4-BROMO-2-(N-MORPHOLINO)-BENZALDEHYDE

Product Name: 4-BROMO-2-(N-MORPHOLINO)-BENZALDEHYDE
CAS No.: 736990-80-0
Chemical Name: 4-BROMO-2-(N-MORPHOLINO)-BENZALDEHYDE
Synonyms: 4-BroMo-2-Morpholinobenzaldehyde;4-BROMO-2-(N-MORPHOLINO)-BENZALDEHYDE;4-bromo-2-(4-morpholinyl)benzaldehyde;4-broMo-2-(Morpholin-4-yl)benzaldehyde;Benzaldehyde, 4-bromo-2-(4-morpholinyl)-
CBNumber: CB8475220
Molecular Formula: C11H12BrNO2
Formula Weight: 270.12
MOL File: 736990-80-0.mol

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4-BROMO-2-(N-MORPHOLINO)-BENZALDEHYDE Property

storage temp.: under inert gas (nitrogen or Argon) at 2-8°C

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Matrix Scientific

Product number: 016626
Product name: 4-Bromo-2-(N-morpholino)-benzaldehyde
Purity: 98%
Packaging: 500mg
Price: $38
Updated: 2021/12/16

Matrix Scientific

Product number: 016626
Product name: 4-Bromo-2-(N-morpholino)-benzaldehyde
Purity: 98%
Packaging: 1g
Price: $59
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB140597
Product name: 4-Bromo-2-morpholinobenzaldehyde
Packaging: 500mg
Price: $60
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB140597
Product name: 4-Bromo-2-morpholinobenzaldehyde
Packaging: 1g
Price: $101
Updated: 2021/12/16

AK Scientific

Product number: W8174
Product name: 4-Bromo-2-(N-morpholino)benzaldehyde
Packaging: 1g
Price: $129
Updated: 2021/12/16

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4-BROMO-2-(N-MORPHOLINO)-BENZALDEHYDE Chemical Properties,Usage,Production

Synthesis

110-91-8

57848-46-1

736990-80-0

General procedure for the synthesis of 4-bromo-2-(N-morpholinyl)benzaldehyde from 4-bromo-2-fluorobenzaldehyde and morpholine: To a solution of 4-bromo-2-fluorobenzaldehyde (1.0 eq.) and K2CO3 (1.15 eq.) in DMF (1.0 M) was added morpholine (1.15 eq.). The reaction mixture was heated to reflux and maintained for 2 hours until TLC monitoring showed complete conversion of the feedstock to the target product. Upon completion of the reaction, the mixture was cooled to room temperature and allowed to stand overnight. The following day, the reaction mixture was diluted with EtOAc and water with vigorous stirring. The organic layer was separated, washed sequentially with water and brine, dried over anhydrous MgSO4 and filtered, and the filtrate was concentrated under reduced pressure. The residue was purified by fast column chromatography (eluent: 0-50% EtOAc/heptane gradient) to afford the target compound 4-bromo-2-(N-morpholino)benzaldehyde as a light yellow solid in 90% isolated yield.LCMS analysis showed [M+H]+ m/z = 271.8 and retention time (Rt) = 1.33 min.

References

[1] Patent: WO2017/103824, 2017, A1. Location in patent: Paragraph 00222; 00223
[2] Chemical Communications, 2010, vol. 46, # 35, p. 6593 - 6595

4-BROMO-2-(N-MORPHOLINO)-BENZALDEHYDE Preparation Products And Raw materials

Raw materials

Preparation Products

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4-BROMO-2-(N-MORPHOLINO)-BENZALDEHYDE Suppliers

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736990-80-0, 4-BROMO-2-(N-MORPHOLINO)-BENZALDEHYDERelated Search:

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4-BROMO-2-(N-MORPHOLINO)-BENZALDEHYDE

4-BroMo-2-Morpholinobenzaldehyde

4-broMo-2-(Morpholin-4-yl)benzaldehyde

4-bromo-2-(4-morpholinyl)benzaldehyde

Benzaldehyde, 4-bromo-2-(4-morpholinyl)-

736990-80-0