ETHYL 3-METHYL-4-NITROBENZOATE

Product Name: ETHYL 3-METHYL-4-NITROBENZOATE
CAS No.: 30650-90-9
Chemical Name: ETHYL 3-METHYL-4-NITROBENZOATE
Synonyms: ethyl 4-nitro-m-toluate;ETHYL 3-METHYL-4-NITROBENZOATE;Ethyl 4-Nitro-3-Methyl benzoate;3-methyl-4-nitrobenzoic acid ethyl ester;Benzoic acid, 3-methyl-4-nitro-, ethyl ester
CBNumber: CB7175413
Molecular Formula: C10H11NO4
Formula Weight: 209.2
MOL File: 30650-90-9.mol

More

Less

ETHYL 3-METHYL-4-NITROBENZOATE Property

Melting point:: 53-55°C
Boiling point:: 331.3±30.0 °C(Predicted)
Density: 1.216±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
Appearance: White to off-white Solid

More

Less

Safety

HS Code: 2916310090

More

Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

More

Less

N-Bromosuccinimide Price

TRC

Product number: E926475
Product name: Ethyl3-methyl-4-nitrobenzoate
Packaging: 1g
Price: $55
Updated: 2021/12/16

TRC

Product number: E926475
Product name: Ethyl3-methyl-4-nitrobenzoate
Packaging: 2.5g
Price: $65
Updated: 2021/12/16

AK Scientific

Product number: J56070
Product name: Ethyl3-methyl-4-nitrobenzoate
Packaging: 25g
Price: $34
Updated: 2021/12/16

Matrix Scientific

Product number: 072805
Product name: Ethyl 3-methyl-4-nitrobenzoate
Purity: 95+%
Packaging: 10g
Price: $70
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4754-1-1D
Product name: Ethyl 3-methyl-4-nitrobenzoate
Packaging: 5G
Price: $96
Updated: 2021/12/16

More

Less

ETHYL 3-METHYL-4-NITROBENZOATE Chemical Properties,Usage,Production

Synthesis

3113-71-1

75-03-6

30650-90-9

A. Synthesis of ethyl 3-methyl-4-nitrobenzoate. A mixture of 3-methyl-4-nitrobenzoic acid (362.3 g, 2.0 mol), N,N-dimethylformamide (200 mL), sodium bicarbonate (200 g, 2.38 mol), and ethyl iodide (623.9 g, 4.0 mol) was stirred for 18 hr. at 70 °C. Upon completion of the reaction, the mixture was cooled to room temperature and poured into water (2000 mL). The resulting solid product was collected by filtration, washed with water and dried. Subsequently, the solid was further washed with hexane and dried to afford the title compound ethyl 3-methyl-4-nitrobenzoate (382.1 g, 91% yield) as an off-white solid with a melting point of 51-52.5°C. The structure of the product was confirmed by 1H NMR (CDCl3) and mass spectrometry (NH3-Cl):1H NMR (CDCl3) δ 8.04-7.98 (m, 3H 3H), 4.42 (q, 2H), 2.63 (s, 3H), 1.42 (t, 3H); mass spectrum (NH3-Cl) m/z 210 (100%, M+H+).

References

[1] Patent: US2001/44535, 2001, A1
[2] Patent: US5760028, 1998, A

ETHYL 3-METHYL-4-NITROBENZOATE Preparation Products And Raw materials

Raw materials

Preparation Products

More

Less

ETHYL 3-METHYL-4-NITROBENZOATE Suppliers

China 58 Germany 2 India 2 United Kingdom 6 United States 11 Global 79

J & K SCIENTIFIC LTD.

Tel: 18210857532; 18210857532
Fax: 86-10-82849933
Email: jkinfo@jkchemical.com
Country: China
ProdList: 96815
Advantage: 76

Alfa Aesar

Tel: 400-6106006
Fax: 021-67582001/03/05
Email: saleschina@alfa-asia.com
Country: China
ProdList: 30123
Advantage: 84

Energy Chemical

Tel: 021-021-58432009 400-005-6266
Fax: 021-58436166
Email: sales8178@energy-chemical.com
Country: China
ProdList: 44801
Advantage: 61

Shanghai Hanhong Scientific Co.,Ltd.

Tel: 021-54306202 13764082696
Email: info@hanhongsci.com
Country: China
ProdList: 42934
Advantage: 64

Shanghai Sunway Pharmaceutical Technology Co., Ltd

Tel: 18270980682
Fax: 021 51613951
Email: mlcheng@sunwaypharm.cn
Country: China
ProdList: 8669
Advantage: 57

Shanghai Topbiochem Technology Co., Ltd

Tel: +86-21-60341587
Fax: +86-21-61294319
Email: sales@topbiochem.com
Country: China
ProdList: 6175
Advantage: 58

Shanghai Raise Chemical Technology Co.,Ltd

Tel: +86-021-50935922
Fax: +86-021-33847795
Country: China
ProdList: 7865
Advantage: 55

Changzhou EFC Chemistry&Science Co.,Ltd

Tel: 18136598690 18136597130
Fax: 86-0519-89617886
Country: China
ProdList: 235
Advantage: 58

Shanghai YuLue Chemical Co., Ltd.

Tel: 021-60345187 13671753212
Fax: 021-34702061
Email: lzz841106@aliyun.com
Country: China
ProdList: 10263
Advantage: 55

Nanjing Derno Pharmaceutical Technology Co., Ltd.

Tel: 025-86957866 13952093866
Fax: 025-68661287
Email: sales@dernopharm.com
Country: China
ProdList: 932
Advantage: 58

More

Less

View Lastest Price from ETHYL 3-METHYL-4-NITROBENZOATE manufacturers

Career Henan Chemical Co

Product: ETHYL 3-METHYL-4-NITROBENZOATE 30650-90-9
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: Customized
Release date: 2019-07-03

30650-90-9, ETHYL 3-METHYL-4-NITROBENZOATERelated Search:

AKOS BB-3093 METHYL 2-AMINO-5-METHYLBENZOATE BENZOIC ACID,4-BROMO-2-METHYL-,METHYL ESTER 7-Chloro-1-cyclopropyl-6-fluoro-1,4-dihydro-4-oxo-1,8-naphthyridine-3-carboxylic Acid Ethyl Ester Methyl 4-hydroxy-2-methylbenzoate ETHYL 2-AMINO-5-METHYLBENZOATE Methyl 2-Methyl-4-nitrobenzoate 4-AMINO-2-METHYLBENZOIC ACID ETHYL ESTER Ethyl 2-methyl-3-nitrobenzoate METHYL 2-BROMO-5-METHYLBENZOATE Methyl-5-amino-2-chlorobenzoate Ethyl 3-bromo-4-methylbenzoate Methyl 5-Methyl-2-Nitrobenzoate 5-AMINO-2-METHYL-BENZOIC ACID METHYL ESTER METHYL 4-CHLORO-3-METHYLBENZOATE 3-BROMO-2-METHYL-BENZOIC ACID METHYL ESTER Methyl4-amino-2-methylbenzoate Ethyl 4-Bromo-3-methylbenzoate

ETHYL 3-METHYL-4-NITROBENZOATE

3-methyl-4-nitrobenzoic acid ethyl ester

ethyl 4-nitro-m-toluate

Ethyl 4-Nitro-3-Methyl benzoate

Benzoic acid, 3-methyl-4-nitro-, ethyl ester

30650-90-9