3-PIPERIDINOPHENOL

Product Name: 3-PIPERIDINOPHENOL
CAS No.: 27292-50-8
Chemical Name: 3-PIPERIDINOPHENOL
Synonyms: Nsc23894;3-PIPERIDINOPHENOL;3-(1-Piperidyl)phenol;3-(Piperidin-1-yl)phenol;Phenol, 3-(1-piperidinyl)-
CBNumber: CB8779634
Molecular Formula: C11H15NO
Formula Weight: 177.24
MOL File: 27292-50-8.mol

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3-PIPERIDINOPHENOL Property

Melting point:: 123-124 °C
Boiling point:: 338.9±25.0 °C(Predicted)
Density: 1.106±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 10.37±0.10(Predicted)
Appearance: White to off-white Solid

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Safety

HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B450193
Product name: 3-(piperidin-1-yl)phenol
Packaging: 100mg
Price: $65
Updated: 2021/12/16

AK Scientific

Product number: W5039
Product name: 3-(Piperidin-1-yl)phenol
Packaging: 1g
Price: $184
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0024101
Product name: 3-PIPERIDINOPHENOL
Purity: 95.00%
Packaging: 10G
Price: $1882.06
Updated: 2021/12/16

Chemenu

Product number: CM179439
Product name: 3-(piperidin-1-yl)phenol
Purity: 95+%
Packaging: 5g
Price: $286
Updated: 2021/12/16

Ambeed

Product number: A137213
Product name: 3-(Piperidin-1-yl)phenol
Purity: 97%
Packaging: 5g
Price: $296
Updated: 2021/12/16

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3-PIPERIDINOPHENOL Chemical Properties,Usage,Production

Synthesis

110-89-4

591-20-8

27292-50-8

General procedure for the synthesis of 3-piperidinylphenol from hexahydropyridine and m-bromophenol: N-(3-hydroxyphenyl)piperidine Pd(OAc)2 (129 mg, 0.578 mmol) was added to a mixture of piperidine (2.95 g, 34.68 mmol) and 3-bromophenol (5.00 g, 28.90 mmol). Under nitrogen protection, 2,8,9-tri-tert-butyl-2,5,8,9-tetraaza-1-phosphabicyclo[3.3.3]undecane (397 mg, 1.16 mmol), LiHMDS (66.5 cm3, 1 M in THF), and anhydrous toluene (110 cm3) were added sequentially. The reaction mixture was heated to 80 °C, maintained for 18 h and subsequently cooled to room temperature. Water (50 cm3) was added for partitioning and the aqueous layer was extracted with toluene (3 x 30 cm3). The organic phases were combined, dried over anhydrous sodium sulfate and concentrated under reduced pressure to remove the solvent. Purification by column chromatography [eluent ratio 3:7 ethyl acetate/hexane (Rf = 0.4)] gave an off-white solid product (2.56 g, 50% yield). NMR hydrogen spectrum (250 MHz, CDCl3) δH: 7.11-7.04 (1H, m, aryl ring H), 6.52 (1H, d, J = 8 Hz, aryl ring H), 6.35 (1H, s, aryl ring H), 6.29 (1H, d, J = 8 Hz, aryl ring H), 5.84 (1H, bs, OH), 3.08 (4H, t, J = 5 Hz , 2 × CH2), 1.75-1.62 (4H, m, 2 × CH2), 1.60-1.50 (2H, m, CH2); NMR carbon spectra (62.5 MHz, CDCl3) δC: 156.7, 153.4, 130.0, 109.3, 107.4, 104.6, 51.0, 25.5, 24.2; IR spectra ( KBr) νmax/cm?1: 3064, 2959, 2937, 2921, 2856, 1597, 1503, 1454, 1276, 1201, 1133, 1104, 971, 877; mass spectra (ESI) m/z: 178.12 (100%, [M + H]+).

References

[1] Advanced Synthesis and Catalysis, 2004, vol. 346, # 6, p. 611 - 616
[2] Patent: WO2010/67078, 2010, A2. Location in patent: Page/Page column 91
[3] Chemistry - A European Journal, 2009, vol. 15, # 12, p. 2742 - 2746
[4] Bioorganic and Medicinal Chemistry, 2013, vol. 21, # 22, p. 7107 - 7117

3-PIPERIDINOPHENOL Preparation Products And Raw materials

Raw materials

Preparation Products

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3-PIPERIDINOPHENOL Suppliers

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27292-50-8, 3-PIPERIDINOPHENOLRelated Search:

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Nsc23894

3-(Piperidin-1-yl)phenol

3-PIPERIDINOPHENOL

Phenol, 3-(1-piperidinyl)-

3-(1-Piperidyl)phenol

27292-50-8

ARYL ALCOHOL