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2-AMINO-4-CHLORO-6-NITROTOLUENE

Product Name
2-AMINO-4-CHLORO-6-NITROTOLUENE
CAS No.
219312-44-4
Chemical Name
2-AMINO-4-CHLORO-6-NITROTOLUENE
Synonyms
2-AMINO-4-CHLORO-6-NITROTOLUENE;5-Chloro-2-Methyl-3-nitroaniline;2-amino-4-chloro-7-nitro-toluene;5-chloro-2-methyl-3-nitrobenzenamine;Benzenamine, 5-chloro-2-methyl-3-nitro-
CBNumber
CB8731818
Molecular Formula
C7H7ClN2O2
Formula Weight
186.6
MOL File
219312-44-4.mol
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2-AMINO-4-CHLORO-6-NITROTOLUENE Property

Boiling point:
333.4±37.0 °C(Predicted)
Density 
1.415±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
pka
1.08±0.10(Predicted)
Appearance
Yellow to orange Solid
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Safety

HS Code 
2921490090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
C994185
Product name
5-Chloro-2-methyl-3-nitroaniline
Packaging
1mg
Price
$45
Updated
2021/12/16
TRC
Product number
C994185
Product name
5-Chloro-2-methyl-3-nitroaniline
Packaging
2mg
Price
$60
Updated
2021/12/16
ChemScene
Product number
CS-0054218
Product name
5-Chloro-2-methyl-3-nitroaniline
Packaging
250mg
Price
$54
Updated
2021/12/16
ChemScene
Product number
CS-0054218
Product name
5-Chloro-2-methyl-3-nitroaniline
Packaging
1g
Price
$144
Updated
2021/12/16
AK Scientific
Product number
2903AL
Product name
5-Chloro-2-methyl-3-nitroaniline
Packaging
100mg
Price
$169
Updated
2021/12/16
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2-AMINO-4-CHLORO-6-NITROTOLUENE Chemical Properties,Usage,Production

Synthesis

35572-79-3

219312-44-4

4-Iodo-2,6-dinitrotoluene (5.9 g, 23.60 mmol) was used as raw material and dissolved in a solvent mixture of methanol (10 mL) and 1,4-dioxane (5 mL). Under ice bath cooling conditions, 10 N hydrochloric acid (12 mL) and iron powder (3.96 g, 70.80 mmol) were slowly added. The reaction mixture was stirred at 80 °C for 3 h. The progress of the reaction was monitored by thin layer chromatography (TLC) until complete conversion of the feedstock. Upon completion of the reaction, 3.55 g of the light yellow powdery product 2-amino-4-chloro-6-nitrotoluene was obtained in 68.4% yield.

References

[1] Patent: CN108689937, 2018, A. Location in patent: Paragraph 0069; 0070; 0073; 0074
[2] Patent: CN108689936, 2018, A. Location in patent: Paragraph 0070; 0072; 0076; 0077
[3] Patent: US2010/63066, 2010, A1. Location in patent: Page/Page column 36
[4] Journal of the Chemical Society, 1905, vol. 87, p. 1265
[5] Patent: US5952362, 1999, A

2-AMINO-4-CHLORO-6-NITROTOLUENE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-AMINO-4-CHLORO-6-NITROTOLUENE Suppliers

China 30 India 3 United Kingdom 1 United States 4 Global 38
Aladdin Scientific
Tel
Email
tp@aladdinsci.com
Country
United States
ProdList
57505
Advantage
58
Combi-Blocks Inc.
Tel
--
Fax
--
Email
sales@combi-blocks.com
Country
United States
ProdList
6618
Advantage
69
3B Scientific Corporation
Tel
--
Fax
--
Email
sales@3bsc.com
Country
United States
ProdList
6718
Advantage
47
Sinova Inc.
Tel
--
Fax
--
Email
sales@sinovainc.com
Country
United States
ProdList
4009
Advantage
58
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View Lastest Price from 2-AMINO-4-CHLORO-6-NITROTOLUENE manufacturers

Career Henan Chemical Co
Product
5-Chloro-2-methyl-3-nitroaniline 219312-44-4
Price
US $1.00/g
Min. Order
1g
Purity
99%
Supply Ability
1ton
Release date
2020-01-10

219312-44-4, 2-AMINO-4-CHLORO-6-NITROTOLUENERelated Search:

BENZENEACETIC ACID, 4-CHLORO-2,6-DINITRO- 1-CHLORO-2,4-DIMETHYL-3,5-DINITRO-BENZEN 2-AMINO-4-CHLORO-6-NITROBENZOIC ACID 4-CHLORO-2,6-DINITROBENZOIC ACID 2-(ACETYL)AMINO-4-CHLORO-6-NITROTOLUENE 4-CHLORO-2,6-DINITROPHENYL ACETALDEHYDE 2-BROMOMETHYL-5-CHLORO-1,3-DINITROBENZENE 2-AMINO-4-CHLORO-6-NITROTOLUENE 4-IODO-2,6-DINITROTOLUENE

  • 2-AMINO-4-CHLORO-6-NITROTOLUENE
  • 5-Chloro-2-Methyl-3-nitroaniline
  • 5-chloro-2-methyl-3-nitrobenzenamine
  • Benzenamine, 5-chloro-2-methyl-3-nitro-
  • 2-amino-4-chloro-7-nitro-toluene
  • 219312-44-4