03-6

423165-33-7

Ethyl iodide (1.79 g, 11.5 mmol) was added to an N,N-dimethylformamide (DMF, 10 mL) mixture of 2-bromo-5-nitrophenol (1.0 g, 4.59 mmol) and potassium carbonate (1.59 g, 11.5 mmol). The reaction mixture was stirred at 70 °C for 4 h and subsequently cooled to room temperature. The reaction mixture was diluted with water (100 mL) and extracted with ethyl acetate (EtOAc, 2 x 75 mL). The organic phases were combined, washed sequentially with water and saturated saline, dried over anhydrous sodium sulfate and concentrated to afford the target product 2-bromo-5-nitrophenylethyl ether (1.10 g, 4.18 mmol, 91% yield). Mass spectrum (ESI) m/z: 248.0 ([M + H]+). 1H NMR (300 MHz, DMSO-d6) δ (ppm): 7.90 (d, J = 8.6 Hz, 1H), 7.81 (d, J = 2.5 Hz, 1H), 7.78-7.73 (m, 1H), 4.27 (q, J = 7.0 Hz, 2H), 1.40 (t, J = 7.0 Hz, 3H).

References

[1] Patent: WO2016/144936, 2016, A1. Location in patent: Page/Page column 111

2-BROMO-5-NITROETHOXYBENZENE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-BROMO-5-NITROETHOXYBENZENE manufacturers

Career Henan Chemical Co

Product: 2-BROMO-5-NITROETHOXYBENZENE 423165-33-7
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100kg
Release date: 2019-12-19

423165-33-7, 2-BROMO-5-NITROETHOXYBENZENERelated Search:

4-NITROPHENETOLE Nitrobenzene Phenetole 4-BROMO-3-METHOXYANILINE 2-Bromo-4-nitrophenol 2-BROMO-5-NITROETHOXYBENZENE 2-BROMO-5-NITROANISOLE 5-amino-2-bromophenol

2-BROMO-5-NITROETHOXYBENZENE

2-BROMO-5-NITROPHENETOLE

1-BROMO-2-ETHOXY-4-NITROBENZENE

2-Bromo-4-nitrophenetole, 99%

2-Bromo-5-nitrophenylethylether

1-broMo-4-(2-nitroethoxy)benzene

Benzene, 1-bromo-2-ethoxy-4-nitro-

423165-33-7

Phenetole

Anisoles, Alkyloxy Compounds & Phenylacetates

Bromine Compounds

Nitro Compounds