2,5-DIBROMOPHENOL
- Product Name
- 2,5-DIBROMOPHENOL
- CAS No.
- 28165-52-8
- Chemical Name
- 2,5-DIBROMOPHENOL
- Synonyms
- Phenol, 2,5-dibromo-;2,5-Dibromophenol 98%;2,5-Dibromophenol 96+%;2,5-Dibromo-1-hydroxybenzene;2,5-Dibromophenol in isopropanol;2,5-Dibromophenol@100 μg/mL in Toluene
- CBNumber
- CB8500692
- Molecular Formula
- C6H4Br2O
- Formula Weight
- 251.9
- MOL File
- 28165-52-8.mol
2,5-DIBROMOPHENOL Property
- Melting point:
- 73-74 °C
- Boiling point:
- 244.6±20.0 °C(Predicted)
- Density
- 2.095±0.06 g/cm3(Predicted)
- storage temp.
- Inert atmosphere,Room Temperature
- solubility
- Chloroform (Slightly), Methanol (Slightly)
- form
- powder
- pka
- 7.47±0.10(Predicted)
- color
- White
- InChI
- InChI=1S/C6H4Br2O/c7-4-1-2-5(8)6(9)3-4/h1-3,9H
- InChIKey
- GUXWVUVLXIJHQF-UHFFFAOYSA-N
- SMILES
- C1(O)=CC(Br)=CC=C1Br
Safety
- HS Code
- 2908190090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- D425983
- Product name
- 2,5-Dibromophenol
- Packaging
- 100mg
- Price
- $50
- Updated
- 2021/12/16
- Product number
- D425983
- Product name
- 2,5-Dibromophenol
- Packaging
- 250mg
- Price
- $65
- Updated
- 2021/12/16
- Product number
- FD153819
- Product name
- 2,5-Dibromophenol
- Packaging
- 2g
- Price
- $140
- Updated
- 2021/12/16
- Product number
- OR18409
- Product name
- 2,5-Dibromophenol
- Purity
- 98%
- Packaging
- 10g
- Price
- $151
- Updated
- 2021/12/16
- Product number
- X0151
- Product name
- 2,5-Dibromophenol
- Packaging
- 5g
- Price
- $171
- Updated
- 2021/12/16
2,5-DIBROMOPHENOL Chemical Properties,Usage,Production
Chemical Properties
2,5-Dibromophenol is a white to pale yellow powder, slightly soluble in water, very slightly soluble in chloroform and methanol. It should be stored under an inert atmosphere and at room temperature to maintain its stability.
Uses
2,5-Dibromophenol is an important intermediate in organic synthesis and is often used to synthesize other complex organic molecules.
Synthesis
3638-73-1
28165-52-8
General procedure for the synthesis of 2,5-dibromophenol from 2,5-dibromoaniline: Sodium nitrite (65.2 mmol) was added in batches to a solution of trifluoroacetic acid (80 mL) containing 2,5-dibromoaniline (55.8 mmol) at 0 °C. Subsequently, the resulting solution was slowly added to a boiling solution of 50% sulfuric acid (120 mL) containing sodium sulfate (10 g) and the reaction mixture was kept at reflux for 1 hour. Upon completion of the reaction, the product was steam distilled and the distillate was extracted using dichloromethane (2 x 200 mL). The organic layers were combined, dried over sodium sulfate and concentrated to give 2,5-dibromophenol as a yellow solid in 41% yield.
References
[1] Environmental Science and Technology, 2001, vol. 35, # 18, p. 3749 - 3756
[2] Patent: WO2009/23844, 2009, A2. Location in patent: Page/Page column 129-130
[3] Patent: US2010/16297, 2010, A1. Location in patent: Page/Page column 33-34
[4] Patent: WO2010/21797, 2010, A1. Location in patent: Page/Page column 94-95
[5] Patent: US2010/29629, 2010, A1. Location in patent: Page/Page column 62
2,5-DIBROMOPHENOL Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2,5-DIBROMOPHENOL manufacturers
- Product
- 2,5-DIBROMOPHENOL 28165-52-8
- Price
- US $0.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 10000KGS
- Release date
- 2025-03-11
- Product
- 2,5-DIBROMOPHENOL 28165-52-8
- Price
- US $6.60/KG
- Min. Order
- 1KG
- Purity
- 97%-99%
- Supply Ability
- 1kg-1000kg
- Release date
- 2019-12-30