7-BROMO-1H-PYRROLO[2,3-C]PYRIDINE

Product Name: 7-BROMO-1H-PYRROLO[2,3-C]PYRIDINE
CAS No.: 165669-35-2
Chemical Name: 7-BROMO-1H-PYRROLO[2,3-C]PYRIDINE
Synonyms: 7-BroMo-6-azaindole;7-Bromo-1H-pyrrolo[2,3-c]pyridine;1H-Pyrrolo[2,3-c]pyridine, 7-bromo-
CBNumber: CB91119225
Molecular Formula: C7H5BrN2
Formula Weight: 197.03
MOL File: 165669-35-2.mol

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7-BROMO-1H-PYRROLO[2,3-C]PYRIDINE Property

Melting point:: 174-178°C
Boiling point:: 362.0±22.0 °C(Predicted)
Density: 1.770±0.06 g/cm3(Predicted)
storage temp.: 2-8°C
form: solid
pka: 12.99±0.40(Predicted)
Appearance: Yellow to brown Solid

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Safety

Hazard Codes: T
Risk Statements: 25-37/38-41
Safety Statements: 26-36/37/39-45
RIDADR: UN 2811 6.1 / PGIII
WGK Germany: 3
HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H301Toxic if swalloed

H315Causes skin irritation

H318Causes serious eye damage

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P310IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 732168
Product name: 7-Bromo-6-azaindole
Purity: 95%
Packaging: 500mg
Price: $132
Updated: 2023/06/20

TRC

Product number: B446735
Product name: 7-Bromo-1H-pyrrolo[2,3-c]pyridine
Packaging: 500mg
Price: $310
Updated: 2021/12/16

Matrix Scientific

Product number: 124776
Product name: 7-Bromo-6-azaindole
Purity: 95+%
Packaging: 1g
Price: $364
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB148704
Product name: 7-Bromo-1H-pyrrolo[2,3-c]pyridine
Packaging: 500mg
Price: $370
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3H31-9-35
Product name: 7-Bromo-1H-pyrrolo[2,3-c]pyridine
Packaging: 250mg
Price: $175
Updated: 2021/12/16

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7-BROMO-1H-PYRROLO[2,3-C]PYRIDINE Chemical Properties,Usage,Production

Synthesis

19755-53-4

1826-67-1

165669-35-2

Example 1: Synthesis of [1-(4-methoxy-benzenesulfonyl)-1H-pyrrolo[2,3-c]pyridin-7-yl]-phenyl-amine (Compound 1); 7-bromo-6-azaindole (2 in Scheme 1): 2-bromo-3-nitropyridine (1 in Schemes 1,2, 2.0 g, 98%, 9.7 mmol) was dissolved in anhydrous THF (80 mL) and cooled the solution to -78 °C. An excess of vinyl magnesium bromide (1.0 M solution of THF, 40 mL, 40 mmol) was slowly added under nitrogen protection. The reaction mixture was stirred at -40 to -50 °C for 1 h. The reaction was subsequently quenched with saturated NaHCO3 solution. The organic and aqueous layers were separated and the aqueous layer was extracted with EtOAc (3 times). The organic layers were combined, dried with anhydrous MgSO4, filtered and the filtrate concentrated. The residue was purified by fast chromatography (eluent: EtOAc/hexane=1:2) to afford the target product 2 (1.1 g, 60%).1H NMR (500 MHz, CDCl3): δ 6.66 (dd, 1H, J=2.9,2.1Hz), 7.43 (dd, 1H, J=2.9,2.1Hz), 7.51 (d, 1H, J =5.2Hz), 8.03 (d, 1H, J=5.3Hz), 8.79 (br, 1H).

References

[1] Patent: WO2011/19634, 2011, A2. Location in patent: Page/Page column 13

7-BROMO-1H-PYRROLO[2,3-C]PYRIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

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7-BROMO-1H-PYRROLO[2,3-C]PYRIDINE Suppliers

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165669-35-2, 7-BROMO-1H-PYRROLO[2,3-C]PYRIDINE Related Search:

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7-Bromo-1H-pyrrolo[2,3-c]pyridine

1H-Pyrrolo[2,3-c]pyridine, 7-bromo-

7-BroMo-6-azaindole

165669-35-2