3-Bromo-4-nitrophenol
- Product Name
- 3-Bromo-4-nitrophenol
- CAS No.
- 5470-65-5
- Chemical Name
- 3-Bromo-4-nitrophenol
- Synonyms
- NSC 2796;NSC 27960;4-Nitro-3-bromophenol;3-Bromo-4-nitrophenol;3-Bromo-4-nitro-phenol;Phenol, 3-broMo-4-nitro-
- CBNumber
- CB91175735
- Molecular Formula
- C6H4BrNO3
- Formula Weight
- 218
- MOL File
- 5470-65-5.mol
3-Bromo-4-nitrophenol Property
- Melting point:
- 125-1270C
- Boiling point:
- 306.7±27.0 °C(Predicted)
- Density
- 1.881±0.06 g/cm3(Predicted)
- storage temp.
- Inert atmosphere,Room Temperature
- solubility
- DMSO (Slightly), Ethyl Acetate (Slightly), Methanol (Slightly)
- form
- Solid
- pka
- 6.32±0.10(Predicted)
- color
- Yellow to Brown
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Danger
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H317May cause an allergic skin reaction
H318Causes serious eye damage
H410Very toxic to aquatic life with long lasting effects
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P272Contaminated work clothing should not be allowed out of the workplace.
P273Avoid release to the environment.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P333+P313IF SKIN irritation or rash occurs: Get medical advice/attention.
P391Collect spillage. Hazardous to the aquatic environment
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- B686255
- Product name
- 3-Bromo-4-nitrophenol
- Packaging
- 10g
- Price
- $225
- Updated
- 2021/12/16
- Product number
- CS-W003684
- Product name
- 3-Bromo-4-nitrophenol
- Purity
- 98.97%
- Packaging
- 10g
- Price
- $159
- Updated
- 2021/12/16
- Product number
- Z4867
- Product name
- 3-Bromo-4-nitrophenol
- Packaging
- 250mg
- Price
- $73
- Updated
- 2021/12/16
- Product number
- CS-W003684
- Product name
- 3-Bromo-4-nitrophenol
- Purity
- 98.97%
- Packaging
- 5g
- Price
- $89
- Updated
- 2021/12/16
- Product number
- Z4867
- Product name
- 3-Bromo-4-nitrophenol
- Packaging
- 1g
- Price
- $91
- Updated
- 2021/12/16
3-Bromo-4-nitrophenol Chemical Properties,Usage,Production
Chemical Properties
Brown Solid
Synthesis
591-20-8
5470-65-5
Example 1 Synthesis of 3-bromo-4-nitrophenol (Compound 4): concentrated sulfuric acid (98%, 10.0 mL, 187.4 mmol) was slowly added dropwise to a solution of NaNO3 (13.5 g, 159.6 mmol) in water (30 mL), and the reaction temperature was maintained at 0-5°C. Subsequently, a solution of 3-bromophenol (12.0 g, 69.4 mmol) dissolved in ethanol (25 mL). The reaction mixture was stirred overnight at room temperature before being poured into ice water (300 mL) and extracted with dichloromethane (3 × 100 mL). The combined organic layers were dried over anhydrous Na2SO4, filtered and concentrated, and purified by silica gel column chromatography (eluent: hexane solution of 30% ethyl acetate) to afford the target product, compound 4, in 37.1% yield (5.59 g) as a yellow solid. The structure of the product was confirmed by 1H-NMR (DMSO-d6, 400 MHz), 13C-NMR (CDCl3, 100 MHz) and mass spectrometry (ESI).
References
[1] Organic Letters, 2013, vol. 15, # 13, p. 3234 - 3237
[2] Patent: US2014/256817, 2014, A1. Location in patent: Page/Page column
[3] Patent: WO2007/30366, 2007, A1. Location in patent: Page/Page column 91-92
[4] Journal of Organic Chemistry, 2009, vol. 74, # 1, p. 212 - 221
[5] Journal of the Chemical Society, 1926, p. 159
3-Bromo-4-nitrophenol Preparation Products And Raw materials
Raw materials
Preparation Products
3-Bromo-4-nitrophenol Suppliers
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View Lastest Price from 3-Bromo-4-nitrophenol manufacturers
- Product
- 3-Bromo-4-nitrophenol 5470-65-5
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 100KG
- Release date
- 2019-12-25