1-ETHYL-4-IODOBENZENE
- Product Name
- 1-ETHYL-4-IODOBENZENE
- CAS No.
- 25309-64-2
- Chemical Name
- 1-ETHYL-4-IODOBENZENE
- Synonyms
- p-Iodoethylbenzene;4-Iodoethylbenzene;P-ETHYLIODOBENZENE;4-ETHYLIODOBENZENE;1-ETHYL-4-IODOBENZENE;4-Iodo-1-ethylbenzene;1-Ethyl-4-iodobenzene,99%; Benzene, 1-ethyl-4-iodo-
- CBNumber
- CB8396961
- Molecular Formula
- C8H9I
- Formula Weight
- 232.06
- MOL File
- 25309-64-2.mol
1-ETHYL-4-IODOBENZENE Property
- Melting point:
- -17 °C
- Boiling point:
- 112-113 °C (20 mmHg)
- Density
- 1,6 g/cm3
- refractive index
- 1.5905-1.5925
- Flash point:
- 107 °C
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- form
- liquid
- Specific Gravity
- 1.6
- color
- Yellow
- Sensitive
- Light Sensitive
- BRN
- 2076973
- CAS DataBase Reference
- 25309-64-2(CAS DataBase Reference)
Safety
- Hazard Codes
- Xi,C
- Risk Statements
- 36/38-36
- Safety Statements
- 37/39-26-36
- HS Code
- 29036990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
N-Bromosuccinimide Price
- Product number
- E678943
- Product name
- 1-Ethyl-4-iodobenzene
- Packaging
- 500mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- J56931
- Product name
- 1-Ethyl-4-iodobenzene
- Packaging
- 1g
- Price
- $14
- Updated
- 2021/12/16
- Product number
- 006113
- Product name
- 4-Ethyliodobenzene
- Packaging
- 5g
- Price
- $30
- Updated
- 2021/12/16
- Product number
- 2029AB
- Product name
- 1-Ethyl-4-iodobenzene
- Packaging
- 5g
- Price
- $37
- Updated
- 2021/12/16
- Product number
- 006113
- Product name
- 4-Ethyliodobenzene
- Packaging
- 25g
- Price
- $90
- Updated
- 2021/12/16
1-ETHYL-4-IODOBENZENE Chemical Properties,Usage,Production
Chemical Properties
clear colorless to yellow liquid
Synthesis
100-41-4
25309-64-2
GENERAL STEPS: To a solution of 1,2-dimethylbenzene (0.106 g, 1 mmol) in acetonitrile (10 mL) was sequentially added iodine (1 mmol, 0.126 g) and polymer-loaded periodate (0.6 g, 1.05 mmol). The reaction mixture was stirred at 40 °C for 1 hour. The progress of the reaction was monitored by thin layer chromatography (TLC) and the unfolding agent was a solvent mixture of ethyl acetate and hexane (1:9, v/v). After completion of the reaction, the mixture was cooled to room temperature and filtered. Excess iodine in the filtrate was quenched by adding sodium bisulfite solution (1 M) dropwise. The organic layer was separated, dried with anhydrous magnesium sulfate, filtered and concentrated under reduced pressure to remove the solvent. The crude product was purified by silica gel column chromatography, eluting with a mixed solvent gradient of hexane and ethyl acetate to give 1-ethyl-4-iodobenzene in 95% isolated yield with a boiling point of 235 °C (literature value: 234 °C).
References
[1] Bulletin of the Chemical Society of Ethiopia, 2014, vol. 28, # 2, p. 305 - 308
[2] Journal of applied chemistry of the USSR, 1984, vol. 57, # 1 pt 2, p. 121 - 123
[3] Journal fuer Praktische Chemie (Leipzig), 1902, vol. <2> 65, p. 568
[4] Journal of the Indian Chemical Society, 1936, vol. 13, p. 187
[5] Journal of the Indian Chemical Society, 1937, vol. 14, p. 157
1-ETHYL-4-IODOBENZENE Preparation Products And Raw materials
Raw materials
Preparation Products
1-ETHYL-4-IODOBENZENE Suppliers
- Tel
- --
- Fax
- --
- chemcontrol@nextra.sk
- Country
- Slovakia
- ProdList
- 6700
- Advantage
- 60
View Lastest Price from 1-ETHYL-4-IODOBENZENE manufacturers
- Product
- 1-Ethyl-4-iodobenzene 25309-64-2
- Price
- US $5.00-0.50/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2024-01-13
- Product
- Benzene, 1-ethyl-4-iodo- 25309-64-2
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 200KG
- Release date
- 2020-01-09