3-METHYL-4-NITROBENZALDEHYDE

Product Name: 3-METHYL-4-NITROBENZALDEHYDE
CAS No.: 18515-67-8
Chemical Name: 3-METHYL-4-NITROBENZALDEHYDE
Synonyms: 3-METHYL-4-NITROBENZALDEHYDE;Benzaldehyde, 3-methyl-4-nitro-;3-Methyl-4-nitrobenzaldehyde 98%;5-Formyl-2-nitrotoluene, 4-Formyl-2-methylnitrobenzene
CBNumber: CB8490362
Molecular Formula: C8H7NO3
Formula Weight: 165.15
MOL File: 18515-67-8.mol

More

Less

3-METHYL-4-NITROBENZALDEHYDE Property

Boiling point:: 304.4±30.0 °C(Predicted)
Density: 1.278±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
form: solid
color: Brown to dark brown
CAS DataBase Reference: 18515-67-8(CAS DataBase Reference)

More

Less

Safety

HS Code: 2913000090

More

Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

More

Less

N-Bromosuccinimide Price

TRC

Product number: M341375
Product name: 3-Methyl-4-nitrobenzaldehyde
Packaging: 500mg
Price: $110
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4754-1-Z2
Product name: 3-Methyl-4-nitrobenzaldehyde
Purity: 97%
Packaging: 1g
Price: $100
Updated: 2021/12/16

AK Scientific

Product number: V1651
Product name: 3-Methyl-4-nitrobenzaldehyde
Packaging: 1g
Price: $115
Updated: 2021/12/16

Matrix Scientific

Product number: 072750
Product name: 3-Methyl-4-nitrobenzaldehyde
Purity: 95+%
Packaging: 1g
Price: $145
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4754-1-Z2
Product name: 3-Methyl-4-nitrobenzaldehyde
Purity: 97%
Packaging: 5G
Price: $373
Updated: 2021/12/16

More

Less

3-METHYL-4-NITROBENZALDEHYDE Chemical Properties,Usage,Production

Synthesis

80866-75-7

18515-67-8

Step 1: 3-methyl-4-nitrobenzyl alcohol (1.0 eq.) was dissolved in dichloromethane, pyridinium chlorochromate (1.1 eq.) was added and the reaction mixture was stirred for 3 hours at room temperature. After completion of the reaction, the mixture was filtered through diatomaceous earth and the filtrate was concentrated under reduced pressure. The concentrated residue was adsorbed onto 100-200 mesh silica and purified by rapid column chromatography on silica gel, using a petroleum ether (60-80 °C) solution of 5% ethyl acetate as eluent to afford 3-methyl-4-nitrobenzaldehyde in milky white crystalline form in 93% yield. The product characterization data were as follows: 1H NMR (300 MHz, CDCl3) δ: 2.66 (s, 3H), 7.84-7.87 (m, 2H), 8.04-8.07 (d, J = 8.7 Hz, 1H), 10.12 (s, 1H); IR (KBr) 3104, 3079, 2981, 2857, 2743, 1702. 1607, 1518, 1383, 1361, 1308, 1226, 1153, 1008, 832, 735 cm-1.

References

[1] Patent: WO2010/23609, 2010, A1. Location in patent: Page/Page column 117
[2] Chemistry - A European Journal, 2015, vol. 21, # 9, p. 3567 - 3571
[3] European Journal of Organic Chemistry, 2016, vol. 2016, # 20, p. 3401 - 3407
[4] Farmaco, 1999, vol. 54, # 9, p. 579 - 583
[5] Patent: WO2007/24843, 2007, A2. Location in patent: Page/Page column 63-64

3-METHYL-4-NITROBENZALDEHYDE Preparation Products And Raw materials

Raw materials

Preparation Products

More

Less

3-METHYL-4-NITROBENZALDEHYDE Suppliers

China 89 Germany 1 India 4 Switzerland 1 United Kingdom 4 United States 12 Global 111

J & K SCIENTIFIC LTD.

Tel: 18210857532; 18210857532
Fax: 86-10-82849933
Email: jkinfo@jkchemical.com
Country: China
ProdList: 96815
Advantage: 76

3B Pharmachem (Wuhan) International Co.,Ltd.

Tel: 821-50328103-801 18930552037
Fax: 86-21-50328109
Email: 3bsc@sina.com
Country: China
ProdList: 15838
Advantage: 69

Capot Chemical Co., Ltd

Tel: +86 (0) 571 85 58 67 18
Fax: 0086-571-85864795
Country: China
ProdList: 18207
Advantage: 66

Shanghai Longsheng chemical Co.,Ltd.

Tel: 021-58099652-8005 13585536065
Fax: 021-58099609
Email: bin.wu@shlschem.com
Country: China
ProdList: 9883
Advantage: 59

Shanghai Hanhong Scientific Co.,Ltd.

Tel: 021-54306202 13764082696
Email: info@hanhongsci.com
Country: China
ProdList: 42934
Advantage: 64

Beijing Eternalchem Co,. Ltd.

Tel: 010-59484199 18611897322
Email: sales@eternalchem.com
Country: China
ProdList: 4383
Advantage: 60

Hangzhou Yuhao Chemical Technology Co., Ltd

Tel: 0571-82693216
Fax: +86-571-82880190
Email: info@yuhaochemical.com
Country: China
ProdList: 6387
Advantage: 52

NovoChemy Ltd.

Tel: 021-31261262/ 49 (0)17662837245
Fax: (0)21-33250524
Email: sales@novochemy.com
Country: Germany
ProdList: 6328
Advantage: 58

Shanghai Topbiochem Technology Co., Ltd

Tel: 021-58170097
Email: info@topbiochem.com
Country: China
ProdList: 9510
Advantage: 58

Shanghai Jian Chao Chemical Technology Co., Ltd.

Tel: 150-2103-5486 18017383231
Fax: qq：2817624287
Email: 983544897@qq.com
Country: China
ProdList: 9342
Advantage: 55

More

Less

View Lastest Price from 3-METHYL-4-NITROBENZALDEHYDE manufacturers

Career Henan Chemical Co

Product: 3-METHYL-4-NITROBENZALDEHYDE 18515-67-8
Price: US $3.00/KG
Min. Order: 1KG
Purity: 98%min
Supply Ability: 200KG
Release date: 2020-01-07

18515-67-8, 3-METHYL-4-NITROBENZALDEHYDERelated Search:

3-METHYL-4-NITROBENZAMIDE 3-Methyl-4-nitrobenzoic acid Methyl 3-methyl-4-nitrobenzoate 2-Bromo-4-methyl-5-nitrobenzaldehyde 4-NITROISOPHTHALIC ACID 3,5-DIMETHYL-4-NITROBENZOIC ACID 3-METHYL-4-NITROBENZHYDRAZIDE ETHYL 3-METHYL-4-NITROBENZOATE 4-METHYL-3-NITROBENZALDEHYDE,4-Methyl-3-nitrobenzaldehyde,98%,4-Methyl-3-nitrobenzaldehyde 98% 5-METHYL-2-NITROBENZALDEHYDE 4-METHYL-2-NITROBENZALDEHYDE 2-METHYL-5-NITROBENZALDEHYDE, 95+%,2-METHYL-5-NITROBENZALDEHYDE N-[2-(2,5-DICHLORO-PHENYL)-BENZOOXAZOL-5-YL]-3-METHYL-4-NITRO-BENZAMIDE 3-METHYL-N-[4-(6-METHYL-BENZOTHIAZOL-2-YL)-PHENYL]-4-NITRO-BENZAMIDE N-[5-(5-CHLORO-BENZOOXAZOL-2-YL)-2-METHYL-PHENYL]-3-METHYL-4-NITROBENZAMIDE N-[2-(3-FLUORO-PHENYL)-BENZOOXAZOL-5-YL]-3-METHYL-4-NITRO-BENZAMIDE 2-(5-HYDROXYCARBONYL-2-NITROPHENYL)MALONDIALDEHYDE MONOHYDRATE, 95 4,6-DINITRO-1,3-BENZENEDICARBOXYLIC ACID

5-Formyl-2-nitrotoluene, 4-Formyl-2-methylnitrobenzene

Benzaldehyde, 3-methyl-4-nitro-

3-METHYL-4-NITROBENZALDEHYDE

3-Methyl-4-nitrobenzaldehyde 98%

18515-67-8