4-(2-hydroxyethyl)benzoic acid

Product Name: 4-(2-hydroxyethyl)benzoic acid
CAS No.: 46112-46-3
Chemical Name: 4-(2-hydroxyethyl)benzoic acid
Synonyms: 4-(2-Hydroxyethyl);4-(2-Hydroxyethyl)benzoic acid;Benzoic acid, 4-(2-hydroxyethyl)-;4-(2-Hydroxyethyl)benzoic acid 95%
CBNumber: CB8947134
Molecular Formula: C9H10O3
Formula Weight: 166.17
MOL File: 46112-46-3.mol

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4-(2-hydroxyethyl)benzoic acid Property

Melting point:: 127-128 °C
Boiling point:: 345.8±25.0 °C(Predicted)
Density: 1.256±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 4.26±0.10(Predicted)
Appearance: White to off-white Solid

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Safety

HS Code: 2916399090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: H515390
Product name: 4-(2-Hydroxyethyl)benzoicAcid
Packaging: 50mg
Price: $45
Updated: 2021/12/16

SynQuest Laboratories

Product number: 2629-1-97
Product name: 4-(2-Hydroxyethyl)benzoic acid
Packaging: 1g
Price: $376
Updated: 2021/12/16

SynQuest Laboratories

Product number: 2629-1-97
Product name: 4-(2-Hydroxyethyl)benzoic acid
Packaging: 250mg
Price: $189
Updated: 2021/12/16

AK Scientific

Product number: X8079
Product name: 4-(2-Hydroxyethyl)benzoicacid
Packaging: 1g
Price: $277
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0307687
Product name: 4-(2-HYDROXYETHYL)BENZOIC ACID
Purity: 95.00%
Packaging: 5MG
Price: $499.57
Updated: 2021/12/16

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4-(2-hydroxyethyl)benzoic acid Chemical Properties,Usage,Production

Synthesis

46190-45-8

46112-46-3

General procedure for the synthesis of 4-(2-hydroxyethyl)benzoic acid from methyl 4-(2-hydroxyethyl)benzoate: sodium hydroxide (58 mg, 1.43 mmol) was added to a mixed solution of methanol (3 mL) and water (1 mL) of methyl 4-(2-hydroxyethyl)benzoate (174 mg, 0.96 mmol) at room temperature. The reaction mixture was stirred at room temperature for 48 hours. Upon completion of the reaction, water (5 mL) was added to dilute and extracted with ether (3 x 20 mL) to remove unreacted feedstock and by-products. The aqueous phase was acidified with a 1:1 hydrochloric acid solution to pH=1 and a white solid was precipitated. The solid was collected by filtration to afford 4-(2-hydroxyethyl)benzoic acid (158 mg, 100% yield), and the product could be used in the next reaction without further purification. The structure of the product was confirmed by 1H NMR (300 MHz, CDCl3): δ 7.97 (d, J = 8.4 Hz, 2H), 7.27 (d, J = 8.4 Hz, 2H), 3.83 (t, J = 6.3 Hz, 2H), 2.88 (t, J = 6.3 Hz, 2H).

References

[1] Bioorganic and Medicinal Chemistry, 2013, vol. 21, # 11, p. 2988 - 2998
[2] Journal of the American Chemical Society, 2006, vol. 128, # 50, p. 16020 - 16021

4-(2-hydroxyethyl)benzoic acid Preparation Products And Raw materials

Raw materials

Preparation Products

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4-(2-hydroxyethyl)benzoic acid Suppliers

Canada 1 China 62 Germany 1 India 2 United Kingdom 3 United States 9 Global 78

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View Lastest Price from 4-(2-hydroxyethyl)benzoic acid manufacturers

R&D Scientific Inc.

Product: 4-(2-Hydroxyethyl)benzoic acid 46112-46-3
Price: US $900.00/g
Min. Order: 1g
Purity: 97
Supply Ability: 5 Kg
Release date: 2024-02-12

46112-46-3, 4-(2-hydroxyethyl)benzoic acid Related Search:

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4-(2-Hydroxyethyl)benzoic acid

Benzoic acid, 4-(2-hydroxyethyl)-

4-(2-Hydroxyethyl)

4-(2-Hydroxyethyl)benzoic acid 95%

46112-46-3

Aromatic Carboxylic Acids, Amides, Anilides, Anhydrides & Salts