Ethyl 4-(aminomethyl)benzoate

Product Name: Ethyl 4-(aminomethyl)benzoate
CAS No.: 366-84-7
Chemical Name: Ethyl 4-(aminomethyl)benzoate
Synonyms: RARECHEM AL BW 1094;ethyl 4-(aminomethyl)benzoate;4-AMINOMETHYL-BENZOIC ACID ETHYL ESTER;Benzoic acid, 4-(aminomethyl)-, ethyl ester
CBNumber: CB8491930
Molecular Formula: C10H13NO2
Formula Weight: 179.22
MOL File: 366-84-7.mol

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Ethyl 4-(aminomethyl)benzoate Property

Melting point:: 215 °C(Solv: ethanol (64-17-5))
Boiling point:: 293.9±23.0 °C(Predicted)
Density: 1.093±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Inert atmosphere,Store in freezer, under -20°C
pka: 8.69±0.10(Predicted)
Appearance: Light yellow to yellow Liquid

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

AK Scientific

Product number: 3372AL
Product name: Ethyl4-(aminomethyl)benzoate
Packaging: 5g
Price: $691
Updated: 2021/12/16

Matrix Scientific

Product number: 144382
Product name: Ethyl 4-(aminomethyl)benzoate
Purity: 95%
Packaging: 1g
Price: $731
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0122074
Product name: ETHYL 4-(AMINOMETHYL)BENZOATE
Purity: 95.00%
Packaging: 1G
Price: $765.23
Updated: 2021/12/16

AK Scientific

Product number: 3372AL
Product name: Ethyl4-(aminomethyl)benzoate
Packaging: 10g
Price: $1011
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0122074
Product name: ETHYL 4-(AMINOMETHYL)BENZOATE
Purity: 95.00%
Packaging: 2.5G
Price: $1065.66
Updated: 2021/12/16

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Ethyl 4-(aminomethyl)benzoate Chemical Properties,Usage,Production

Synthesis

56-91-7

64-17-5

366-84-7

Example 1: Preparation of ethyl 4-(aminomethyl)benzoate Add 7.5 g (50 mmol) of 4-(aminomethyl)benzoic acid to a 250 mL three-necked round-bottomed flask. 100mL of anhydrous ethanol was added. Under the condition of ice bath, 20.8 g (175 mmol) of thionyl chloride was slowly added dropwise, and after completion of the dropwise addition, the reaction was stirred at room temperature for 30 min, followed by heating and refluxing for 4 hours. Upon completion of the reaction, the heating was stopped and the ethanol was removed by distillation under reduced pressure to give a white solid product. The resulting solid was dissolved in 150 mL of ethyl acetate, and the pH was adjusted to 7-8 by slowly adding 35% aqueous sodium hydroxide under the condition of an ice bath. the organic layer and the aqueous layer were separated, and the organic layer was washed with saturated saline three times, each time 30 mL. the organic layer was dried with anhydrous sodium sulfate, filtered, and concentrated to give a yellow solid product in 90% yield.

References

[1] Patent: CN104016942, 2016, B. Location in patent: Paragraph 0090; 0091; 0092
[2] Journal of the American Chemical Society, 1943, vol. 65, p. 2281,2283
[3] Organic and Biomolecular Chemistry, 2013, vol. 11, # 36, p. 6023 - 6028
[4] Journal of the American Society for Mass Spectrometry, 2018, vol. 29, # 4, p. 694 - 703

Ethyl 4-(aminomethyl)benzoate Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from Ethyl 4-(aminomethyl)benzoate manufacturers

Career Henan Chemical Co

Product: 4-AMINOMETHYL-BENZOIC ACID ETHYL ESTER 366-84-7
Price: US $6.60/KG
Min. Order: 1KG
Purity: 97%-99%
Supply Ability: 1kg -1000kg
Release date: 2020-01-02

366-84-7, Ethyl 4-(aminomethyl)benzoateRelated Search:

4-(Aminomethyl)benzoic acid

RARECHEM AL BW 1094

4-AMINOMETHYL-BENZOIC ACID ETHYL ESTER

Benzoic acid, 4-(aminomethyl)-, ethyl ester

ethyl 4-(aminomethyl)benzoate

366-84-7

pharmacetical