METHYL-(3-NITRO-PYRIDIN-2-YL)-AMINE
- Product Name
- METHYL-(3-NITRO-PYRIDIN-2-YL)-AMINE
- CAS No.
- 4093-88-3
- Chemical Name
- METHYL-(3-NITRO-PYRIDIN-2-YL)-AMINE
- Synonyms
- N-METHYL-3-NITROPYRIDIN-2-AMINE;2-(Methylamino)-3-nitropyridine;N-METHYL-3-NITRO-2-PYRIDINAMINE;methyl-(3-nitro-2-pyridyl)amine;2-Pyridinamine, N-methyl-3-nitro-;METHYL-(3-NITRO-PYRIDIN-2-YL)-AMINE
- CBNumber
- CB8848400
- Molecular Formula
- C6H7N3O2
- Formula Weight
- 153.14
- MOL File
- 4093-88-3.mol
METHYL-(3-NITRO-PYRIDIN-2-YL)-AMINE Property
- Melting point:
- 67-69
- Boiling point:
- 262-262.5 °C(Press: 740 Torr)
- Density
- 1.343±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- pka
- 2.87±0.10(Predicted)
- Appearance
- Light yellow to yellow Solid
Safety
- Hazard Codes
- Xi
- HazardClass
- IRRITANT
- HS Code
- 2933399990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P260Do not breathe dust/fume/gas/mist/vapours/spray.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
N-Bromosuccinimide Price
- Product number
- B426508
- Product name
- N-Methyl-3-nitropyridin-2-amine
- Packaging
- 50mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- 4H54-1-Y8
- Product name
- 2-(Methylamino)-3-nitropyridine
- Packaging
- 250mg
- Price
- $35
- Updated
- 2021/12/16
- Product number
- 4H54-1-Y8
- Product name
- 2-(Methylamino)-3-nitropyridine
- Packaging
- 1g
- Price
- $105
- Updated
- 2021/12/16
- Product number
- V5831
- Product name
- N-Methyl-3-nitropyridin-2-amine
- Packaging
- 5g
- Price
- $271
- Updated
- 2021/12/16
- Product number
- 032311
- Product name
- N-Methyl-3-nitro-2-pyridinamine
- Packaging
- 500mg
- Price
- $342
- Updated
- 2021/12/16
METHYL-(3-NITRO-PYRIDIN-2-YL)-AMINE Chemical Properties,Usage,Production
Synthesis
5470-18-8
4093-88-3
Synthesis of N-methyl-3-nitropyridin-2-amine: methylamine (33% ethanol solution, 110 mL, 883 mmol) was added to a 500 mL three-necked round-bottomed flask and cooled to 0 °C in an ice bath. Under stirring, 2-chloro-3-nitropyridine (20 g, 126 mmol) was added in batches, and care was taken to control the dosing rate to alleviate the exothermic reaction. After the addition was completed, the reaction mixture was continued to be stirred at 0 °C for 2 h, followed by slow warming to room temperature and stirring for 1 h. The reaction was then concentrated under reduced pressure. Upon completion of the reaction, the solvent was removed by concentration under reduced pressure and the residue was dissolved in 500 mL of water and extracted with ethyl acetate (3 x 150 mL). The organic layers were combined, dried over anhydrous sodium sulfate, filtered and concentrated under reduced pressure to give the bright orange-yellow solid product N-methyl-3-nitropyridin-2-amine (19 g, 98.5% yield).
References
[1] Patent: US2012/228583, 2012, A1
METHYL-(3-NITRO-PYRIDIN-2-YL)-AMINE Preparation Products And Raw materials
Raw materials
Preparation Products
METHYL-(3-NITRO-PYRIDIN-2-YL)-AMINE Suppliers
- Tel
- --
- Fax
- --
- sales@apolloscientific.co.uk
- Country
- United Kingdom
- ProdList
- 6084
- Advantage
- 88
- Tel
- --
- Fax
- --
- enquiries@keyorganics.ltd.uk
- Country
- United Kingdom
- ProdList
- 6663
- Advantage
- 50
View Lastest Price from METHYL-(3-NITRO-PYRIDIN-2-YL)-AMINE manufacturers
- Product
- METHYL-(3-NITRO-PYRIDIN-2-YL)-AMINE 4093-88-3
- Price
- US $30.00-20.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 200000KG
- Release date
- 2024-08-01