ChemicalBook > CAS DataBase List >  4-(Iodomethyl)tetrahydro-2H-pyran

4-(Iodomethyl)tetrahydro-2H-pyran

Product Name
4-(Iodomethyl)tetrahydro-2H-pyran
CAS No.
101691-94-5
Chemical Name
4-(Iodomethyl)tetrahydro-2H-pyran
Synonyms
4-(iodomethyl)oxane;4-IODOMETHYLTETRAHYDROPYRAN;4-(Iodomethyl)tetrahydropyrane;4-(IODOMETHYL)TETRAHYDRO-2H-PYRAN;(4-TETRAHYDROPYRANYL)METHYL IODIDE;Tetrahydro-4-(iodomethyl)-2H-pyran;4-(Iodomethyl)tetrahydro-2H-pyrane;2H-Pyran, tetrahydro-4-(iodomethyl)-
CBNumber
CB9120260
Molecular Formula
C6H11IO
Formula Weight
226.06
MOL File
101691-94-5.mol
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4-(Iodomethyl)tetrahydro-2H-pyran Property

Boiling point:
229.1±13.0 °C(Predicted)
Density 
1.645±0.06 g/cm3(Predicted)
storage temp. 
Keep in dark place,Sealed in dry,Store in freezer, under -20°C
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Safety

Risk Statements 
34
Safety Statements 
23-26-36/37/39-45
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H314Causes severe skin burns and eye damage

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P363Wash contaminated clothing before reuse.

P405Store locked up.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

SynQuest Laboratories
Product number
2H10-H-03
Product name
4-(Iodomethyl)oxane
Packaging
1g
Price
$83
Updated
2021/12/16
Matrix Scientific
Product number
092540
Product name
4-(Iodomethyl)tetrahydro-2H-pyran
Purity
95+%
Packaging
250mg
Price
$189
Updated
2021/12/16
SynQuest Laboratories
Product number
2H10-H-03
Product name
4-(Iodomethyl)oxane
Packaging
5G
Price
$300
Updated
2021/12/16
Matrix Scientific
Product number
092540
Product name
4-(Iodomethyl)tetrahydro-2H-pyran
Purity
95+%
Packaging
1g
Price
$420
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0022345
Product name
4-(IODOMETHYL)TETRAHYDRO-2H-PYRAN
Purity
95.00%
Packaging
1G
Price
$750.68
Updated
2021/12/16
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4-(Iodomethyl)tetrahydro-2H-pyran Chemical Properties,Usage,Production

Synthesis

4-(Iodomethyl)tetrahydro-2H-pyran is prepared from 4-(methanesulfonyloxymethyl)tetrahydropyran by heating and refluxing under conditions of reaction with sodium iodide in acetone. The specific method of operation is described below: .
Preparation: A mixture of Preparation (328g, 1.69mol) and sodium iodide (507g, 3.4mol) in acetone (3.3L) was refluxed for 4h. TLC (diethyl ether) showed significant mesylate remaining so further sodium iodide (127g, 0.65mol) was added and reflux continued for 16h. The mixture was cooled and filtered. The resulting cake was washed with acetone, dried, and11then partitioned between diethyl ether (800mL) and water (800mL). The aqueous phase was re-extracted with diethyl ether (200mL), the ether extracts combined and washed with 10% sodium thiosulphate solution (300mL) which decolourised the extract. Final washing with water (300mL), drying (MgS04) and then removal of the solvent provided the 4-(IODOMETHYL)TETRAHYDRO-2H-PYRAN (365g, 92% yield).

4-(Iodomethyl)tetrahydro-2H-pyran Preparation Products And Raw materials

Raw materials

Preparation Products

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4-(Iodomethyl)tetrahydro-2H-pyran Suppliers

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View Lastest Price from 4-(Iodomethyl)tetrahydro-2H-pyran manufacturers

Career Henan Chemical Co
Product
4-(Iodomethyl)tetrahydro-2H-pyran 101691-94-5
Price
US $1.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
500kg
Release date
2018-08-16

101691-94-5, 4-(Iodomethyl)tetrahydro-2H-pyranRelated Search:

3,5-bis(acetyloxy)-2-[4-(hexyloxy)phenoxy]-6-(iodomethyl)tetrahydro-2H-pyran-4-yl acetate 2,3,5-TRI(ACETYLOXY)-6-(IODOMETHYL)TETRAHYDRO-2H-PYRAN-4-YL ACETATE 8-(IODOMETHYL)-1,8-DIMETHYL-3-OXABICYCLO[3.2.1]OCTANE-2,4-DIONE 4-(Iodomethyl)tetrahydro-2H-pyran

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  • 101691-94-5