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3-BROMOFLUORANTHENE

Product Name
3-BROMOFLUORANTHENE
CAS No.
13438-50-1
Chemical Name
3-BROMOFLUORANTHENE
Synonyms
3-BROMOFLUORANTHENE;3-Bromof|uoranthene;3-Bromofluoranthene >Fluoranthene, 3-?bromo-
CBNumber
CB9146576
Molecular Formula
C16H9Br
Formula Weight
281.15
MOL File
13438-50-1.mol
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3-BROMOFLUORANTHENE Property

Melting point:
106.0 to 200.0 °C
Boiling point:
207°C/0.2mmHg(lit.)
Density 
1.578±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
solubility 
Chloroform (Slightly), Ethyl Acetate (Slightly)
form 
Solid
color 
Light Yellow to Yellow
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Safety

HS Code 
2902900000
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

TCI Chemical
Product number
B4599
Product name
3-Bromofluoranthene
Purity
>98.0%(GC)
Packaging
1g
Price
$33
Updated
2025/07/31
TCI Chemical
Product number
B4599
Product name
3-Bromofluoranthene
Purity
>98.0%(GC)
Packaging
5g
Price
$98
Updated
2025/07/31
TRC
Product number
B694833
Product name
3-Bromofluoranthene
Packaging
2.5mg
Price
$75
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB139551
Product name
3-Bromofluoranthene
Packaging
1g
Price
$74
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB139551
Product name
3-Bromofluoranthene
Packaging
2g
Price
$129
Updated
2021/12/16
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3-BROMOFLUORANTHENE Chemical Properties,Usage,Production

Uses

3-Bromofluoranthene is an intermediate in synthesizing 3-Methylfluoranthene (M305315), an environmental pollutant that is an active tumor initiator.

Synthesis

206-44-0

13438-50-1

Preparation of Compound 2-1: 50 g (247 mmol) of fluoranthene was dissolved in 1 L of nitrobenzene, and a dilute solution consisting of 12 mL (234.7 mmol) of bromine and 200 mL of nitrobenzene was added slowly and dropwise. After the dropwise addition, the reaction mixture was stirred at room temperature for 20 hours. Upon completion of the reaction, 500 mL of saturated aqueous sodium thiosulfate solution was added to quench the reaction. The reaction mixture was extracted with 3 L of ethyl acetate, followed by washing the organic phase with 1 L of distilled water. The organic layer was dried over anhydrous magnesium sulfate and concentrated under reduced pressure to remove the solvent. The crude product was filtered through silica gel column and purified by recrystallization to give the final compound 2-1 (65 g, 94% yield).

References

[1] Patent: WO2012/30145, 2012, A1. Location in patent: Page/Page column 15-16
[2] Patent: WO2013/32278, 2013, A1. Location in patent: Paragraph 94; 95
[3] Patent: KR2016/64432, 2016, A. Location in patent: Paragraph 0089-0091
[4] Journal of the American Chemical Society, 1966, vol. 88, # 24, p. 5837 - 5845
[5] Patent: US2011/34744, 2011, A1. Location in patent: Page/Page column 24

3-BROMOFLUORANTHENE Preparation Products And Raw materials

Raw materials

Preparation Products

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3-BROMOFLUORANTHENE Suppliers

J & K SCIENTIFIC LTD.
Tel
18210857532; 18210857532
Fax
86-10-82849933
Email
jkinfo@jkchemical.com
Country
China
ProdList
96815
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76
TCI (Shanghai) Development Co., Ltd.
Tel
021-67121386
Fax
021-67121385
Email
Sales-CN@TCIchemicals.com
Country
China
ProdList
24529
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81
Beijing Green Guardee Technology CO,.LTD
Tel
010-69706062-8011 15045616674
Fax
+86-10-69706062
Email
zhangr@greenguardee.com
Country
China
ProdList
295
Advantage
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Adamas Reagent, Ltd.
Tel
400-6009262 16621234537
Fax
021-64823266
Email
chenyj@titansci.com
Country
China
ProdList
14101
Advantage
59
Shanghai Hanhong Scientific Co.,Ltd.
Tel
021-54306202 13764082696
Email
info@hanhongsci.com
Country
China
ProdList
42934
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64
HANSHANG CHEMICAL SCIENTIFIC LIMITED
Tel
021-50521775 15800962688
Fax
86-21-58306291
Email
sales@hanshangchem.com
Country
China
ProdList
471
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China Langchem Inc.
Tel
0086-21-58956006
Fax
0086-21-58956100
Country
China
ProdList
7811
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Springchem New Material Technology Co.,Limited
Tel
+86-021-62885108 +8613917661608
Email
info@spring-chem.com
Country
China
ProdList
2068
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T&W GROUP
Tel
021-61551611 13296011611
Fax
+86 21-50676805
Email
contact@trustwe.com
Country
China
ProdList
9895
Advantage
58
Xi'an Manareco New Materials Co., Ltd.
Tel
029-68669089-8816
Fax
+86-29-68669073
Email
market@xarlm.com
Country
China
ProdList
499
Advantage
55
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View Lastest Price from 3-BROMOFLUORANTHENE manufacturers

ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD
Product
3-Bromofluoranthene 13438-50-1
Price
US $2.20-8.80/kg
Min. Order
1kg
Purity
99%min
Supply Ability
1000kg
Release date
2025-06-17
Hebei Xinsheng New Material Technology Co., LTD.
Product
3-BROMOFLUORANTHENE 13438-50-1
Price
US $35.00-25.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
20 Ton
Release date
2023-09-21
Hebei Xinsheng New Material Technology Co., LTD.
Product
3-BROMOFLUORANTHENE 13438-50-1
Price
US $35.00-25.00/kg
Min. Order
1kg
Purity
99%
Supply Ability
20 Ton
Release date
2023-11-02

13438-50-1, 3-BROMOFLUORANTHENERelated Search:


  • 3-BROMOFLUORANTHENE
  • Fluoranthene, 3-?bromo-
  • 3-Bromofluoranthene &gt
  • 3-Bromof|uoranthene
  • 13438-50-1