Ethyl4-methylamino-3-nitrobenzoate

Product Name: Ethyl4-methylamino-3-nitrobenzoate
CAS No.: 71254-71-2
Chemical Name: Ethyl4-methylamino-3-nitrobenzoate
Synonyms: -3-nitrobenzoate;Ethyl4-methylamino-3-nitrobenzoate;4-(Methylamino)-3-nitro-benzoic acid ethylester;Benzoic acid, 4-(methylamino)-3-nitro-, ethyl ester
CBNumber: CB91073525
Molecular Formula: C10H12N2O4
Formula Weight: 224.21
MOL File: 71254-71-2.mol

More

Less

Ethyl4-methylamino-3-nitrobenzoate Property

Melting point:: 101 °C
Boiling point:: 372.8±32.0 °C(Predicted)
Density: 1.280±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: -2.62±0.25(Predicted)
Appearance: Yellow to orange Solid

More

Less

Safety

HS Code: 2922390090

More

Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

More

Less

N-Bromosuccinimide Price

AK Scientific

Product number: W8024
Product name: Ethyl4-(methylamino)-3-nitrobenzoate
Packaging: 1g
Price: $212
Updated: 2021/12/16

Matrix Scientific

Product number: 175038
Product name: Ethyl 4-(methylamino)-3-nitrobenzoate
Packaging: 1g
Price: $432
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0079483
Product name: ETHYL 4-METHYLAMINO-3-NITROBENZOATE
Purity: 95.00%
Packaging: 5G
Price: $909.56
Updated: 2021/12/16

Matrix Scientific

Product number: 175038
Product name: Ethyl 4-(methylamino)-3-nitrobenzoate
Packaging: 5g
Price: $1206
Updated: 2021/12/16

Matrix Scientific

Product number: 175038
Product name: Ethyl 4-(methylamino)-3-nitrobenzoate
Packaging: 10g
Price: $1602
Updated: 2021/12/16

More

Less

Ethyl4-methylamino-3-nitrobenzoate Chemical Properties,Usage,Production

Synthesis

367-80-6

74-89-5

71254-71-2

Ethyl 4-fluoro-3-nitrobenzoate (10.0 g, 46.9 mmol) prepared in Step 1-1-1 was dissolved in methanol (40 mL) and triethylamine (10 mL, 70.4 mmol) was added. A 40% methylamine-methanol solution (5.50 g, 70.4 mmol) was slowly added to the reaction mixture under ice bath cooling conditions. The reaction mixture was stirred continuously for 1 h under ice bath cooling and then ice water was added to quench the reaction. The precipitate was separated by filtration and washed with cold water. The washed product was subjected to cyclic drying overnight to afford ethyl 4-methylamino-3-nitrobenzoate (10.4 g, 99% yield) as a yellow powder.1H-NMR (CDCl3) δ: 8.87 (d, J = 1.9 Hz, 1H), 8.33 (brs, 1H), 8.08 (dd, J = 1.9, 9.2 Hz, 1H), 6.87- 6.84 (m, 1H), 4.35 (q, J = 6.9 Hz, 2H), 3.08 (d, J = 5.0 Hz, 3H), 1.38 (t, J = 6.9 Hz, 3H). Mass spectrum (m/z): 224 (M+), 179, 105 (base peak).

References

[1] Patent: US2013/79306, 2013, A1. Location in patent: Paragraph 0230; 0231; 0232; 0233

Ethyl4-methylamino-3-nitrobenzoate Preparation Products And Raw materials

Raw materials

Preparation Products

More

Less

Ethyl4-methylamino-3-nitrobenzoate Suppliers

China 58 France 1 Germany 2 India 1 United Kingdom 1 United States 11 Global 74

Hangzhou Yuhao Chemical Technology Co., Ltd

Tel: 0571-82693216
Fax: +86-571-82880190
Email: info@yuhaochemical.com
Country: China
ProdList: 6387
Advantage: 52

Chengdu HappySyn Pharmaceutical Technology Co., Ltd.

Tel: 028-85114309 18982182443
Email: yangli@happysyn.com
Country: China
ProdList: 2151
Advantage: 55

Nanjing Norris-Pharm Technology Co., Ltd

Tel: 18652989687
Fax: +86-25-52131256
Email: sales@norris-pharm.com
Country: China
ProdList: 8878
Advantage: 55

ShangHai Yuchuan Pharmaceutical Technology Co., Ltd.

Tel: 02161555100
Fax: -
Country: China
ProdList: 820
Advantage: 58

AN PharmaTech Co Ltd

Tel: 86(21)68097365
Fax: 86(21)33321566
Email: sales@anpharma.net
Country: China
ProdList: 4891
Advantage: 55

Zhengzhou Guancheng Laboratory equipment Sales

Tel: 0371-88888888 272369594
Fax: QQ:272369594
Email: 2723695949@qq.com
Country: China
ProdList: 4960
Advantage: 50

Chengdu Research Accelerators Technology Co., Ltd.

Tel: 028-64353063
Fax: 028-64353063 QQ:784253935
Email: reacchemical@163.com
Country: China
ProdList: 5253
Advantage: 58

Zhengzhou Alfachem Co., Ltd.

Tel: 0371-53765687 18937137882
Fax: QQ:2885373884
Email: 2853979813@qq.com
Country: China
ProdList: 7991
Advantage: 55

Quzhou AMK BioTech Co., Ltd

Tel: 0570-3081766 18357083060
Fax: 0570-3072337
Email: sales@qzamkbio.com
Country: China
ProdList: 1047
Advantage: 55

Shanghai Brain Biotechnology Co., Ltd.

Tel: 13564638271
Fax: 021-68948280
Email: shhjiang1977@163.com
Country: China
ProdList: 2987
Advantage: 55

More

Less

View Lastest Price from Ethyl4-methylamino-3-nitrobenzoate manufacturers

Career Henan Chemical Co

Product: Ethyl4-methylamino-3-nitrobenzoate 71254-71-2
Price: US $1.00/KG
Min. Order: 1KG
Purity: 95-99%
Supply Ability: 1ton
Release date: 2020-01-02

71254-71-2, Ethyl4-methylamino-3-nitrobenzoateRelated Search:

Ethyl4-methylamino-3-nitrobenzoate ETHYL 4-ACETAMIDO-3-NITROBENZOATE ETHYL 3-NITRO-4-(PIPERIDIN-4-CARBOXAMID-1-YL)BENZOATE 4-ETHYLAMINO-3-NITRO-BENZOIC ACID ETHYL ESTER ETHYL 3-NITRO-4-(HEXAMETHYLENEIMIN-1-YL)BENZOATE ETHYL 4-(3-METHYLPIPERAZIN-1-YL)-3-NITROBENZOATE HYDROCHLORIDE Ethyl 4-(4-methylpiperazin-1-yl)-3-nitrobenzoate ETHYL 3-NITRO-4-(4-METHYLPIPERIDIN-1-YL)BENZOATE ETHYL 3-NITRO-4-PIPERAZIN-1-YLBENZOATE ETHYL 3-NITRO-4-[4-(2-HYDROXYETHYL)PIPERAZIN-1-YL]BENZOATE ETHYL 3-NITRO-4-(PROPYLAMINO)BENZOATE ETHYL 3-NITRO-4-(PIPERIDIN-4-OL-1-YL)BENZOATE 4NNDIMETHYLAMINO3NITROBENZOICACID2ETHYLHEXYLESTER RARECHEM AL BI 1086 RARECHEM AL BI 0479 RARECHEM AL BI 0459 RARECHEM AL BI 1182

-3-nitrobenzoate

Ethyl4-methylamino-3-nitrobenzoate

Benzoic acid, 4-(methylamino)-3-nitro-, ethyl ester

4-(Methylamino)-3-nitro-benzoic acid ethylester

71254-71-2